#------------------------------------------------------------------------------ #$Date: 2025-07-01 13:49:47 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1130 $ #$URL: svn://localhost/testcod/cif/7/70/00/7700004.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7700004 loop_ _publ_author_name 'Lipina, Olga A.' 'Surat, Ludmila L.' 'Chufarov, Alexander Yu.' 'Tyutyunnik, Alexander P.' 'Enyashin, Andrey N.' 'Baklanova, Yana V.' 'Chvanova, Anastasia V.' 'Mironov, Leonid Yu.' 'Belova, Ksenia G.' 'Zubkov, Vladimir G.' _publ_section_title ; Structural and spectroscopic characterization of a new series of Ba2RE2Ge4O13 (RE = Pr, Nd, Gd, and Dy) and Ba2Gd2−xEuxGe4O13 tetragermanates ; _journal_issue 31 _journal_name_full 'Dalton Transactions' _journal_page_first 10935 _journal_page_last 10946 _journal_paper_doi 10.1039/D1DT01780B _journal_volume 50 _journal_year 2021 _chemical_formula_structural 'Ba2 Pr2 Ge4 O13' _chemical_formula_sum 'Ba2 Ge4 O13 Pr2' _chemical_formula_weight 1054.82 _chemical_name_common 'Barium Praseodymium Germanate' _chemical_name_systematic 'Dibarium dipraseodymium(III) tetragermanate' _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _audit_creation_date 2021-05-26T14:29 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2021-05-26T14:29 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 105.4404(7) _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 13.28238(16) _cell_length_b 5.42142(7) _cell_length_c 18.05076(26) _cell_measurement_temperature 298(2) _cell_volume 1252.91(3) _computing_data_collection 'STOE Powder Software Package (STOE, Germany)' _computing_data_reduction 'STOE Powder Software Package (STOE, Germany)' _computing_molecular_graphics 'VESTA Ver. 3.4.4' _computing_structure_refinement GSAS _computing_structure_solution 'GSAS (A.C. Larson and R.B. Von Dreele, 2004), EXPGUI (Toby, B.H., 2001)' _diffrn_ambient_temperature 298 _diffrn_detector 'position sensitive detector' _diffrn_detector_type 'linear mini-PSD (STOE)' _diffrn_measurement_device_type 'transmission diffractometer Stadi-P (STOE)' _diffrn_radiation_monochromator 'Primary, curved Ge 111' _diffrn_radiation_polarisn_ratio 0.8 _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a~1~' _diffrn_radiation_wavelength 1.54056 _diffrn_source 'sealed X-ray tube' _diffrn_source_target Cu _diffrn_source_type 'PHILIPS PW 2283/20' _exptl_absorpt_correction_T_max 2.09072 _exptl_absorpt_correction_T_min 1.40592 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 4 Flat plate transmission absorption correction Terms = -0.22028 0.0000 Correction is not refined. ; _exptl_crystal_density_diffrn 5.592 _exptl_crystal_density_method 'not measured' _pd_block_id 2021-05-26T14:29|BA2PR2GE4O13|Chufarov|Stadi-P _pd_calc_method 'Rietveld Refinement' _pd_char_colour white _pd_instr_dist_mono/spec 130 _pd_instr_dist_spec/detc 220 _pd_instr_dist_src/mono 260 _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.02 _pd_meas_2theta_range_max 119.98 _pd_meas_2theta_range_min 5.0 _pd_meas_number_of_points 5750 _pd_meas_scan_method step _pd_phase_name BA2PR2GE4O13 _pd_proc_2theta_range_inc 0.02 _pd_proc_2theta_range_max 119.96308 _pd_proc_2theta_range_min 4.98308 _pd_proc_info_datetime 2021-05-26T14:29:33 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 16 terms. Shifted Chebyshev function of 1st kind 1: 3879.15 2: -2826.74 3: 1156.04 4: -738.216 5: 209.786 6: -22.3072 7: -19.9144 8: 1.21828 9: 13.6987 10: -30.5536 11: 38.3649 12: -22.5625 13: 6.98545 14: 0.847730 15: 1.05683 16: -5.89515 ; _pd_proc_ls_peak_cutoff 0.00100 _pd_proc_ls_profile_function ; CW Profile function number 3 with 19 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. #1(GU) = 75.579 #2(GV) = 0.000 #3(GW) = 21.566 #4(GP) = 0.000 #5(LX) = 2.578 #6(LY) = 8.732 #7(S/L) = 0.0230 #8(H/L) = 0.0230 #9(trns) = 0.00 #10(shft)= 0.0000 #11(stec)= 9.70 #12(ptec)= -2.13 #13(sfec)= 0.00 #14(L11) = 0.033 #15(L22) = 0.142 #16(L33) = 0.014 #17(L12) = -0.048 #18(L13) = 0.026 #19(L23) = -0.037 Peak tails are ignored where the intensity is below 0.0010 