#------------------------------------------------------------------------------ #$Date: 2025-07-01 13:39:59 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1111 $ #$URL: svn://localhost/testcod/cif/7/20/00/7200027.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7200027 loop_ _publ_author_name 'Gu\'nka, Piotr A.' 'Hanfland, Michael' 'Chen, Yu-Sheng' 'Zachara, Janusz' _publ_section_title ; High-pressure and low-temperature structural study of claudetite I, a monoclinic layered As2O3 polymorph ; _journal_issue 3 _journal_name_full CrystEngComm _journal_page_first 638 _journal_page_last 644 _journal_paper_doi 10.1039/D0CE01401J _journal_volume 23 _journal_year 2021 _chemical_formula_moiety 'As2 O3' _chemical_formula_sum 'As2 O3' _chemical_formula_weight 197.84 _chemical_name_common 'claudetite I' _chemical_name_systematic ; arsenic(III) oxide ; _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/n 1' _audit_creation_date 2020-10-21T14:10 _audit_creation_method 'created in GSAS-II' _audit_update_record ; 2020-10-22 deposited with the CCDC. 2020-12-10 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 94.821(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.5726(6) _cell_length_b 11.4835(9) _cell_length_c 4.0105(4) _cell_measurement_pressure 2.98e7(5) _cell_measurement_temperature 293 _cell_volume 209.84(4) _computing_data_reduction Fit2D _computing_structure_refinement 'GSAS-II (Toby & Von Dreele, J. Appl. Cryst. 46, 544-549, 2013)' _diffrn_ambient_pressure 2.98e7(5) _diffrn_ambient_temperature 293 _diffrn_detector 'Mar555 flat panel' _diffrn_detector_type 'Mar555 flat panel' _diffrn_measurement_device_type 'ESRF ID09A beamline' _diffrn_radiation_monochromator Si _diffrn_radiation_polarisn_ratio 0.9900 _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 0.41421 _diffrn_source 'ESRF ID09A' _diffrn_source_type synchrotron _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 6.2622 _exptl_crystal_description 'white powder' _pd_block_id 2020-10-21T14:10|clau1_022rietveld||id09a _pd_calc_method 'Rietveld Refinement' _pd_meas_number_of_points 4000 _pd_phase_name claudetiteI _pd_prep_pressure 100.0(1) _pd_prep_temperature 293 _pd_proc_info_datetime 2020-10-21T14:10 _pd_proc_ls_background_function ; Background function: "chebyschev" function with 36 terms: 766.4(10), 446.5(28), 100(11), 4096(18), -1.78(4)e3, -610580(22), 250029(23), 1.9643935(17)e7, -7.85815(4)e6, -3.17743806(8)e8, 1.39145235(19)e8, 3.107503937(17)e9, -1.506039008(18)e9, -2.0116752030(20)e10, 1.049747135(4)e10, 9.1079941967(16)e10, -4.958747496(4)e10, -2.98733616615(10)e11, 1.64960067436(29)e11, 7.25532807575(8)e11, -3.96148973046(11)e11, -1.320387406690(13)e12, 