#------------------------------------------------------------------------------ #$Date: 2025-07-01 13:54:44 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1144 $ #$URL: svn://localhost/testcod/cif/7/70/00/7700023.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7700023 loop_ _publ_author_name 'Benjamin, Sophie L.' 'Chang, Yao-Pang' 'Hector, Andrew L.' 'Jura, Marek' 'Levason, William' 'Reid, Gillian' 'Stenning, Gavin' _publ_section_title ; Niobium tetrahalide complexes with neutral diphosphine ligands ; _journal_issue 19 _journal_name_full 'Dalton Transactions' _journal_page_first 8192 _journal_page_last 8200 _journal_paper_doi 10.1039/C6DT01099G _journal_volume 45 _journal_year 2016 _chemical_formula_analytical 'Br4 Nb' _chemical_formula_moiety 'Br4 Nb' _chemical_formula_structural 'Br4 Nb' _chemical_formula_sum 'Br4 Nb' _chemical_formula_weight 412.52 _chemical_name_common 'Niobium(IV) Tetrabromoide' _chemical_name_systematic 'Niobium(IV) Tetrabromoide' _space_group_IT_number 12 _space_group_name_Hall '-I 2y' _space_group_name_H-M_alt 'I 1 2/m 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-I 2y' _symmetry_space_group_name_H-M 'I 1 2/m 1' _audit_creation_date 2016-02-09T10:29 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ; 2016-02-15 deposited with the CCDC. 2016-04-11 downloaded from the CCDC. ; _cell_angle_alpha 90.0 _cell_angle_beta 92.212(4) _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 8.6119(6) _cell_length_b 7.1821(5) _cell_length_c 9.3626(8) _cell_measurement_temperature 298 _cell_volume 578.66(8) _computing_data_collection 'DIFFRAC.SUITE COMMANDER' _computing_data_reduction 'PowDLL Converter' _computing_publication_material GSAS _computing_structure_refinement GSAS _diffrn_ambient_temperature 298 _diffrn_detector '1D LYNXEYE' _diffrn_measurement_device_type 'Bruker D2 Phaser' _diffrn_radiation_monochromator none _diffrn_radiation_polarisn_ratio 0.7 _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_source 'sealed X-ray tube' _diffrn_source_target Cu _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_crystal_density_diffrn 4.735 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 724 _pd_block_id 2016-02-09T10:29|NBBR4_2|YP_Chang|D2_phaser _pd_calc_method 'Rietveld Refinement' _pd_char_colour Brown _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.02026 _pd_meas_2theta_range_max 84.99538 _pd_meas_2theta_range_min 13.002 _pd_meas_number_of_points 3555 _pd_phase_name 'from C:/GSAS/MyWork/NbCl4.cif' _pd_prep_cool_rate 0 _pd_prep_pressure 100 _pd_prep_temperature 298 _pd_proc_2theta_range_inc 0.02026 _pd_proc_2theta_range_max 84.86036 _pd_proc_2theta_range_min 12.86698 _pd_proc_info_datetime 2016-02-09T10:29:39 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 36 terms. Shifted Chebyshev function of 1st kind 1: 5633.33 2: -262.308 3: -573.988 4: 372.446 5: 433.322 6: -555.263 7: 415.686 8: -2.09579 9: -136.286 10: 250.245 11: 64.5635 12: -136.380 13: 45.9897 14: 80.3626 15: -1.43480 16: -154.686 17: 97.8114 18: -165.955 19: 182.124 20: -141.059 21: 76.1504 22: -11.9297 23: 73.8984 24: -102.286 25: 9.91100 26: 31.3136 27: -69.7405 28: 75.5684 29: -145.760 30: 168.715 31: -174.654 32: 98.8768 33: -55.8614 34: 101.608 35: -128.550 36: 96.4285 ; _pd_proc_ls_peak_cutoff 0.00010 _pd_proc_ls_profile_function ; CW Profile function number 2 with 18 terms Profile coefficients for Simpson's rule integration of pseudovoigt function C.J. Howard (1982). J. Appl. Cryst.,15,615-620. P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. #1(GU) = 882.863 #2(GV) = -161.687 #3(GW) = 23.032 #4(LX) = 30.179 #5(LY) = 1.000 #6(trns) = 0.000 #7(asym) = 0.0000 #8(shft) = 0.0000 #9(GP) = 0.000 #10(stec)= 0.00 #11(ptec)= 0.00 #12(sfec)= 0.00 #13(L11) = 0.000 #14(L22) = 0.000 #15(L33) = 0.000 #16(L12) = 0.000 #17(L13) = 0.000 #18(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0001 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0270 _pd_proc_ls_prof_wR_expected 0.0113 _pd_proc_ls_prof_wR_factor 0.0371 _pd_proc_number_of_points 3555 _pd_spec_mounting 'Aluminium plate' _pd_spec_mount_mode reflection _pd_spec_shape cylinder _pd_spec_size_axial 5 _pd_spec_size_equat 5 _pd_spec_size_thick 1 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_all 3.31 _refine_ls_hydrogen_treatment none _refine_ls_matrix_type full _refine_ls_number_constraints none _refine_ls_number_parameters 22 _refine_ls_number_restraints 0 _refine_ls_R_Fsqd_factor 0.04651 _refine_ls_shift/su_max 0.04 _refine_ls_shift/su_mean 0.01 _refine_ls_weighting_details 1/\s(Y~obs~)^2^ _refine_ls_weighting_scheme sigma _reflns_d_resolution_high 1.201 _reflns_d_resolution_low 6.459 _reflns_limit_h_max 9 _reflns_limit_h_min 0 _reflns_limit_k_max 7 _reflns_limit_k_min 0 _reflns_limit_l_max 9 _reflns_limit_l_min -9 _reflns_number_total 380 _cod_data_source_file c6dt01099g2.cif _cod_data_source_block NBBR4_2_publ _cod_original_cell_volume 578.65(9) _cod_database_code 7700023 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x,+y,-z -1 -x,-y,-z -2 +x,-y,+z 101 +x+1/2,+y+1/2,+z+1/2 102 -x+1/2,+y+1/2,-z+1/2 -101 -x+1/2,-y+1/2,-z+1/2 -102 +x+1/2,-y+1/2,+z+1/2 loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Nb Nb1 0.0 0.2168(7) 0.0 1.0 Uiso 0.0154(12) 4 Br Br1 0.0399(7) 0.0 0.2175(7) 1.0 Uiso 0.0285(23) 4 Br Br2 -0.27946(29) 0.2649(7) 0.02692(28) 1.0 Uiso 0.0246(11) 8 Br Br3 0.0261(7) 0.5 0.1951(6) 1.0 Uiso 0.0130(17) 4 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Nb 4.0 0.000 0.000 17.6142 1.18865 12.0144 11.7660 4.04183 0.20479 3.53346 69.7957 3.75591 International_Tables_Vol_C Br-1 16.0 0.000 0.000 17.1718 2.20590 6.33380 19.3345 5.57540 0.28710 3.72720 58.1535 3.17760 International_Tables_Vol_C loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Br1 Nb1 Br1 105.62(26) 1_555 . 2_555 N Br1 Nb1 Br2 96.04(14) 1_555 . 1_555 N Br1 Nb1 Br2 93.73(15) 1_555 . 2_555 N Br1 Nb1 Br3 85.21(8) 1_555 . 1_555 N Br1 Nb1 Br3 169.03(23) 1_555 . 2_555 N Br1 Nb1 Br2 93.73(15) 2_555 . 1_555 N Br1 Nb1 Br2 96.04(14) 2_555 . 2_555 N Br1 Nb1 Br3 169.03(23) 2_555 . 1_555 N Br1 Nb1 Br3 85.21(8) 2_555 . 2_555 N Br2 Nb1 Br2 163.81(19) 1_555 . 2_555 N Br2 Nb1 Br3 83.24(14) 1_555 . 1_555 N Br2 Nb1 Br3 84.74(15) 1_555 . 2_555 N Br2 Nb1 Br3 84.74(15) 2_555 . 1_555 N Br2 Nb1 Br3 83.24(14) 2_555 . 2_555 N Br3 Nb1 Br3 84.02(22) 1_555 . 2_555 N Nb1 Br1 Nb1 74.38(26) 1_555 . -1_555 N Nb1 Br3 Nb1 95.98(22) 1_555 . -1_565 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Nb1 Nb1 3.114(10) . -1_555 N Nb1 Br1 2.575(6) . 1_555 N Nb1 Br1 2.575(6) . 2_555 N Nb1 Br2 2.4540(25) . 1_555 N Nb1 Br2 2.4540(25) . 2_555 N Nb1 Br3 2.738(6) . 1_555 N Nb1 Br3 2.738(6) . 2_555 N Br1 Nb1 2.575(6) . 1_555 N Br1 Nb1 2.575(6) . -1_555 N Br1 Br3 3.5988(9) . 1_545 N Br1 Br3 3.5988(9) . 1_555 N Br2 Nb1 2.4540(25) . 1_555 N Br2 Br2 3.377(10) . -2_565 N Br2 Br3 3.455(6) . 1_555 N Br2 Br3 3.505(6) . 2_555 N Br3 Nb1 2.738(6) . 1_555 N Br3 Nb1 2.738(6) . -1_565 N Br3 Br1 3.5988(9) . 1_555 N Br3 Br1 3.5988(9) . 1_565 N Br3 Br2 3.455(6) . 1_555 N Br3 Br2 3.505(6) . 2_555 N Br3 Br2 3.505(6) . -1_565 N Br3 Br2 3.455(6) . -2_565 N loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 7744.0 0.0001291 6002.93066 6760.84033 7568.0 0.0001321 6373.32666 7164.04688 7682.0 0.0001302 6648.37451 7474.14258 7446.0 0.0001343 6840.40381 7703.67627 7524.0 0.0001329 6960.61279 7864.07813 7594.0 0.0001317 7019.14844 7965.76318 7530.0 0.0001328 7025.23730 8018.25000 7379.0 0.0001355 6987.21582 8030.21729 7530.0 0.0001328 6912.58789 8009.55615 7485.0 0.0001336 6808.11816 7963.46289 7518.0 0.0001330 6679.86084 7898.48730 7545.0 0.0001325 6533.22461 7820.61523 7626.0 0.0001311 6372.98633 7735.29395 7636.0 0.0001310 6203.44678 7647.58105 7537.0 0.0001327 6028.33154 7562.11523 7596.0 0.0001316 5850.90332 7483.23193 7694.0 0.0001300 5674.02979 7415.06299 7625.0 0.0001311 5500.19092 7361.60547 7702.0 0.0001298 5331.47607 7326.78418 7759.0 0.0001289 5169.64600 7314.61230 7898.0 0.0001266 5016.20508 7329.20117 7875.0 0.0001270 4872.35938 7375.00586 7968.0 0.0001255 4739.08545 7456.91211 8024.0 0.0001246 4617.11035 7580.33838 8024.0 0.0001246 4507.01074 7751.34863 8329.0 0.0001201 4409.15234 7976.79639 8726.0 0.0001146 4323.75830 8264.43652 8816.0 0.0001134 