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0155 _pd_proc_ls_prof_wR_expected 0.0155 _pd_proc_ls_prof_wR_factor 0.0198 _pd_proc_number_of_points 5750 _pd_spec_mounting 'powder on Mylar film' _pd_spec_mount_mode transmission _pd_spec_shape flat_sheet _pd_spec_size_axial 7 _pd_spec_size_equat 0.1 _refine_ls_goodness_of_fit_all 1.29 _refine_ls_matrix_type full _refine_ls_number_parameters 69 _refine_ls_number_restraints 0 _refine_ls_R_Fsqd_factor 0.02024 _refine_ls_shift/su_max 0.04 _refine_ls_shift/su_mean 0.00 _reflns_d_resolution_high 0.890 _reflns_d_resolution_low 8.700 _reflns_limit_h_max 15 _reflns_limit_h_min 0 _reflns_limit_k_max 6 _reflns_limit_k_min 0 _reflns_limit_l_max 20 _reflns_limit_l_min -20 _reflns_number_total 923 _cod_data_source_file d1dt01780b4.cif _cod_data_source_block BA2PR2GE4O13_publ _cod_original_cell_volume 1252.91(4) _cod_database_code 7700004 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x,+y,-z+1/2 -1 -x,-y,-z -2 +x,-y,+z+1/2 101 +x+1/2,+y+1/2,+z 102 -x+1/2,+y+1/2,-z+1/2 -101 -x+1/2,-y+1/2,-z -102 +x+1/2,-y+1/2,+z+1/2 loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Ba Ba 0.15698(10) 0.5035(5) 0.33231(7) 1.0 Uiso 0.0263(6) 8 Pr Pr 0.11713(10) 0.5112(4) 0.08758(7) 1.0 Uiso 0.0249(6) 8 Ge Ge1 0.06606(18) 0.0463(7) 0.18570(15) 1.0 Uiso 0.0243(10) 8 Ge Ge2 -0.11945(22) -0.0312(8) 0.04059(15) 1.0 Uiso 0.0233(9) 8 O O1 0.0752(11) -0.2727(25) 0.1921(9) 1.0 Uiso 0.022(5) 8 O O2 0.1749(11) 0.2338(21) 0.1990(8) 1.0 Uiso 0.017(5) 8 O O3 0.0 0.1803(33) 0.25 1.0 Uiso 0.018(6) 4 O O4 -0.0178(11) 0.1732(22) 0.0951(7) 1.0 Uiso 0.014(4) 8 O O5 -0.1620(10) 0.1023(23) -0.0482(8) 1.0 Uiso 0.027(5) 8 O O6 -0.2037(8) -0.0428(34) 0.0983(6) 1.0 Uiso 0.028(5) 8 O O7 -0.0669(9) -0.3419(24) 0.0346(7) 1.0 Uiso 0.022(5) 8 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Ba 8.0 0.000 0.000 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310 International_Tables_Vol_C Pr 8.0 0.000 0.000 22.0440 2.77393 19.6697 0.22209 12.3856 16.7669 2.82428 143.644 2.05830 International_Tables_Vol_C Ge 16.0 0.000 0.000 16.0816 2.85090 6.37470 0.25160 3.70680 11.4468 3.68300 54.7625 2.13130 International_Tables_Vol_C O 52.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Ba O2 63.65(33) 1_565 . 1_555 N O1 Ba O2 75.8(4) 1_565 . 102_555 N O1 Ba O3 74.6(4) 1_565 . 1_555 N O1 Ba O4 120.5(4) 1_565 . 2_555 N O1 Ba O5 146.8(4) 1_565 . -102_555 N O1 Ba O6 90.6(4) 1_565 . 2_565 N O1 Ba O7 117.22(34) 1_565 . 2_565 N O2 Ba O2 78.82(29) 1_555 . 102_555 N O2 Ba O3 57.26(29) 1_555 . 1_555 N O2 Ba O4 104.5(4) 1_555 . 2_555 N O2 Ba O5 106.9(4) 1_555 . -102_555 N O2 Ba O6 140.75(34) 1_555 . 2_565 N O2 Ba O7 158.2(4) 1_555 . 2_565 N O2 Ba O3 134.51(29) 102_555 . 1_555 N O2 Ba O4 163.34(35) 102_555 . 2_555 N O2 Ba O5 71.1(4) 102_555 . -102_555 N O2 Ba O6 65.80(34) 102_555 . 2_565 N O2 Ba O7 123.0(4) 102_555 . 2_565 N O3 Ba O4 54.87(26) 1_555 . 2_555 N O3 Ba O5 129.4(4) 1_555 . -102_555 N O3 Ba O6 146.99(34) 1_555 . 2_565 N O3 Ba O7 101.18(26) 1_555 . 2_565 N O4 Ba O5 92.43(30) 2_555 . -102_555 N O4 Ba O6 114.26(32) 2_555 . 2_565 N O4 Ba O7 55.08(34) 2_555 . 2_565 N O5 Ba O6 78.0(4) -102_555 . 2_565 N O5 Ba O7 83.58(35) -102_555 . 2_565 N O6 Ba O7 59.23(32) 2_565 . 2_565 N O1 Pr O2 75.2(4) 1_565 . 1_555 N O1 Pr O4 89.7(4) 1_565 . 1_555 N O1 Pr O5 86.1(5) 1_565 . -1_565 N O1 Pr O6 115.8(5) 1_565 . 101_555 N O1 Pr O7 74.8(4) 1_565 . 1_565 N O1 Pr O7 150.5(5) 1_565 . -1_555 N O2 Pr O4 66.1(4) 1_555 . 1_555 N O2 Pr O5 138.1(5) 1_555 . -1_565 N O2 Pr O6 76.6(5) 1_555 . 101_555 N O2 Pr O7 124.4(4) 1_555 . 1_565 N O2 Pr O7 118.9(5) 1_555 . -1_555 N O4 Pr O5 152.2(4) 1_555 . -1_565 N O4 Pr O6 127.3(5) 1_555 . 101_555 N O4 Pr O7 68.1(4) 1_555 . 1_565 N O4 Pr O7 75.1(4) 1_555 . -1_555 N O5 Pr O6 78.6(6) -1_565 . 101_555 N O5 Pr O7 84.3(5) -1_565 . 1_565 N O5 Pr O7 95.6(5) -1_565 . -1_555 N O6 Pr O7 158.9(4) 101_555 . 1_565 N O6 Pr O7 93.3(4) 101_555 . -1_555 N O7 Pr O7 76.0(5) 1_565 . -1_555 N O1 Ge1 O2 122.3(8) 1_555 . 1_555 N O1 Ge1 O3 113.6(8) 1_555 . 1_555 N O1 Ge1 O4 116.4(7) 1_555 . 1_555 N O2 Ge1 O3 102.0(6) 1_555 . 