6.95542054556(20)e11, 1.806430135782(18)e12, -8.9415651509(4)e11, -1.847735508477(20)e12, 8.3271917038(5)e11, 1.390792040927(19)e12, -5.4701088897(4)e11, -7.47049458161(14)e11, 2.40400371117(24)e11, 2.70715010363(6)e11, -6.3444311316(19)e10, -5.9241595750(14)e10, 7.60353201(8)e9, 5.90560337(3)e9, ; _pd_proc_ls_pref_orient_corr ; Simple spherical harmonic correction Order = 6 Coefficients: 0:0:C(6,6) = -0.116(29); 0:0:C(4,4) = 0.151(24); 0:0:C(6,-2) = -0.14(3); 0:0:C(2,-2) = -0.043(21); 0:0:C(4,-4) = -0.373(23); 0:0:C(2,2) = 0.396(16); 0:0:C(4,0) = -0.081(22); 0:0:C(6,-6) = -0.190(31); 0:0:C(6,4) = -0.135(31); 0:0:C(4,2) = -0.104(22); 0:0:C(6,2) = 0.094(30); 0:0:C(6,-4) = 0.051(23); 0:0:C(6,0) = -0.183(31); 0:0:C(2,0) = -0.454(15); 0:0:C(4,-2) = 0.159(26); ; _pd_proc_ls_profile_function ; Finger-Cox-Jephcoat function parameters U, V, W, X, Y, SH/L: peak variance(Gauss) = Utan(Th)^2^+Vtan(Th)+W: peak HW(Lorentz) = X/cos(Th)+Ytan(Th); SH/L = S/L+H/L U, V, W in (centideg)^2^, X & Y in centideg 4.9(6)e3, -4.9(9)e2, 21(4), 3.8(5), -17(14), 0.002, Crystallite size in microns with "isotropic" model: parameters: Size, G/L mix 1.000, 1.000, Microstrain, "isotropic" model (10^6^ * delta Q/Q) parameters: Mustrain, G/L mix 1000.000, 1.000, ; _pd_proc_ls_prof_R_factor 0.00679 _pd_proc_ls_prof_wR_expected 0.03533 _pd_proc_ls_prof_wR_factor 0.01073 _refine_ls_goodness_of_fit_all 0.310 _refine_ls_matrix_type full _refine_ls_number_parameters 78 _refine_ls_R_Fsqd_factor 0.04561 _refine_ls_shift/su_max 0.0044 _refine_ls_wR_factor_obs 0.01074 _reflns_d_resolution_high 1.113 _reflns_d_resolution_low 5.742 _reflns_limit_h_max 4 _reflns_limit_h_min 0 _reflns_limit_k_max 10 _reflns_limit_k_min 0 _reflns_limit_l_max 3 _reflns_limit_l_min -3 _reflns_number_total 161 _cod_data_source_file d0ce01401j3.cif _cod_data_source_block clau1_022rietveld _cod_original_cell_volume 209.846(18) _cod_database_code 7200027 _refine_ls_r_f_factor 0.02366 _gsas_proc_ls_prof_r_b_factor 0.01227 _gsas_proc_ls_prof_wr_b_factor 0.02328 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 1/2-x,1/2+y,1/2-z 3 -x,-y,-z 4 1/2+x,1/2-y,1/2+z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity As1 As 0.2883(9) 0.0844(3) 0.0877(9) 1.000 Uiso 0.0161(19) 4 As2 As 0.3142(7) 0.3576(4) 0.0405(8) 1.000 Uiso 0.0161 4 O3 O 0.4788(19) 0.2188(4) 0.098(5) 1.000 Uiso 0.0161 4 O4 O 0.6570(24) 0.4236(16) 0.1598(17) 1.000 Uiso 0.0161 4 O5 O -0.0870(16) 0.1147(24) 0.1294(15) 1.000 Uiso 0.0161 4 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_length_neutron _atom_type_scat_source _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_dispersion_source As 8 16.6723 6.0701 3.4313 4.2779 2.6345 0.2647 12.9479 