4250.89160 8622.96191 9143.0 0.0001094 4190.52734 9061.81836 9491.0 0.0001054 4142.49902 9591.34668 9853.0 0.0001015 4106.55566 10222.36719 10496.0 0.0000953 4082.37158 10965.54688 11237.0 0.0000890 4069.54517 11830.43750 12274.0 0.0000815 4067.61377 12823.82422 13492.0 0.0000741 4076.06738 13946.78418 15333.0 0.0000652 4094.35596 15190.11328 16700.0 0.0000599 4121.89795 16528.31445 18280.0 0.0000547 4158.08154 17912.83984 19746.0 0.0000506 4202.28906 19266.54297 21239.0 0.0000471 4253.87549 20484.56445 21648.0 0.0000462 4312.20117 21447.12891 22033.0 0.0000454 4376.61816 22045.45508 21934.0 0.0000456 4446.49512 22212.74219 21602.0 0.0000463 4521.17822 21946.20117 20925.0 0.0000478 4600.05273 21307.69531 20556.0 0.0000486 4682.51416 20402.86523 19622.0 0.0000510 4767.96143 19353.85938 18292.0 0.0000547 4855.80811 18263.05469 17106.0 0.0000585 4945.50586 17215.10352 15923.0 0.0000628 5036.52881 16264.35547 15002.0 0.0000667 5128.35400 15443.42578 14281.0 0.0000700 5220.49609 14764.57910 13932.0 0.0000718 5312.49170 14233.75977 13649.0 0.0000733 5403.91602 13850.13574 13477.0 0.0000742 5494.34619 13610.50098 13177.0 0.0000759 5583.40625 13511.08691 13238.0 0.0000755 5670.73193 13548.51953 13303.0 0.0000752 5756.01367 13720.28516 13305.0 0.0000752 5838.92188 14024.37988 13875.0 0.0000721 5919.19141 14458.70020 14170.0 0.0000706 5996.57910 15019.49023 15240.0 0.0000656 6070.85059 15698.69434 16131.0 0.0000620 6141.79736 16480.23633 17283.0 0.0000579 6209.25000 17335.19531 18173.0 0.0000550 6273.05957 18216.54297 19443.0 0.0000514 6333.08691 19056.11133 20069.0 0.0000498 6389.21729 19767.90625 20276.0 0.0000493 6441.36865 20260.87500 20527.0 0.0000487 6489.47314 20459.88086 19889.0 0.0000503 6533.47559 20327.69336 19446.0 0.0000514 6573.34570 19876.68555 18591.0 0.0000538 6609.06787 19163.44727 17958.0 0.0000557 6640.64453 18270.42188 16881.0 0.0000592 6668.08789 17283.68164 15794.0 0.0000633 6691.43408 16276.28320 14978.0 0.0000668 6710.72510 15300.98926 14326.0 0.0000698 6726.01758 14390.46289 13762.0 0.0000727 6737.37842 13561.19238 13095.0 0.0000764 6744.88818 12818.34082 12912.0 0.0000774 6748.63623 12160.11719 12924.0 0.0000774 6748.71777 11580.90820 12887.0 0.0000776 6745.24072 11073.20605 12384.0 0.0000807 6738.31689 10628.80957 12188.0 0.0000820 6728.06543 10239.49316 11619.0 0.0000861 6714.61230 9897.64746 10999.0 0.0000909 6698.08643 9596.29980 10404.0 0.0000961 6678.62354 9329.19434 9681.0 0.0001033 6656.35986 9090.89941 8977.0 0.0001114 6631.43994 8876.76270 8651.0 0.0001156 6604.00244 8683.77344 8193.0 0.0001221 6574.19385 8506.69922 7861.0 0.0001272 6542.15918 8343.76563 7592.0 0.0001317 6508.04932 8192.73047 7553.0 0.0001324 6472.00732 8052.21387 7504.0 0.0001333 6434.17725 7919.76367 7307.0 0.0001369 6394.70654 7794.63818 7457.0 0.0001341 6353.74414 7675.85498 7535.0 0.0001327 6311.42822 7562.60010 7483.0 0.0001336 6267.89551 7454.93164 7696.0 0.0001299 6223.29053 7350.86182 7676.0 0.0001303 6177.74756 7250.67236 7792.0 0.0001283 6131.39795 7153.99561 7587.0 0.0001318 6084.36865 7060.88574 7524.0 0.0001329 6036.79346 6970.38232 7528.0 0.0001328 5988.78711 6882.63184 7571.0 0.0001321 5940.47168 6797.46143 7069.0 0.0001415 5891.95752 6714.73584 6883.0 0.0001453 5843.36328 6634.35547 6747.0 0.0001482 5794.79004 6556.21924 6773.0 0.0001476 5746.33496 6480.25586 6346.0 0.0001576 5698.10010 6406.41748 6117.0 0.0001635 5650.18213 6334.67041 6087.0 0.0001643 5602.66553 6264.98975 5948.0 0.0001681 5555.62646 6197.34668 5689.0 0.0001758 5509.15723 6131.75977 5836.0 0.0001714 5463.32373 6068.23047 5590.0 0.0001789 5418.19727 6006.77197 5546.0 0.0001803 5373.84082 5947.41064 5416.0 0.0001846 5330.32080 5890.19043 5528.0 0.0001809 5287.68799 5835.14404 5502.0 0.0001818 5245.99365 5782.31836 5445.0 0.0001837 5205.28467 5731.77002 5395.0 0.0001854 5165.60840 5683.55176 5415.0 0.0001847 5127.00000 5637.70898 5459.0 0.0001832 5089.48877 5594.27295 5415.0 0.0001847 5053.10986 5553.35498 5392.0 0.0001855 5017.89160 5514.73486 5413.0 0.0001847 4983.85303 5478.39551 5460.0 0.0001832 4951.00781 5444.11963 5386.0 0.0001857 4919.37842 5411.57813 