1_555 N O2 Ge1 O4 100.8(7) 1_555 . 1_555 N O3 Ge1 O4 98.0(5) 1_555 . 1_555 N O4 Ge2 O5 105.2(6) 1_555 . 1_555 N O4 Ge2 O6 101.7(6) 1_555 . 1_555 N O4 Ge2 O7 110.6(6) 1_555 . 1_555 N O5 Ge2 O6 118.5(6) 1_555 . 1_555 N O5 Ge2 O7 111.6(7) 1_555 . 1_555 N O6 Ge2 O7 108.7(7) 1_555 . 1_555 N Ge1 O3 Ge1 132.0(11) 1_555 . 2_555 N Ge1 O4 Ge2 115.9(7) 1_555 . 1_555 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ba O1 2.756(14) . 1_565 N Ba O1 3.233(14) . 2_565 N Ba O2 2.880(14) . 1_555 N Ba O2 2.745(13) . 102_555 N Ba O3 2.824(11) . 1_555 N Ba O4 3.103(13) . 2_555 N Ba O5 2.828(13) . -102_555 N Ba O6 3.211(18) . 2_555 N Ba O6 2.755(17) . 2_565 N Ba O7 3.071(12) . 2_565 N Pr O1 2.409(14) . 1_565 N Pr O2 2.464(13) . 1_555 N Pr O4 2.592(14) . 1_555 N Pr O5 2.340(12) . -1_565 N Pr O6 2.354(10) . 101_555 N Pr O7 2.506(13) . 1_565 N Pr O7 2.317(12) . -1_555 N Ge1 Ge2 3.1100(34) . 1_555 N Ge1 O1 1.735(14) . 1_555 N Ge1 O2 1.732(13) . 1_555 N Ge1 O3 1.785(7) . 1_555 N Ge1 O4 1.848(12) . 1_555 N Ge2 Ge1 3.1100(34) . 1_555 N Ge2 O4 1.820(13) . 1_555 N Ge2 O5 1.712(13) . 1_555 N Ge2 O6 1.722(10) . 1_555 N Ge2 O7 1.838(13) . 1_555 N loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 8868.0 0.0001128 8929.37598 8929.37305 8729.0 0.0001146 8919.12598 8919.12207 8783.0 0.0001139 8908.93652 8908.93359 9054.0 0.0001104 8898.80762 8898.80469 9093.0 0.0001100 8888.73828 8888.73535 8901.0 0.0001123 8878.72852 8878.72559 8962.0 0.0001116 8868.77832 8868.77539 8751.0 0.0001143 8858.88574 8858.88281 8692.0 0.0001150 8849.05078 8849.04785 8907.0 0.0001123 8839.27344 8839.27148 9052.0 0.0001105 8829.55273 8829.55078 8874.0 0.0001127 8819.88965 8819.88672 8895.0 0.0001124 8810.28125 8810.27832 8833.0 0.0001132 8800.72754 8800.72559 8842.0 0.0001131 8791.23047 8791.22852 8967.0 0.0001115 8781.78711 8781.78516 8665.0 0.0001154 8772.39844 8772.39648 8661.0 0.0001155 8763.06250 8763.06152 8759.0 0.0001142 8753.78027 8753.77832 8832.0 0.0001132 8744.55078 8744.54980 8848.0 0.0001130 8735.37402 8735.37207 8609.0 0.0001162 8726.24805 8726.24707 8740.0 0.0001144 8717.17383 8717.17188 8641.0 0.0001157 8708.15137 8708.14941 8641.0 0.0001157 8699.17773 8699.17676 8662.0 0.0001154 8690.25488 8690.25391 8546.0 0.0001170 8681.38184 8681.38086 8612.0 0.0001161 8672.55762 8672.55664 8705.0 0.0001149 8663.78320 8663.78125 8566.0 0.0001167 8655.05566 8655.05469 8618.0 0.0001160 8646.37695 8646.37598 8582.0 0.0001165 8637.74512 8637.74414 8625.0 0.0001159 8629.16113 8629.16016 8555.0 0.0001169 8620.62305 8620.62207 8633.0 0.0001158 8612.13184 8612.13086 8579.0 0.0001166 8603.68652 8603.68555 8470.0 0.0001181 8595.28613 8595.28613 8465.0 0.0001181 8586.93164 8586.93066 8676.0 0.0001153 8578.62109 8578.62109 8501.0 0.0001176 8570.35547 8570.35449 8474.0 0.0001180 8562.13379 8562.13281 8494.0 0.0001177 8553.95508 8553.95410 8483.0 0.0001179 8545.81934 8545.81836 8500.0 0.0001176 8537.72754 8537.72656 8417.0 0.0001188 8529.67676 8529.67578 8482.0 0.0001179 8521.66895 8521.66797 8395.0 0.0001191 8513.70215 8513.70117 8500.0 0.0001176 8505.77734 8505.77637 8505.0 0.0001176 8497.89258 8497.89258 8443.0 0.0001184 8490.04883 8490.04785 8553.0 0.0001169 8482.24512 8482.24512 8246.0 0.0001213 8474.48145 8474.48145 8552.0 0.0001169 8466.75781 8466.75781 8573.0 0.0001166 8459.07227 8459.07227 8519.0 0.0001174 8451.42578 8451.42578 8416.0 0.0001188 8443.81836 8443.81836 8492.0 0.0001178 8436.24805 8436.24805 8391.0 0.0001192 8428.71680 8428.71680 8553.0 0.0001169 8421.22168 8421.22168 8610.0 0.0001161 8413.76465 8413.76465 8466.0 0.0001181 8406.34375 8406.34375 8270.0 0.0001209 8398.95996 8398.95898 8353.0 0.0001197 8391.61133 8391.61133 8522.0 0.0001173 8384.29883 8384.29883 8233.0 0.0001215 8377.02148 8377.02148 8412.0 0.0001189 8369.78027 8369.78027 8263.0 0.0001210 8362.57227 8362.57227 8243.0 0.0001213 8355.40039 8355.40039 8541.0 0.0001171 8348.26172 8348.26172 8469.0 0.0001181 8341.15723 8341.15723 8460.0 0.0001182 8334.08691 8334.08691 8283.0 0.0001207 8327.04883 8327.04883 8287.0 0.0001207 8320.04395 8320.04395 8451.0 0.0001183 8313.07129 8313.07129 