47.7972 2.531 0.658 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.283 0.775 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py O 12 3.0485 2.2868 1.5463 0.867 13.2771 5.7011 0.3239 32.9089 0.2508 0.5805 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.002 0.002 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 As1 O4 101.2(10) 1_555 1_555 4_454 yes O3 As1 O5 107.7(10) 1_555 1_555 1_555 yes O4 As1 O5 81.4(4) 4_454 1_555 1_555 yes O3 As2 O4 89.6(6) 1_555 1_555 1_555 yes O3 As2 O5 98.3(13) 1_555 1_555 4_554 yes O4 As2 O5 83.4(4) 1_555 1_555 4_554 yes As1 O3 As2 125.4(5) 1_555 1_555 1_555 yes As1 O4 As2 117.4(4) 4_555 1_555 1_555 yes As1 O5 As2 116.5(4) 1_555 1_555 4_455 yes loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag As1 O3 1.7711(30) 1_555 1_555 yes As1 O4 1.7723(30) 1_555 4_454 yes As1 O5 1.7727(30) 1_555 1_555 yes As2 O3 1.7695(30) 1_555 1_555 yes As2 O4 1.7707(31) 1_555 1_555 yes As2 O5 1.7745(30) 1_555 4_554 yes loop_ _pd_meas_2theta_scan _pd_meas_intensity_total _pd_calc_intensity_total _pd_proc_intensity_bkg_calc _pd_proc_ls_weight 0.00440 123.55812 0 0 0 0.01320 120.93942 0 0 0 0.02201 122.92802 0 0 0 0.03081 117.33517 0 0 0 0.03961 109.45241 0 0 0 0.04841 106.89235 0 0 0 0.05721 108.24887 0 0 0 0.06602 108.98679 0 0 0 0.07482 108.46229 0 0 0 0.08362 108.07855 0 0 0 0.09242 107.1226 0 0 0 0.10122 108.49148 0 0 0 0.11003 108.09016 0 0 0 0.11883 106.49725 0 0 0 0.12763 106.80907 0 0 0 0.13643 107.56809 0 0 0 0.14523 106.87467 0 0 0 0.15404 105.88436 0 0 0 0.16284 105.38555 0 0 0 0.17164 106.17921 0 0 0 0.18044 106.37264 0 0 0 0.18925 105.92779 0 0 0 0.19805 105.23566 0 0 0 0.20685 105.26104 0 0 0 0.21565 106.18977 0 0 0 0.22445 106.53265 0 0 0 0.23326 106.14673 0 0 0 0.24206 104.53188 0 0 0 0.25086 104.96959 0 0 0 0.25966 105.98267 0 0 0 0.26846 107.43164 0 0 0 0.27727 108.67992 0 0 0 0.28607 109.68424 0 0 0 0.29487 108.63837 0 0 0 0.30367 108.79155 0 0 0 0.31248 107.57991 0 0 0 0.32128 107.75385 0 0 0 0.33008 108.41134 0 0 0 0.33888 109.61581 0 0 0 0.34768 109.10374 0 0 0 0.35649 108.48344 0 0 0 0.36529 108.80511 0 0 0 0.37409 108.65018 0 0 0 0.38289 109.06806 0 0 0 0.39169 109.27916 0 0 0 0.40050 109.05614 0 0 0 0.40930 109.25861 0 0 0 0.41810 110.09598 0 0 0 0.42690 110.70638 0 0 0 0.43570 110.94786 0 0 0 0.44451 111.45959 0 0 0 0.45331 111.21628 0 0 0 0.46211 110.81545 0 0 0 0.47091 109.91901 0 0 0 0.47972 109.47006 0 0 0 0.48852 108.20916 0 0 0 0.49732 107.56028 0 0 0 0.50612 107.6401 0 0 0 0.51492 108.40923 0 0 0 0.52373 109.2906 0 0 0 0.53253 110.18373 0 0 0 0.54133 109.61496 0 0 0 0.55013 109.16758 0 0 0 0.55893 110.12597 0 0 0 0.56774 110.17021 0 0 0 0.57654 109.19323 0 0 0 0.58534 110.03387 0 0 0 