5302.0 0.0001886 4888.97461 5380.31055 5239.0 0.0001909 4859.80127 5349.80371 5277.0 0.0001895 4831.86230 5319.58984 5297.0 0.0001888 4805.16406 5289.40918 5299.0 0.0001887 4779.70068 5259.28271 5206.0 0.0001921 4755.46826 5229.52539 5247.0 0.0001906 4732.45947 5200.67529 5317.0 0.0001881 4710.66699 5173.36475 5136.0 0.0001947 4690.07520 5148.20117 5315.0 0.0001881 4670.67139 5125.71484 5283.0 0.0001893 4652.43701 5106.34033 5175.0 0.0001932 4635.35547 5090.45068 5097.0 0.0001962 4619.40527 5078.36230 5122.0 0.0001952 4604.56055 5070.38672 5190.0 0.0001927 4590.80127 5066.85156 5242.0 0.0001908 4578.10059 5068.09375 5216.0 0.0001917 4566.42969 5074.47998 5249.0 0.0001905 4555.76025 5086.38281 5161.0 0.0001938 4546.06494 5104.15186 5131.0 0.0001949 4537.31055 5128.06543 5226.0 0.0001914 4529.46582 5158.24170 5358.0 0.0001866 4522.49902 5194.49072 5183.0 0.0001929 4516.37695 5236.09082 5261.0 0.0001901 4511.06592 5281.54834 5304.0 0.0001885 4506.53027 5328.30615 5215.0 0.0001918 4502.73682 5372.62061 5119.0 0.0001954 4499.65137 5409.77051 5300.0 0.0001887 4497.23730 5434.79590 5235.0 0.0001910 4495.45947 5443.64307 5151.0 0.0001941 4494.28369 5434.33105 5225.0 0.0001914 4493.67383 5407.54688 5104.0 0.0001959 4493.59619 5366.36621 5232.0 0.0001911 4494.01465 5315.28857 5103.0 0.0001960 4494.89551 5259.08057 5029.0 0.0001988 4496.20459 5201.86133 5050.0 0.0001980 4497.90820 5146.65820 5062.0 0.0001976 4499.97266 5095.40039 5030.0 0.0001988 4502.36621 5049.09131 5044.0 0.0001983 4505.05664 5008.08203 5068.0 0.0001973 4508.01221 4972.29834 5098.0 0.0001962 4511.20215 4941.43213 4950.0 0.0002020 4514.59717 4915.05664 5133.0 0.0001948 4518.16748 4892.68262 5060.0 0.0001976 4521.88525 4873.82959 5059.0 0.0001977 4525.72266 4858.03467 5067.0 0.0001974 4529.65332 4844.86377 4963.0 0.0002015 4533.65186 4833.93359 4883.0 0.0002048 4537.69287 4824.89355 5097.0 0.0001962 4541.75195 4817.44775 4975.0 0.0002010 4545.80762 4811.34131 5007.0 0.0001997 4549.83789 4806.34424 4847.0 0.0002063 4553.82080 4802.26855 5002.0 0.0001999 4557.73730 4798.95947 4794.0 0.0002086 4561.56836 4796.27930 4942.0 0.0002023 4565.29590 4794.11816 4876.0 0.0002051 4568.90332 4792.37695 4918.0 0.0002033 4572.37451 4790.97461 4913.0 0.0002035 4575.69482 4789.84521 4739.0 0.0002110 4578.85107 4788.92920 4884.0 0.0002048 4581.82910 4788.17236 4919.0 0.0002033 4584.61768 4787.52832 4886.0 0.0002047 4587.20654 4786.96484 4784.0 0.0002090 4589.58496 4786.43994 4817.0 0.0002076 4591.74414 4785.92969 4950.0 0.0002020 4593.67627 4785.40479 4954.0 0.0002019 4595.37500 4784.84180 4821.0 0.0002074 4596.83252 4784.22314 4798.0 0.0002084 4598.04492 4783.52832 4846.0 0.0002064 4599.00732 4782.74561 4716.0 0.0002120 4599.71631 4781.85547 4910.0 0.0002037 4600.16895 4780.85645 4908.0 0.0002037 4600.36279 4779.72754 4735.0 0.0002112 4600.29785 4778.47217 4898.0 0.0002042 4599.97266 4777.08008 4776.0 0.0002094 4599.38770 4775.54150 4857.0 0.0002059 4598.54443 4773.85742 4755.0 0.0002103 4597.44385 4772.02734 4779.0 0.0002092 4596.08838 4770.04834 4746.0 0.0002107 4594.48145 4767.91846 4754.0 0.0002103 4592.62598 4765.64355 4713.0 0.0002122 4590.52637 4763.22070 4773.0 0.0002095 4588.18701 4760.65527 4634.0 0.0002158 4585.61328 4757.95313 4729.0 0.0002115 4582.81006 4755.11328 4637.0 0.0002157 4579.78369 4752.14697 4727.0 0.0002116 4576.54102 4749.05469 4593.0 0.0002177 4573.08887 4745.85010 4830.0 0.0002070 4569.43408 4742.53467 4812.0 0.0002078 4565.58350 4739.11816 4797.0 0.0002085 4561.54639 4735.61133 4720.0 0.0002119 4557.33057 4732.02100 4659.0 0.0002146 4552.94336 4728.35889 4621.0 0.0002164 4548.39355 4724.63281 4689.0 0.0002133 4543.69141 4720.85645 4540.0 0.0002203 4538.84521 4717.04150 4616.0 0.0002166 4533.86279 4713.19434 4668.0 0.0002142 4528.75488 4709.33203 4625.0 0.0002162 4523.53076 4705.46826 4685.0 0.0002134 4518.20020 4701.61035 4794.0 0.0002086 4512.77148 4697.77637 4661.0 0.0002145 4507.25488 4693.97754 4733.0 0.0002113 4501.66016 4690.23193 4716.0 0.0002120 4495.99658 4686.55029 4676.0 0.0002139 4490.27393 4682.94873 4558.0 0.0002194 4484.50195 4679.44531 4690.0 0.0002132 