8346.0 0.0001198 8306.13184 8306.13281 8249.0 0.0001212 8299.22461 8299.22461 8251.0 0.0001212 8292.34863 8292.34863 8133.0 0.0001230 8285.50391 8285.50391 8293.0 0.0001206 8278.69043 8278.69043 8341.0 0.0001199 8271.90820 8271.90820 8329.0 0.0001201 8265.15625 8265.15625 8214.0 0.0001217 8258.43457 8258.43555 8100.0 0.0001235 8251.74316 8251.74414 8270.0 0.0001209 8245.08203 8245.08203 8322.0 0.0001202 8238.45020 8238.45020 8322.0 0.0001202 8231.84668 8231.84668 8223.0 0.0001216 8225.27246 8225.27344 8197.0 0.0001220 8218.72754 8218.72754 8259.0 0.0001211 8212.21094 8212.21094 8376.0 0.0001194 8205.72168 8205.72168 8231.0 0.0001215 8199.26074 8199.26074 8228.0 0.0001215 8192.82715 8192.82715 8133.0 0.0001230 8186.42139 8186.42139 8281.0 0.0001208 8180.04248 8180.04248 8398.0 0.0001191 8173.69043 8173.69043 8136.0 0.0001229 8167.36523 8167.36572 8202.0 0.0001219 8161.06592 8161.06592 8064.0 0.0001240 8154.79297 8154.79297 8062.0 0.0001240 8148.54590 8148.54590 8215.0 0.0001217 8142.32422 8142.32422 8365.0 0.0001195 8136.12842 8136.12842 8155.0 0.0001226 8129.95703 8129.95703 7984.0 0.0001253 8123.81055 8123.81055 8008.0 0.0001249 8117.68945 8117.68945 8357.0 0.0001197 8111.59180 8111.59229 8241.0 0.0001213 8105.51953 8105.51953 8080.0 0.0001238 8099.47021 8099.47021 8162.0 0.0001225 8093.44482 8093.44482 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0.000427 2047.80359 2345.91992 2352.0 0.000425 2047.20288 2345.54932 2285.0 0.000438 2046.60144 2343.92847 2391.0 0.000418 2045.99927 2340.75269 2335.0 0.000428 2045.39600 2335.88184 2278.0 0.000439 2044.79211 2329.15747 2259.0 0.000443 2044.18713 2320.74487 2282.0 0.000438 2043.58167 2310.89990 2396.0 0.000417 2042.97510 2299.98999 2347.0 0.000426 2042.36780 2288.42725 2307.0 0.000433 2041.75977 2276.62891 2190.0 0.000457 2041.15063 2264.98828 2220.0 0.000450 2040.54089 2253.84229 2212.0 0.000452 2039.93005 2243.47900 2163.0 0.000462 2039.31860 2234.12695 2237.0 0.000447 2038.70593 2225.96924 2220.0 0.000450 2038.09290 2219.14917 2235.0 0.000447 2037.47852 2213.45068 2196.0 0.000455 2036.86365 2209.59644 2243.0 0.000446 2036.24792 2207.32886 2214.0 0.000452 2035.63098 2206.71289 2190.0 0.000457 2035.01343 2207.85767 2260.0 0.000442 2034.39478 2210.74634 2177.0 0.000459 2033.77563 2215.50757 2270.0 0.000441 2033.15527 2222.34082 2241.0 0.000446 2032.53418 2231.06885 2238.0 0.000447 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2198.0 0.000455 1997.66064 2171.73242 2139.0 0.000468 1996.98987 2175.82520 2189.0 0.000457 1996.31799 2179.84619 2232.0 0.000448 1995.64539 2183.57153 2286.0 0.000437 1994.97156 2186.78174 2249.0 0.000445 1994.29724 2189.33301 2200.0 0.000455 1993.62195 2191.09399 2204.0 0.000454 1992.94543 2192.07080 2159.0 0.000463 1992.26843 2192.33130 2210.0 0.000452 1991.59009 2192.02051 2226.0 0.000449 1990.91113 2191.32178 2227.0 0.000449 1990.23096 2190.43506 2180.0 0.000459 1989.55029 2189.55371 2191.0 0.000456 1988.86841 2188.84351 2222.0 0.000450 1988.18579 2188.43555 2153.0 0.000464 1987.50232 2188.42261 2206.0 0.000453 1986.81775 2188.86060 2258.0 0.000443 1986.13245 2189.76978 2321.0 0.000431 1985.44592 2191.18896 2132.0 0.000469 1984.75903 2193.04443 2130.0 0.000469 1984.07080 2195.30542 2072.0 0.000483 1983.38184 2197.94409 2236.0 0.000447 1982.69189 2200.90698 2265.0 0.000442 1982.00122 2204.12354 2106.0 0.000475 1981.30969 2207.57959 2168.0 0.000461 1980.61707 2211.01978 2185.0 0.000458 1979.92371 2214.38232 2195.0 0.000456 1979.22925 2217.51660 2198.0 0.000455 1978.53430 2220.25513 2185.0 0.000458 1977.83801 2222.43457 2232.0 0.000448 1977.14111 2223.90967 2170.0 0.000461 1976.44336 2224.57520 2180.0 0.000459 1975.74463 2224.38623 2255.0 0.000443 1975.04517 2223.37476 2198.0 0.000455 1974.34448 2221.62549 2124.0 0.000471 1973.64331 2219.32739 2225.0 0.000449 1972.94092 2216.60938 2252.0 0.000444 1972.23804 2213.72119 2213.0 0.000452 1971.53394 2210.80493 2203.0 0.000454 1970.82935 2208.03271 2175.0 0.000460 1970.12366 2205.50000 2181.0 0.000459 1969.41699 2203.25220 2224.0 0.000450 1968.70984 2201.30176 2167.0 