0.59414 111.18174 0 0 0 0.60295 111.35846 0 0 0 0.61175 110.74066 0 0 0 0.62055 109.77939 0 0 0 0.62935 108.35408 0 0 0 0.63815 106.99469 0 0 0 0.64696 107.49648 0 0 0 0.65576 109.23294 0 0 0 0.66456 110.30535 0 0 0 0.67336 109.5407 0 0 0 0.68216 109.95036 0 0 0 0.69097 110.70779 0 0 0 0.69977 111.29282 0 0 0 0.70857 110.06356 0 0 0 0.71737 109.56662 0 0 0 0.72617 109.37945 0 0 0 0.73498 109.13495 0 0 0 0.74378 109.75466 0 0 0 0.75258 110.4618 0 0 0 0.76138 110.97642 0 0 0 0.77019 111.03584 0 0 0 0.77899 110.9129 0 0 0 0.78779 109.57475 0 0 0 0.79659 109.20807 0 0 0 0.80539 110.55334 0 0 0 0.81420 111.65931 0 0 0 0.82300 113.20338 0 0 0 0.83180 112.75336 0 0 0 0.84060 113.32253 0 0 0 0.84940 113.57771 0 0 0 0.85821 115.075 0 0 0 0.86701 116.4992 0 0 0 0.87581 119.12157 0 0 0 0.88461 119.24162 0 0 0 0.89342 118.98831 0 0 0 0.90222 119.59948 0 0 0 0.91102 120.10953 0 0 0 0.91982 119.88456 0 0 0 0.92862 120.62733 0 0 0 0.93743 120.58004 0 0 0 0.94623 124.31991 0 0 0 0.95503 127.48731 0 0 0 0.96383 132.57372 0 0 0 0.97263 134.1682 0 0 0 0.98144 133.2993 0 0 0 0.99024 134.01561 0 0 0 0.99904 137.70692 0 0 0 1.00784 141.84351 0 0 0 1.01664 145.82269 0 0 0 1.02545 149.64551 0 0 0 1.03425 157.8775 0 0 0 1.04305 164.4088 0 0 0 1.05185 170.86931 0 0 0 1.06066 175.90364 0 0 0 1.06946 188.45908 0 0 0 1.07826 195.15785 0 0 0 1.08706 199.60533 0 0 0 1.09586 204.03349 0 0 0 1.10467 211.1107 0 0 0 1.11347 218.04807 0 0 0 1.12227 221.79057 0 0 0 1.13107 225.61436 0 0 0 1.13987 230.18839 0 0 0 1.14868 234.26454 0 0 0 1.15748 238.69354 0 0 0 1.16628 241.51338 0 0 0 1.17508 243.52486 0 0 0 1.18389 245.8232 0 0 0 1.19269 248.57402 0 0 0 1.20149 250.47205 0 0 0 1.21029 252.60234 0 0 0 1.21909 254.61615 0 0 0 1.22790 255.754 0 0 0 1.23670 257.60425 0 0 0 1.24550 259.04099 0 0 0 1.25430 261.98984 0 0 0 1.26310 263.74042 0 0 0 1.27191 264.98615 0 0 0 1.28071 266.26486 0 0 0 1.28951 267.73206 0 0 0 1.29831 270.47867 0 0 0 1.30711 272.48117 0 0 0 1.31592 274.24692 0 0 0 1.32472 276.08127 0 0 0 1.33352 276.73511 0 0 0 1.34232 277.302 0 0 0 1.35113 279.64859 0 0 0 1.35993 281.12366 0 0 0 1.36873 281.66254 0 0 0 1.37753 282.19986 0 0 0 1.38633 283.96628 0 0 0 1.39514 284.85068 0 0 0 1.40394 285.53485 0 0 0 1.41274 287.52371 0 0 0 1.42154 290.12344 0 0 0 1.43034 290.83765 0 0 0 1.43915 290.80414 0 0 0 1.44795 290.88559 0 0 0 1.45675 292.03528 0 0 0 1.46555 293.90738 0 0 0 1.47436 294.73639 0 0 0 1.48316 295.63336 0 0 0 1.49196 297.05801 0 0 0 1.50076 298.3826 0 0 0 1.50956 299.80777 0 0 0 1.51837 301.75262 0 0 0 1.52717 301.90265 0 0 0 1.53597 302.11469 0 0 0 1.54477 302.79987 0 0 0 1.55357 304.64236 0 0 0 1.56238 305.95898 0 0 0 1.57118 306.44211 0 0 0 1.57998 306.58862 0 