4478.68994 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0.0002136 4341.15088 4700.55078 4751.0 0.0002105 4337.25586 4710.15527 4647.0 0.0002152 4333.51123 4720.94629 4818.0 0.0002076 4329.92139 4733.02734 4817.0 0.0002076 4326.48779 4746.51660 4728.0 0.0002115 4323.21436 4761.54932 4774.0 0.0002095 4320.10254 4778.27490 4752.0 0.0002104 4317.15430 4796.85889 4821.0 0.0002074 4314.37158 4817.50684 5014.0 0.0001994 4311.75635 4840.43701 5111.0 0.0001957 4309.30908 4865.90869 4816.0 0.0002076 4307.03125 4894.22461 4974.0 0.0002010 4304.92334 4925.73975 5117.0 0.0001954 4302.98633 4960.87744 5037.0 0.0001985 4301.22021 5000.13232 5233.0 0.0001911 4299.62500 5044.11084 5274.0 0.0001896 4298.20020 5093.54102 5248.0 0.0001905 4296.94580 5149.29736 5265.0 0.0001899 4295.86133 5212.44482 5325.0 0.0001878 4294.94580 5284.26953 5456.0 0.0001833 4294.19775 5366.34668 5461.0 0.0001831 4293.61670 5460.48438 5616.0 0.0001781 4293.20068 5568.88330 5693.0 0.0001757 4292.94824 5694.11230 5632.0 0.0001776 4292.85791 5839.13867 5982.0 0.0001672 4292.92725 6007.28467 6181.0 0.0001618 4293.15479 6202.27002 6170.0 0.0001621 4293.53857 6428.15771 6642.0 0.0001506 4294.07520 6689.17969 6841.0 0.0001462 4294.76270 6989.56885 7325.0 0.0001365 4295.59863 7333.25488 7542.0 0.0001326 4296.58057 7723.27637 8064.0 0.0001240 4297.70508 8160.81006 8698.0 0.0001150 4298.96924 8643.79883 9226.0 0.0001084 4300.37061 9165.06543 9618.0 0.0001040 4301.90576 9709.82617 10292.0 0.0000972 4303.57178 10253.44043 10621.0 0.0000942 4305.36475 10760.54883 10980.0 0.0000911 4307.28223 11187.82129 10996.0 0.0000909 4309.32031 11490.59961 11168.0 0.0000895 4311.47656 11633.05566 11068.0 0.0000904 4313.74609 11598.00195 10826.0 0.0000924 4316.12646 11391.44238 10495.0 0.0000953 4318.61328 11040.35059 10121.0 0.0000988 4321.20410 10584.87012 9711.0 0.0001030 4323.89502 10068.62793 9344.0 0.0001070 4326.68262 9530.81543 8802.0 0.0001136 4329.56348 9001.77148 8302.0 0.0001205 4332.53320 8501.91602 7984.0 0.0001253 4335.58936 8042.92139 7599.0 0.0001316 4338.72803 7629.95068 7266.0 0.0001376 4341.94629 7263.85498 6999.0 0.0001429 4345.23975 6942.80029 6757.0 0.0001480 4348.60596 6663.43066 6522.0 0.0001533 4352.04150 6421.70264 6333.0 0.0001579 4355.54297 6213.43164 6232.0 0.0001605 4359.10645 6034.42773 6012.0 0.0001663 4362.72998 5880.77637 5791.0 0.0001727 4366.40918 5748.90576 5583.0 0.0001791 4370.14258 5635.63867 5457.0 0.0001833 4373.92529 5538.16260 5443.0 0.0001837 4377.75684 5454.06641 5374.0 0.0001861 4381.63184 5381.29541 5222.0 0.0001915 4385.54932 5318.12793 5161.0 0.0001938 4389.50586 5263.11523 5160.0 0.0001938 4393.49902 5215.05811 5190.0 0.0001927 4397.52686 5172.97754 5023.0 0.0001991 4401.58643 5136.06201 4930.0 0.0002028 4405.67529 5103.63281 5113.0 0.0001956 4409.79199 5075.14063 5065.0 0.0001974 4413.93359 5050.12988 5054.0 0.0001979 4418.09766 5028.21045 4948.0 0.0002021 4422.28418 5009.06543 5155.0 0.0001940 4426.48975 4992.41992 4976.0 0.0002010 4430.71289 4978.05127 5121.0 0.0001953 4434.95215 4965.76123 4931.0 0.0002028 4439.20654 4955.38574 4936.0 0.0002026 4443.47412 4946.79102 5081.0 0.0001968 4447.75342 4939.93115 4988.0 0.0002005 4452.04346 4934.55713 5130.0 0.0001949 4456.34326 4930.66211 5126.0 0.0001951 4460.65186 4928.18994 5175.0 0.0001932 4464.96729 4927.08691 5338.0 0.0001873 4469.29004 4927.41992 5340.0 0.0001873 4473.61963 4928.96729 5490.0 0.0001821 4477.95361 4931.81738 5491.0 0.0001821 4482.29297 4935.98291 5665.0 0.0001765 4486.63721 4941.89355 5800.0 0.0001724 4490.98535 4948.78564 5715.0 0.0001750 4495.33789 4957.05518 5827.0 0.0001716 4499.69385 4966.80273 5728.0 0.0001746 4504.05371 4978.11816 5688.0 0.0001758 4508.41699 4991.31104 5524.0 0.0001810 4512.78467 5006.09521 5641.0 0.0001773 4517.15576 5022.84912 5515.0 0.0001813 4521.53174 5041.77197 5613.0 0.0001782 4525.91211 5063.10400 5388.0 0.0001856 4530.29688 5087.14893 5474.0 0.0001827 4534.68750 5114.27588 5325.0 0.0001878 4539.08447 5144.94092 5200.0 0.0001923 4543.48682 5179.68701 5145.0 0.0001944 4547.89697 5219.18896 5259.0 0.0001902 4552.31494 5264.26074 5376.0 0.0001860 