0.000461 1968.00146 2199.55811 2257.0 0.000443 1967.29248 2197.94897 2189.0 0.000457 1966.58240 2196.36206 2169.0 0.000461 1965.87183 2194.68433 2147.0 0.000466 1965.16003 2192.76807 2221.0 0.000450 1964.44763 2190.51025 2235.0 0.000447 1963.73462 2187.79614 2117.0 0.000472 1963.02026 2184.53491 2122.0 0.000471 1962.30542 2180.64966 2106.0 0.000475 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1818.0 0.000550 1681.45947 1915.87646 1895.0 0.000528 1680.59998 1908.16162 1848.0 0.000541 1679.73621 1900.54993 1898.0 0.000527 1678.86865 1893.18799 1910.0 0.000524 1677.99731 1886.20142 1794.0 0.000557 1677.12146 1879.69385 1866.0 0.000536 1676.24170 1873.75549 1846.0 0.000542 1675.35754 1868.44800 1871.0 0.000534 1674.46912 1863.81128 1884.0 0.000531 1673.57593 1859.86011 1893.0 0.000528 1672.67871 1856.58618 1834.0 0.000545 1671.77661 1853.95435 1862.0 0.000537 1670.86963 1851.91052 1811.0 0.000552 1669.95801 1850.38135 1864.0 0.000536 1669.04138 1849.27490 1811.0 0.000552 1668.11987 1848.48853 1872.0 0.000534 1667.19299 1847.91516 1805.0 0.000554 1666.26123 1847.44995 1798.0 0.000556 1665.32385 1846.99292 1856.0 0.000539 1664.38135 1846.46558 1785.0 0.000560 1663.43347 1845.80981 1780.0 0.000562 1662.47949 1844.98987 1830.0 0.000546 1661.52026 1843.99438 1863.0 0.000537 1660.55469 1842.82739 1818.0 0.000550 1659.58386 1841.50269 1815.0 0.000551 1658.60632 1840.03125 1806.0 0.000554 1657.62317 1838.41772 1831.0 0.000546 1656.63330 1836.65808 1856.0 0.000539 1655.63757 1834.74023 1931.0 0.000518 1654.63525 1832.64453 1865.0 0.000536 1653.62598 1830.35559 1833.0 0.000546 1652.61047 1827.87231 1834.0 0.000545 1651.58752 1825.20593 1810.0 0.000552 1650.55811 1822.39453 1854.0 0.000539 1649.52148 1819.50037 1870.0 0.000535 1648.47778 1816.60291 1828.0 0.000547 1647.42676 1813.80017 1799.0 0.000556 1646.36792 1811.19397 1802.0 0.000555 1645.30200 1808.88367 1804.0 0.000554 1644.22791 1806.96582 1884.0 0.000531 1643.14636 1805.52380 1842.0 0.000543 1642.05664 1804.62329 1849.0 0.000541 1640.95898 1804.32263 1799.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 0 0 2 o 2335.400 2963.099 0.00 8.69964 0.78 2 0 0 o 13128.952 12411.738 0.00 6.40149 2.95 2 0 -2 o 13449.319 9745.976 0.00 5.97035 2.67 1 1 0 o 14964.488 14555.040 180.00 4.99228 6.12 1 1 -1 o 220.874 201.574 0.00 4.93644 0.06 1 1 1 o 5687.458 6031.964 180.00 4.67181 1.39 2 0 2 o 8292.168 10237.549 180.00 4.60400 0.76 1 1 -2 o 338.609 731.302 180.00 4.53815 0.00 0 0 4 o 83904.97 91221.71 180.00 4.34982 9.20 1 1 2 o 450.002 489.309 180.00 4.14808 0.12 2 0 -4 o 69390.79 74058.12 0.00 4.14757 7.80 1 1 -3 o 1942.573 1998.235 180.00 3.99419 0.33 1 1 3 o 17242.742 10570.969 0.00 3.60320 2.55 1 1 -4 o 139116.02 132727.94 180.00 3.46242 18.70 3 1 -1 o 123.174 126.619 0.00 3.42873 0.02 3 1 0 o 220074.98 219046.39 0.00 3.35334 28.48 3 1 -2 o 179226.62 176973.14 180.00 3.37483 22.76 4 0 -2 o 38865.10 37217.63 0.00 3.30227 2.54 2 0 4 o 11028.635 11372.145 180.00 3.22117 1.13 4 0 0 o 684696.5 688028.1 180.00 3.20075 38.85 3 1 -3 o 2233.312 2221.852 0.00 3.20840 0.24 3 1 1 o 5181.611 5719.599 180.00 3.17176 0.56 1 1 4 o 923679.7 927864.8 0.00 3.12292 100.00 1 1 -5 o 16943.797 17909.215 180.00 3.00485 1.68 4 0 -4 o 68579.19 67637.99 180.00 2.98518 3.57 3 1 -4 o 877298.6 878520.4 180.00 2.97355 85.08 2 0 -6 o 28951.742 28328.244 180.00 2.95353 1.44 3 1 2 o 23996.914 20886.160 180.00 2.93000 2.63 0 0 6 o 7464.851 6232.232 0.00 2.89988 0.40 4 0 2 o 351565.1 354659.8 180.00 2.77408 14.75 1 1 5 o 26.848 27.021 180.00 2.72513 0.00 3 1 -5 o 12.355 12.405 180.00 2.71508 0.00 0 2 0 o 900591.6 902966.4 0.00 2.71071 36.43 3 1 3 o 18915.381 19421.482 180.00 2.67098 1.61 0 2 1 o 25322.514 25731.443 180.00 2.67840 2.01 1 1 -6 o 35848.93 36267.86 0.00 2.62887 2.60 0 2 2 o 11740.121 12199.935 0.00 2.58799 0.83 2 2 -1 o 336.991 1394.796 0.00 2.50771 0.06 4 0 -6 o -100.235 441.846 0.00 2.50659 0.02 2 2 0 o 2471.723 3306.133 180.00 2.49614 0.23 2 2 -2 o -84.359 3.002 0.00 2.46822 0.07 3 1 -6 o 30144.223 32770.641 0.00 2.46318 2.20 0 2 3 o 3153.576 3325.007 0.00 2.45573 0.22 2 0 6 o 20.394 26.301 0.00 2.41120 0.00 3 1 4 o 37605.50 38461.66 0.00 2.42205 2.25 2 2 1 o 39166.67 39671.98 180.00 2.43556 2.49 1 1 6 o 15641.324 16584.857 0.00 2.40159 0.81 2 2 -3 o 10835.326 11429.416 0.00 2.38445 0.74 5 1 -2 o 20652.236 21526.750 0.00 2.38468 1.16 5 1 -1 o 2914.745 3319.386 0.00 2.37095 0.20 5 1 -3 o 79.570 111.245 180.00 2.35432 0.02 2 2 2 o 76.904 76.471 180.00 2.33591 0.00 1 1 -7 o 5223.037 5047.231 180.00 2.32339 0.35 4 0 4 o 332495.16 324798.50 0.00 2.30200 9.93 5 1 0 o 7495.579 6593.273 0.00 2.31534 0.56 0 2 4 o 100332.12 96293.02 180.00 2.30056 6.16 2 2 -4 o 165015.06 158510.86 0.00 2.26907 10.25 5 1 -4 o 9651.725 9693.405 0.00 2.28465 0.73 2 0 -8 o 587781.0 574970.6 180.00 2.24981 16.37 3 1 -7 o 5480.724 4774.994 180.00 2.23277 0.34 5 1 1 o 10015.738 8815.836 180.00 2.22610 0.59 6 0 -2 o 49055.77 45004.68 180.00 2.21321 1.48 3 1 5 o 13975.261 12376.009 180.00 2.19600 0.75 2 2 3 o 897.522 810.055 0.00 2.21097 0.05 0 0 8 o 359096.2 355217.0 180.00 2.17491 9.44 5 1 -5 o 4977.981 4671.922 0.00 2.18550 0.27 6 0 -4 o 242779.12 242230.55 180.00 2.15611 6.48 1 1 7 o 5726.724 5723.917 0.00 2.13827 0.33 6 0 0 o 5331.722 5265.724 0.00 2.13383 0.19 0 2 5 o 7975.100 7981.128 0.00 2.13847 0.39 2 2 -5 o 31.305 30.481 180.00 2.13603 0.00 5 1 2 o 7905.257 8014.022 0.00 2.11451 0.56 4 2 -1 o 599.986 649.230 180.00 2.09682 0.03 4 2 -2 o 34027.418 36806.75 0.00 2.09522 1.81 1 1 -8 o 106626.12 110132.04 0.00 2.07432 5.77 2 2 4 o 66050.69 68039.51 180.00 2.07404 3.56 4 0 -8 o 170496.72 174916.52 0.00 2.07378 4.16 4 2 0 o 474174.1 474918.5 180.00 2.06856 22.57 5 1 -6 o 90094.34 90096.20 180.00 2.06837 4.50 4 2 -3 o 15604.323 15150.230 0.00 2.06395 0.74 3 1 -8 o -65.407 0.139 180.00 2.02874 0.01 4 2 1 o 546.663 1010.981 180.00 2.01387 0.02 2 2 -6 o 36589.08 39408.73 180.00 1.99710 1.66 3 1 6 o 13303.738 14322.081 0.00 1.99653 0.65 4 2 -4 o 4017.057 5848.711 180.00 2.00680 0.22 5 1 3 o 2831.458 2878.758 180.00 1.99156 0.14 6 0 -6 o 244934.06 243708.64 0.00 1.99012 5.44 0 2 6 o 3775.719 4218.563 0.00 1.98026 0.20 6 0 2 o 2239.584 2606.378 180.00 1.95545 0.05 2 2 5 o 3057.678 3031.095 180.00 1.93536 0.14 5 1 -7 o 62.139 66.043 180.00 1.94354 0.00 4 2 2 o 269843.88 271684.91 180.00 1.93878 11.19 4 0 6 o 78.321 54.746 0.00 1.91077 0.01 2 0 8 o 372333.8 357867.5 0.00 1.91021 7.77 1 1 8 o 152567.50 151790.95 180.00 1.92218 6.32 4 2 -5 o 95.422 95.006 180.00 1.92995 0.00 1 1 -9 o 2772.848 2626.963 180.00 1.86933 0.12 5 1 4 o 249222.16 245978.67 180.00 1.86599 9.92 2 2 -7 o 9776.310 9275.304 0.00 1.86052 0.36 3 1 -9 o 5092.883 5063.411 0.00 1.85074 0.20 4 2 3 o 4210.210 4232.028 0.00 1.85022 0.16 4 2 -6 o 29428.787 27422.766 0.00 1.84036 1.05 3 1 7 o 46.926 27.976 0.00 1.82276 0.00 0 2 7 o 8.196 0.990 180.00 1.83201 0.00 5 1 -8 o 36090.73 30450.596 180.00 1.81868 1.60 2 0 -10 o 5948.577 5317.364 180.00 1.80505 0.09 2 2 6 o 18090.930 17327.098 0.00 1.80160 0.65 1 3 0 o 33880.641 33514.750 180.00 1.78940 1.41 1 3 -1 o 40.698 40.399 0.00 1.78679 0.00 7 1 -3 o 3825.745 3795.494 0.00 1.78889 0.14 7 1 -2 o 482903.8 479070.7 0.00 1.78827 17.28 1 3 1 o 7963.503 8002.767 180.00 1.77331 0.27 7 1 -1 o 580.371 592.444 0.00 1.76908 0.03 6 0 -8 o 293650.38 294082.12 0.00 1.77809 5.05 1 3 -2 o -1.814 10.375 0.00 1.76572 0.01 7 1 -4 o 169854.97 169158.34 0.00 1.77087 5.88 4 2 4 o 174516.05 178744.03 0.00 1.75466 6.14 5 1 5 o 2907.021 3214.193 180.00 1.74374 0.09 1 1 9 o 3749.490 4153.065 0.00 1.74290 0.12 6 0 4 o 55178.39 60903.00 0.00 1.74119 0.95 0 0 10 o 10455.396 11396.445 0.00 1.73993 0.17 4 2 -7 o 6083.173 6722.878 0.00 1.74440 0.19 2 2 -8 o 361093.0 361324.6 180.00 1.73121 12.05 1 3 2 o 1334.321 1456.566 0.00 1.73998 0.04 1 3 -3 o 15287.319 15953.963 180.00 1.72808 0.50 4 0 -10 o 121434.14 124571.45 180.00 1.73469 2.08 7 1 0 o 138281.38 138721.53 180.00 1.73303 4.75 7 1 -5 o 193.409 204.504 180.00 1.73585 0.01 1 1 -10 o 55210.68 55642.68 180.00 1.69872 1.79 3 1 -10 o 5932.523 5942.798 0.00 1.69628 0.20 6 2 -2 o 21748.580 22472.768 180.00 1.71437 0.85 6 2 -1 o 757.360 778.396 0.00 1.70331 0.03 6 2 -3 o 9335.141 9008.696 