4556.74170 5315.87207 5287.0 0.0001891 4561.17725 5375.18408 5310.0 0.0001883 4565.62354 5443.54053 5474.0 0.0001827 4570.08057 5522.51367 5414.0 0.0001847 4574.55029 5613.87695 5443.0 0.0001837 4579.03223 5719.60254 5664.0 0.0001766 4583.52832 5841.84912 5753.0 0.0001738 4588.03906 5982.88281 5925.0 0.0001688 4592.56641 6145.00732 6196.0 0.0001614 4597.11133 6330.42090 6315.0 0.0001584 4601.67334 6541.27441 6651.0 0.0001504 4606.25537 6777.71680 7007.0 0.0001427 4610.85840 7039.76953 7209.0 0.0001387 4615.48145 7324.38770 7593.0 0.0001317 4620.12842 7625.34326 7915.0 0.0001263 4624.79932 7931.54785 8325.0 0.0001201 4629.49365 8225.71973 8307.0 0.0001204 4634.21631 8486.43359 8521.0 0.0001174 4638.96484 8689.39258 8493.0 0.0001177 4643.74170 8812.88770 8459.0 0.0001182 4648.54883 8842.87793 8330.0 0.0001200 4653.38477 8776.70117 8236.0 0.0001214 4658.25391 8623.46777 8033.0 0.0001245 4663.15576 8401.33984 7527.0 0.0001329 4668.08984 8133.00146 7523.0 0.0001329 4673.06006 7840.85400 7199.0 0.0001389 4678.06543 7544.05127 6932.0 0.0001443 4683.10596 7256.80029 6552.0 0.0001526 4688.18506 6988.23291 6336.0 0.0001578 4693.30225 6743.12109 6312.0 0.0001584 4698.45850 6523.52881 6138.0 0.0001629 4703.65430 6329.38086 6016.0 0.0001662 4708.88965 6159.49072 5924.0 0.0001688 4714.16797 6011.93994 5714.0 0.0001750 4719.48682 5884.41357 5651.0 0.0001770 4724.84717 5774.73242 5548.0 0.0001802 4730.25146 5680.60059 5363.0 0.0001865 4735.69824 5599.97803 5424.0 0.0001844 4741.18945 5530.94971 5285.0 0.0001892 4746.72412 5471.80762 5237.0 0.0001909 4752.30225 5421.08252 5114.0 0.0001955 4757.92529 5377.47852 5202.0 0.0001922 4763.59326 5339.89746 5217.0 0.0001917 4769.30469 5307.43408 5078.0 0.0001969 4775.06104 5279.30518 5019.0 0.0001992 4780.86279 5254.87305 5119.0 0.0001954 4786.70654 5233.62451 5126.0 0.0001951 4792.59668 5215.10498 5080.0 0.0001969 4798.52979 5198.96484 5030.0 0.0001988 4804.50586 5184.89600 5050.0 0.0001980 4810.52588 5172.65137 5051.0 0.0001980 4816.58740 5162.02490 4964.0 0.0002015 4822.69141 5152.82520 4956.0 0.0002018 4828.83691 5144.90820 5062.0 0.0001976 4835.02197 5138.14307 5024.0 0.0001990 4841.24854 5132.40723 4979.0 0.0002008 4847.51318 5127.60596 4875.0 0.0002051 4853.81494 5123.65576 4754.0 0.0002103 4860.15479 5120.47217 5097.0 0.0001962 4866.53076 5117.99023 4976.0 0.0002010 4872.94092 5116.15186 4968.0 0.0002013 4879.38477 5114.89453 5024.0 0.0001990 4885.86035 5114.17676 4858.0 0.0002058 4892.36816 5113.95068 5036.0 0.0001986 4898.90527 5114.18115 5156.0 0.0001939 4905.46875 5114.82861 4983.0 0.0002007 4912.06006 5115.89502 5098.0 0.0001962 4918.67578 5117.28418 4918.0 0.0002033 4925.31494 5119.00635 5270.0 0.0001898 4931.97559 5121.03027 5113.0 0.0001956 4938.65576 5123.33691 5183.0 0.0001929 4945.35303 5125.92432 5157.0 0.0001939 4952.06787 5128.73682 5265.0 0.0001899 4958.79443 5131.77490 5551.0 0.0001801 4965.53467 5135.02588 5364.0 0.0001864 4972.28467 5138.46729 5372.0 0.0001862 4979.04004 5142.08984 5453.0 0.0001834 4985.80371 5145.87988 5473.0 0.0001827 4992.56885 5149.82617 5583.0 0.0001791 4999.33545 5153.91357 5502.0 0.0001818 5006.10156 5158.13477 5440.0 0.0001838 5012.86328 5162.48291 5311.0 0.0001883 5019.61865 5166.93750 5288.0 0.0001891 5026.36670 5171.49658 5407.0 0.0001849 5033.10205 5176.15381 5093.0 0.0001963 5039.82617 5180.89746 5229.0 0.0001912 5046.53418 5185.71777 5183.0 0.0001929 5053.22217 5190.60938 5052.0 0.0001979 5059.89111 5195.59863 5034.0 0.0001986 5066.53564 5200.61328 5094.0 0.0001963 5073.15430 5205.67822 5086.0 0.0001966 5079.74463 5210.79102 5202.0 0.0001922 5086.30225 5215.94043 5019.0 0.0001992 5092.82813 5221.13867 4921.0 0.0002032 5099.31689 5226.35156 4837.0 0.0002067 5105.76563 5231.87061 5115.0 0.0001955 5112.17334 5237.11914 4977.0 0.0002009 5118.53760 5242.38037 4984.0 0.0002006 5124.85303 5247.64746 4978.0 0.0002009 5131.11963 5252.91553 5064.0 0.0001975 5137.33398 5258.18457 5216.0 0.0001917 5143.49316 5263.58398 5287.0 0.0001891 5149.59619 5268.83350 5417.0 0.0001846 5155.63818 5274.06836 5403.0 0.0001851 5161.61816 5279.28174 5390.0 0.0001855 5167.53369 5284.47217 