0.00 1.70892 0.29 5 1 -9 o 433.375 436.175 0.00 1.69873 0.01 0 2 8 o 139316.44 139339.67 180.00 1.69638 4.45 7 1 1 o 16.510 16.481 0.00 1.68313 0.00 1 3 3 o 26389.459 27319.959 0.00 1.69222 0.84 6 2 -4 o 100484.85 100831.12 180.00 1.68742 3.37 1 3 -4 o 50925.29 49192.83 180.00 1.67695 1.64 7 1 -6 o 1617.518 1613.619 180.00 1.68675 0.08 2 2 7 o 1080.116 1043.718 0.00 1.67643 0.04 3 1 8 o 111669.73 111596.00 180.00 1.67201 3.72 6 2 0 o 858.479 789.348 0.00 1.67667 0.06 3 3 -1 o 2399.994 2395.455 0.00 1.67308 0.09 4 2 5 o 27057.990 26760.578 180.00 1.65728 0.84 3 3 -2 o 66523.46 66384.07 180.00 1.66670 2.08 3 3 0 o 113221.80 112925.23 0.00 1.66409 3.73 4 2 -8 o 89406.48 87839.73 0.00 1.64707 2.81 8 0 -2 o 1376.496 1435.170 0.00 1.65428 0.03 6 2 -5 o 4214.097 4232.937 180.00 1.65162 0.14 8 0 -4 o 21648.791 21546.943 0.00 1.65114 0.36 5 1 6 o 248468.72 250854.95 180.00 1.62830 7.34 3 3 -3 o 21505.766 21447.348 0.00 1.64548 0.65 3 3 1 o 33624.504 34806.723 180.00 1.64047 1.02 6 2 1 o 14064.407 14399.140 0.00 1.63657 0.41 1 3 4 o 490250.6 494774.2 0.00 1.63360 14.95 7 1 2 o 38059.50 39027.81 180.00 1.62300 1.20 2 2 -9 o 1134.849 1130.071 180.00 1.61158 0.04 4 0 8 o 60005.66 60131.82 0.00 1.61059 0.88 7 1 -7 o 808.932 810.856 180.00 1.62717 0.02 1 3 -5 o 41460.41 40907.75 180.00 1.61598 1.18 3 3 -4 o 385410.9 385459.9 180.00 1.61106 11.27 1 1 10 o 4575.239 4529.859 0.00 1.59243 0.16 8 0 0 o 28991.092 29763.742 0.00 1.60037 0.43 6 2 -6 o 226580.08 229123.72 0.00 1.60420 6.73 3 3 2 o 380.521 397.472 180.00 1.60402 0.04 5 1 -10 o 116088.12 118604.52 0.00 1.58641 3.47 6 2 2 o 1381.644 1420.040 180.00 1.58588 0.05 2 0 10 o 76036.19 72975.07 0.00 1.57616 1.01 8 0 -6 o 110793.26 109668.95 180.00 1.59187 1.58 0 2 9 o 22422.332 21192.652 0.00 1.57397 0.61 1 3 5 o 4139.899 4213.876 0.00 1.56779 0.12 3 3 -5 o 20074.264 20295.332 180.00 1.56587 0.55 7 1 3 o 3268.705 3385.758 0.00 1.55628 0.09 1 1 -11 o 94.614 97.926 180.00 1.55508 0.00 3 1 -11 o 67.323 66.909 0.00 1.56224 0.00 4 2 6 o 1560.825 1551.043 0.00 1.56176 0.05 2 2 8 o 210909.64 209884.89 0.00 1.56146 6.03 6 0 -10 o 9377.747 9552.618 180.00 1.56839 0.14 1 3 -6 o 16973.832 16811.039 0.00 1.54879 0.45 3 3 3 o -1.519 0.872 0.00 1.55727 0.00 6 0 6 o 15404.424 7957.513 180.00 1.53467 0.24 7 1 -8 o 66565.84 66472.94 0.00 1.56078 1.89 4 2 -9 o 25249.820 25123.043 0.00 1.55190 0.69 3 1 9 o 2017.658 1475.647 0.00 1.54115 0.05 6 2 -7 o 13885.759 13889.742 180.00 1.54824 0.39 5 1 7 o 137.764 70.022 180.00 1.52135 0.01 6 2 3 o 13429.519 9846.244 0.00 1.52770 0.37 3 3 -6 o 20660.992 16350.913 0.00 1.51272 0.60 8 0 2 o 361975.9 345588.25 0.00 1.50431 4.71 2 0 -12 o 11372.332 11096.891 0.00 1.50295 0.14 2 2 -10 o 264.758 261.140 180.00 1.50242 0.00 3 3 4 o 27424.195 26846.414 0.00 1.50304 0.69 1 3 6 o 35523.08 36344.92 0.00 1.49811 0.87 7 1 4 o 8319.674 8153.865 0.00 1.48620 0.25 6 2 -8 o 180990.27 178038.92 0.00 1.48677 4.46 1 3 -7 o 1516.649 1360.810 0.00 1.47855 0.04 5 3 -2 o 8755.199 8822.494 0.00 1.49398 0.20 8 0 -8 o 104.034 87.666 0.00 1.49259 0.02 7 1 -9 o 20.677 19.624 180.00 1.49083 0.00 5 3 -1 o 10700.865 10382.894 180.00 1.49059 0.29 5 1 -11 o 859.261 817.384 0.00 1.48289 0.03 5 3 -3 o 48539.44 47924.99 0.00 1.48643 1.19 4 2 7 o 294.391 284.328 180.00 1.47045 0.01 4 0 -12 o 2113.657 1199.199 180.00 1.47677 0.11 5 3 0 o 645.093 389.100 180.00 1.47647 0.06 6 2 4 o 22826.205 21107.164 0.00 1.46500 0.59 1 1 11 o 219.720 203.877 0.00 1.46473 0.01 0 2 10 o 86.133 52.527 0.00 1.46425 0.01 4 2 -10 o 64964.29 62480.48 180.00 1.46112 1.65 5 3 -4 o 10890.795 9987.210 0.00 1.46841 0.33 0 0 12 o 95510.77 99421.59 0.00 1.44994 1.27 2 2 9 o 3780.071 3860.508 0.00 1.45697 0.08 3 3 -7 o 12886.736 13589.440 0.00 1.45436 0.32 3 1 -12 o 284114.03 286613.25 0.00 1.44557 6.94 5 3 1 o 99.815 111.994 0.00 1.45251 0.00 1 1 -12 o 143879.39 139129.45 180.00 1.43281 3.51 3 3 5 o 47272.88 48758.25 180.00 1.44405 1.13 3 1 10 o 18927.752 19432.643 0.00 1.42717 0.42 5 3 -5 o 676.190 747.784 0.00 1.44105 0.02 5 1 8 o 78056.82 81848.83 0.00 1.42341 1.91 7 1 5 o 2180.042 2299.960 180.00 1.41535 0.06 1 3 7 o 6233.654 6408.236 180.00 1.42726 0.15 9 1 -3 o 55.337 57.657 180.00 1.42369 0.00 1 3 -8 o 52586.93 53509.71 0.00 1.40776 1.43 6 2 -9 o 1544.136 1598.533 0.00 1.42249 0.03 9 1 -4 o 2017.208 2105.831 180.00 1.42137 0.07 5 3 2 o 2671.767 2864.272 0.00 1.42013 0.11 7 1 -10 o 135864.80 141720.31 180.00 1.41997 3.18 2 2 -11 o 1891.863 1892.111 180.00 1.40359 0.05 9 1 -2 o 5090.730 5486.613 180.00 1.41653 0.15 8 2 -2 o 62.211 150.088 0.00 1.41209 0.02 9 1 -5 o -0.231 0.638 0.00 1.40972 0.00 8 2 -3 o 333.327 351.049 0.00 1.41578 0.01 6 2 5 o 2892.919 3097.743 180.00 1.40027 0.06 5 3 -6 o 37537.71 37520.27 180.00 1.40590 0.94 4 0 10 o 104007.00 105559.05 0.00 1.38205 1.19 8 2 -4 o 20356.922 21864.271 0.00 1.41013 0.52 8 0 4 o 64127.36 64704.08 180.00 1.38704 0.77 9 1 -1 o 4.624 7.009 0.00 1.40032 0.00 3 3 -8 o 5692.223 6296.485 180.00 1.39326 0.16 8 2 -1 o 233.036 270.906 0.00 1.39930 0.01 8 2 -5 o 246.822 294.360 180.00 1.39550 0.01 5 1 -12 o 144575.38 144262.17 0.00 1.38837 3.15 4 2 8 o 18769.549 18983.941 0.00 1.38462 0.40 3 3 6 o 24608.480 25008.443 0.00 1.38269 0.61 9 1 -6 o 53939.43 52935.00 0.00 1.38940 1.43 9 1 0 o 118.590 122.118 180.00 1.37597 0.01 4 2 -11 o 1588.176 1609.968 180.00 1.37592 0.03 6 0 -12 o 25031.484 25422.637 0.00 1.38252 0.29 5 3 3 o 164.772 169.592 0.00 1.38104 0.01 8 2 0 o 51984.69 52325.12 0.00 1.37812 1.17 2 2 10 o 31711.012 29632.500 0.00 1.36257 0.63 6 0 8 o 141082.64 141416.12 180.00 1.35362 1.59 8 0 -10 o 66029.58 67650.66 0.00 1.37420 0.83 0 2 11 o 20.090 16.690 180.00 1.36617 0.00 8 2 -6 o 51406.03 53805.36 180.00 1.37268 1.13 5 3 -7 o 2441.336 2233.150 0.00 1.36472 0.06 1 1 12 o 102668.02 103213.02 180.00 1.35523 2.24 6 2 -10 o 5629.640 5401.415 180.00 1.35754 0.14 1 3 8 o 59955.08 58019.61 180.00 1.35727 1.34 0 4 0 o 328011.69 330927.31 0.00 1.35536 3.62 9 1 -7 o 2759.777 2583.091 180.00 1.36153 0.06 2 0 12 o 28054.561 29468.006 180.00 1.33938 0.30 7 1 6 o 72117.37 73466.34 180.00 1.34563 1.57 1 3 -9 o 1521.682 1603.187 180.00 1.33827 0.04 0 4 1 o 5518.685 5341.082 180.00 1.35126 0.11 3 1 -13 o 8751.465 8888.775 0.00 1.34358 0.19 8 2 1 o 12958.161 12644.891 0.00 1.34968 0.28 5 1 9 o 800.284 829.294 0.00 1.33432 0.02 9 1 1 o 2807.135 2846.837 0.00 1.34475 0.06 7 1 -11 o 970.255 941.896 180.00 1.35013 0.02 6 2 6 o 736.192 866.075 0.00 1.33549 0.07 1 1 -13 o 5009.386 4987.468 0.00 1.32769 0.11 3 1 11 o 3745.716 3732.508 0.00 1.32745 0.09 0 4 2 o 288.370 321.859 180.00 1.33920 0.01 3 3 -9 o 2440.562 2448.331 0.00 1.33140 0.05 5 3 4 o 145941.11 152280.47 180.00 1.33704 3.21 8 2 -7 o 39719.86 40593.37 180.00 1.34287 0.85 2 2 -12 o 126.335 124.896 0.00 1.31443 0.00 2 4 -1 o 14251.348 14168.404 180.00 1.32769 0.30 2 4 0 o 1712.027 1732.346 180.00 1.32596 0.04 2 4 -2 o 2932.066 2807.530 0.00 1.32173 0.06 10 0 -4 o 20125.846 20006.100 0.00 1.32767 0.21 9 1 -8 o 16764.779 16685.314 0.00 1.32747 0.36 3 3 7 o 5142.671 4880.113 180.00 1.32087 0.11 0 4 3 o 5081.583 4771.278 0.00 1.31980 0.11 5 3 -8 o 41901.67 39253.48 180.00 1.31931 1.00 10 0 -2 o 80277.52 75992.02 0.00 1.31822 0.90 2 4 1 o 47364.12 45767.47 180.00 1.31664 0.94 8 2 2 o 224945.20 216992.83 0.00 1.31534 4.70 9 1 2 o 111.888 77.308 0.00 1.30809 0.04 4 2 9 o 164.268 166.536 180.00 1.30486 0.00 5 1 -13 o 434.267 431.470 0.00 1.30254 0.01 2 4 -3 o 1048.657 1026.051 180.00 1.30838 0.02 4 2 -12 o 12780.834 12488.516 180.00 1.29681 0.38 7 3 -3 o 4370.389 4299.905 0.00 1.30781 0.09 7 3 -2 o 210846.92 207977.56 0.00 1.30756 4.38 8 2 -8 o 16483.732 16248.858 180.00 1.30748 0.39 10 0 -6 o 352722.2 351855.1 180.00 1.30681 3.65 2 4 2 o 47.776 47.580 0.00 1.30019 0.00 7 3 -4 o 74489.55 74142.88 0.00 1.30072 1.50 2 4 -4 o 48691.23 48873.45 0.00 1.28831 1.12 7 3 -1 o 11626.895 11629.481 180.00 1.30000 0.24 0 4 4 o 35659.00 35246.81 180.00 1.29399 0.78 6 2 -11 o 6846.199 6770.317 180.00 1.29353 0.14 2 0 -14 o 1774.985 1905.923 180.00 1.28575 0.04 7 1 7 o 2747.868 2778.595 0.00 1.27834 0.05 5 3 5 o 19491.783 19097.396 180.00 1.28985 0.39 1 3 9 o 18087.811 17804.541 0.00 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