5404.0 0.0001850 5173.38037 5289.63281 5397.0 0.0001853 5179.15820 5294.78564 5438.0 0.0001839 5184.86279 5299.88184 5389.0 0.0001856 5190.49268 5305.30566 5334.0 0.0001875 5196.04688 5310.32324 5513.0 0.0001814 5201.52051 5315.29590 5488.0 0.0001822 5206.91211 5320.22217 5331.0 0.0001876 5212.22021 5325.10596 5324.0 0.0001878 5217.44141 5330.10400 5284.0 0.0001893 5222.57568 5334.86816 5333.0 0.0001875 5227.61914 5339.57422 5447.0 0.0001836 5232.56934 5344.21387 5402.0 0.0001851 5237.42627 5348.79492 5362.0 0.0001865 5242.18604 5353.30615 5329.0 0.0001877 5246.84766 5357.74609 5507.0 0.0001816 5251.40967 5362.11719 5316.0 0.0001881 5255.86865 5366.41260 5429.0 0.0001842 5260.22607 5370.63330 5392.0 0.0001855 5264.47754 5374.77930 5255.0 0.0001903 5268.62207 5378.84375 5408.0 0.0001849 5272.65918 5382.84326 5364.0 0.0001864 5276.58740 5386.74756 5396.0 0.0001853 5280.40332 5390.56689 5400.0 0.0001852 5284.10840 5394.29883 5360.0 0.0001866 5287.69971 5397.94873 5485.0 0.0001823 5291.17676 5401.51025 5338.0 0.0001873 5294.53906 5404.99805 5431.0 0.0001841 5297.78418 5408.38037 5404.0 0.0001850 5300.91309 5411.67822 5498.0 0.0001819 5303.92432 5414.88428 5473.0 0.0001827 5306.81641 5418.00293 5448.0 0.0001836 5309.58984 5421.03125 5382.0 0.0001858 5312.24365 5423.96826 5378.0 0.0001859 5314.77734 5426.81299 5333.0 0.0001875 5317.19141 5429.56982 5353.0 0.0001868 5319.48438 5432.23730 5435.0 0.0001840 5321.65674 5434.81494 5427.0 0.0001843 5323.70898 5437.30566 5303.0 0.0001886 5325.63965 5439.70752 5370.0 0.0001862 5327.45020 5442.02637 5460.0 0.0001832 5329.14063 5444.25439 5280.0 0.0001894 5330.71094 5446.40137 5517.0 0.0001813 5332.16211 5448.46582 5428.0 0.0001842 5333.49365 5450.44629 5369.0 0.0001863 5334.70703 5452.34912 5268.0 0.0001898 5335.80273 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0.0001619 5327.39746 5488.00684 6244.0 0.0001602 5325.90479 5489.66113 6027.0 0.0001659 5324.34912 5491.45264 6151.0 0.0001626 5322.73438 5493.40234 6054.0 0.0001652 5321.06250 5495.52588 5946.0 0.0001682 5319.33691 5497.84619 5896.0 0.0001696 5317.56152 5500.39355 6016.0 0.0001662 5315.73975 5503.19434 5860.0 0.0001706 5313.87402 5506.28223 5694.0 0.0001756 5311.96826 5509.68750 5668.0 0.0001764 5310.02588 5513.50391 5584.0 0.0001791 5308.05029 5517.67627 5526.0 0.0001810 5306.04492 5522.30566 5728.0 0.0001746 5304.01367 5527.44824 5565.0 0.0001797 5301.95996 5533.16943 5571.0 0.0001795 5299.88770 5539.57324 5543.0 0.0001804 5297.80029 5546.70996 5557.0 0.0001800 5295.70117 5554.67773 5507.0 0.0001816 5293.59424 5563.62109 5470.0 0.0001828 5291.48438 5573.67432 5557.0 0.0001800 5289.37354 5585.01855 5367.0 0.0001863 5287.26660 5597.86035 5540.0 0.0001805 5285.16797 5612.42578 5312.0 0.0001883 5283.07959 5629.02295 5266.0 0.0001899 5281.00732 5647.99023 5375.0 0.0001860 5278.95410 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0.0001636 5484.73486 6025.41992 5941.0 0.0001683 5484.52002 6035.78320 5870.0 0.0001704 5486.11084 6048.96973 5868.0 0.0001704 5490.11328 6065.60596 6025.0 . . . 6048.0 . . . 6043.0 . . . 6091.0 . . . 6139.0 . . . 6021.0 . . . 5917.0 . . . 6143.0 . . . 6192.0 . . . 6189.0 . . . 6085.0 . . . 6136.0 . . . 6153.0 . . . 6173.0 . . . 6209.0 . . . 6226.0 . . . 6279.0 . . . 6455.0 . . . 6476.0 . . . 6377.0 . . . 6425.0 . . . 6603.0 . . . 6525.0 . . . 6505.0 . . . 6587.0 . . . 6628.0 . . . 6638.0 . . . 6667.0 . . . 6755.0 . . . 6814.0 . . . 6699.0 . . . 6752.0 . . . 6776.0 . . . 6828.0 . . . 6741.0 . . . 6638.0 . . . 6733.0 . . . 6776.0 . . . 6732.0 . . . 6600.0 . . . 6685.0 . . . 6533.0 . . . 5938.0 . . . 6711.0 . . . 6586.0 . . . 6447.0 . . . 6549.0 . . . 6515.0 . . . 6398.0 . . . 6512.0 . . . 6351.0 . . . 6459.0 . . . 6415.0 . . . 6457.0 . . . 6379.0 . . . 6337.0 . . . 6262.0 . . . 6340.0 . . . 6387.0 . . . 6395.0 . . . 6270.0 . . . 6209.0 . . . 6436.0 . . . 6285.0 . . . 6329.0 . . . 6420.0 . . . 6250.0 . . . 6552.0 . . . 6636.0 . . . 6650.0 . . . 6589.0 . . . 6618.0 . . . 6820.0 . . . 6971.0 . . . 6800.0 . . . 6854.0 . . . 7082.0 . . . 7105.0 . . . 7375.0 . . . 7410.0 . . . 7621.0 . . . 7734.0 . . . 7822.0 . . . 7881.0 . . . 8348.0 . . . 8410.0 . . . 8636.0 . . . 8927.0 . . . 9134.0 . . . 9533.0 . . . 10201.0 . . . 10703.0 . . . 11854.0 . . . 12995.0 . . . 14596.0 . . . 16687.0 . . . 19405.0 . . . 22782.0 . . . 26943.0 . . . 31412.0 . . . 35721.0 . . . 39037.0 . . . 41780.0 . . . 42777.0 . . . 41085.0 . . . 38657.0 . . . 35318.0 . . . 31874.0 . . . 28934.0 . . . 27299.0 . . . 26311.0 . . . 25790.0 . . . 26450.0 . . . 27163.0 . . . 27688.0 . . . 27312.0 . . . 26612.0 . . . 24918.0 . . . 22731.0 . . . 20201.0 . . . 17986.0 . . . 15816.0 . . . 14379.0 . . . 12919.0 . . . 11927.0 . . . 11059.0 . . . 10554.0 . . . 10091.0 . . . 9760.0 . . . 9380.0 . . . 9360.0 . . . 8860.0 . . . 8764.0 . . . 8614.0 . . . 8460.0 . . . 8314.0 . . . 8300.0 . . . 8094.0 . . . 8072.0 . . . 7911.0 . . . 7839.0 . . . 7762.0 . . . 7911.0 . . . 7813.0 . . . 7769.0 . . . 7606.0 . . . 7676.0 . . . 7573.0 . . . 7799.0 . . . 7662.0 . . . 7555.0 . . . 7513.0 . . . 7471.0 . . . 7654.0 . . . 7688.0 . . . 7576.0 . . . 7971.0 . . . 7709.0 . . . 7588.0 . . . 7642.0 . . . 7626.0 . . . 7659.0 . . . 7651.0 . . . 7722.0 . . . 7505.0 . . . 7626.0 . . . 7653.0 . . . 7408.0 . . . 7502.0 . . . 7365.0 . . . 7553.0 . . . 7448.0 . . . 7403.0 . . . 7338.0 . . . 7435.0 . . . 7281.0 . . . 7380.0 . . . 7288.0 . . . 7151.0 . . . 7096.0 . . . 7114.0 . . . 7033.0 . . . 7033.0 . . . 7146.0 . . . 6960.0 . . . 7041.0 . . . 6969.0 . . . 7006.0 . . . 7043.0 . . . 6973.0 . . . 7049.0 . . . 7030.0 . . . 6913.0 . . . 6831.0 . . . 6897.0 . . . 6786.0 . . . 6887.0 . . . 6814.0 . . . 6929.0 . . . 6806.0 . . . 6921.0 . . . 6896.0 . . . 6849.0 . . . 6803.0 . . . 6778.0 . . . 6854.0 . . . 6773.0 . . . 7074.0 . . . 6944.0 . . . 6734.0 . . . 6733.0 . . . 6893.0 . . . 6738.0 . . . 6840.0 . . . 6791.0 . . . 6707.0 . . . 6916.0 . . . 6696.0 . . . 6798.0 . . . 6686.0 . . . 6622.0 . . . 6646.0 . . . 6603.0 . . . 6798.0 . . . 6611.0 . . . 6690.0 . . . 6545.0 . . . 6357.0 . . . 6386.0 . . . 6458.0 . . . 6319.0 . . . 6402.0 . . . 6247.0 . . . 6445.0 . . . 6338.0 . . . 6266.0 . . . 6295.0 . . . 6273.0 . . . 6130.0 . . . 6309.0 . . . 6183.0 . . . 6091.0 . . . 6334.0 . . . 6060.0 . . . 6169.0 . . . 6151.0 . . . 6144.0 . . . loop_ _gsas_i100_meas 37.89 18.82 28.90 14.48 0.17 0.09 1.66 0.83 16.85 8.39 9.28 4.54 0.15 0.07 0.41 0.21 1.47 0.74 4.80 2.44 0.16 0.08 7.50 3.74 1.61 0.81 5.40 23.24 2.68 11.54 9.12 4.58 1.16 0.57 0.74 0.37 100.00 49.90 1.94 37.49 18.58 28.30 14.04 0.00 0.00 3.89 0.59 0.30 1.54 0.81 0.04 4.06 0.02 3.06 1.90 19.34 1.46 9.38 0.30 0.14 18.60 1.98 9.33 0.95 5.73 2.87 0.22 0.11 1.38 0.69 1.36 0.69 12.54 6.39 0.97 16.87 0.49 8.56 0.83 0.41 0.11 0.05 1.99 0.99 0.73 0.37 0.84 0.43 2.68 1.38 3.92 1.83 0.04 0.02 0.46 1.35 0.23 5.13 0.12 2.48 0.06 2.66 0.80 0.38 0.01 0.00 29.41 1.86 1.38 14.82 0.94 0.70 0.57 0.29 3.62 1.90 0.73 0.08 0.39 0.04 6.03 2.99 1.29 0.32 0.65 0.08 0.91 0.16 0.48 0.04 0.46 0.24 0.97 0.47 20.72 0.20 10.14 0.10 0.10 0.61 0.05 0.30 0.86 0.42 0.63 0.00 0.31 0.00 0.79 0.39 0.41 0.02 0.29 0.20 0.01 0.15 0.29 4.47 0.15 2.25 0.00 0.00 8.73 0.24 4.34 0.12 0.12 0.06 0.26 1.88 0.13 0.93 2.00 0.41 1.02 5.63 8.06 0.21 2.83 4.03 1.21 3.87 0.60 2.58 1.92 1.27 2.08 7.67 0.03 1.02 3.72 0.04 0.75 0.02 0.41 0.37 0.20 0.28 0.14 0.06 0.87 0.17 0.45 0.09 0.22 2.39 0.11 1.15 0.00 0.00 0.75 0.39 0.17 0.09 0.10 0.05 0.29 0.11 0.06 0.14 0.66 1.87 0.03 0.41 0.13 0.15 0.94 0.31 0.86 0.19 0.06 0.08 4.76 0.44 2.41 0.00 0.01 1.01 0.58 0.00 0.01 0.22 0.51 0.28 0.41 0.16 0.01 0.21 0.08 1.31 0.00 0.07 4.87 0.65 0.04 2.43 0.01 0.00 0.00 0.09 0.00 0.05 0.00 0.34 1.10 0.00 0.18 0.12 0.61 0.56 0.47 0.06 0.30 0.01 0.04 0.53 1.34 0.21 0.60 0.02 0.23 0.59 0.78 0.30 0.11 1.01 0.39 0.08 0.01 0.06 0.11 0.48 0.04 0.00 0.05 0.02 0.00 0.16 0.28 0.00 0.08 0.15 0.23 0.10 0.07 1.22 0.03 0.55 0.07 0.07 0.04 0.04 0.92 0.46 0.45 0.45 0.04 0.00 0.47 0.23 0.22 0.23 0.02 0.36 0.18 3.95 1.95 1.00 0.01 0.52 0.20 0.01 0.07 0.11 0.45 1.86 0.10 0.01 0.03 0.05 0.57 0.22 0.90 0.28 0.37 0.13 5.12 0.19 0.34 0.07 2.63 0.41 0.18 0.62 0.14 0.22 0.50 0.60 0.74 0.07 0.21 0.32 0.14 0.11 0.32 3.58 0.37 0.03 0.29 0.07 0.16 1.77 0.14 0.15 0.19 0.29 0.07 0.04 1.01 1.20