0 0 1.58878 308.19049 0 0 0 1.59758 308.41946 0 0 0 1.60639 308.45874 0 0 0 1.61519 309.07712 0 0 0 1.62399 311.04617 0 0 0 1.63279 312.96381 0 0 0 1.64160 314.31299 0 0 0 1.65040 314.15552 0 0 0 1.65920 312.94443 0 0 0 1.66800 313.72992 0 0 0 1.67680 316.04889 0 0 0 1.68561 317.58777 0 0 0 1.69441 317.94403 0 0 0 1.70321 318.06723 0 0 0 1.71201 318.95465 0 0 0 1.72081 319.56927 0 0 0 1.72962 320.23141 0 0 0 1.73842 319.89532 0 0 0 1.74722 320.03851 0 0 0 1.75602 321.15887 0 0 0 1.76483 322.81677 0 0 0 1.77363 322.99023 0 0 0 1.78243 322.93289 0 0 0 1.79123 323.75601 0 0 0 1.80003 325.21945 0 0 0 1.80884 326.52737 0 0 0 1.81764 326.88852 0 0 0 1.82644 325.88251 0 0 0 1.83524 325.8317 0 0 0 1.84404 327.25723 0 0 0 1.85285 329.95654 0 0 0 1.86165 331.23181 0 0 0 1.87045 331.13773 0 0 0 1.87925 331.35184 0 0 0 1.88805 331.17145 0 0 0 1.89686 331.54996 0 0 0 1.90566 331.77402 0 0 0 1.91446 332.58539 0 0 0 1.92326 333.51324 0 0 0 1.93207 333.89224 0 0 0 1.94087 334.75507 0 0 0 1.94967 335.5459 0 0 0 1.95847 335.53079 0 0 0 1.96727 336.26172 0 0 0 1.97608 338.08578 0 0 0 1.98488 339.987 0 0 0 1.99368 339.16565 0 0 0 2.00248 338.33774 0 0 0 2.01128 339.15186 0 0 0 2.02009 341.77048 0 0 0 2.02889 342.9368 0 0 0 2.03769 342.78476 0 0 0 2.04649 342.85684 0 0 0 2.05530 343.2905 0 0 0 2.06410 343.98456 0 0 0 2.07290 345.21323 0 0 0 2.08170 345.72415 0 0 0 2.09050 345.1503 0 0 0 2.09931 344.65332 0 0 0 2.10811 346.63181 0 0 0 2.11691 347.58997 0 0 0 2.12571 349.01376 0 0 0 2.13451 349.30554 0 0 0 2.14332 349.44675 0 0 0 2.15212 349.80606 0 0 0 2.16092 350.50558 0 0 0 2.16972 350.5365 0 0 0 2.17852 351.02676 0 0 0 2.18733 351.04956 0 0 0 2.19613 350.96774 0 0 0 2.20493 351.22208 0 0 0 2.21373 351.65326 0 0 0 2.22254 352.83603 0 0 0 2.23134 353.50357 0 0 0 2.24014 354.05829 0 0 0 2.24894 354.78058 0 0 0 2.25774 356.20605 0 0 0 2.26655 356.8172 0 0 0 2.27535 356.88358 0 0 0 2.28415 357.16159 0 0 0 2.29295 357.74939 0 0 0 2.30175 358.02927 0 0 0 2.31056 357.94992 0 0 0 2.31936 358.23019 0 0 0 2.32816 358.30545 0 0 0 2.33696 357.85931 0 0 0 2.34576 357.61591 0 0 0 2.35457 359.10736 0 0 0 2.36337 360.55173 0 0 0 2.37217 360.54086 0 0 0 2.38097 360.32031 0 0 0 2.38978 361.41177 0 0 0 2.39858 361.8494 0 0 0 2.40738 361.75861 0 0 0 2.41618 361.26474 0 0 0 2.42498 361.6409 0 0 0 2.43379 362.4939 0 0 0 2.44259 363.53647 0 0 0 2.45139 363.68698 0 0 0 2.46019 365.07208 0 0 0 2.46899 366.22043 0 0 0 2.47780 365.51779 0 0 0 2.48660 364.1777 0 0 0 2.49540 364.30347 0 0 0 2.50420 366.36545 0 0 0 2.51301 367.21112 0 0 0 2.52181 368.00946 0 0 0 2.53061 368.20297 0 0 0 2.53941 367.98801 0 0 0 2.54821 367.72696 0 0 0 2.55702 368.06479 0 0 0 2.56582 368.39249 0 0 0 2.57462 368.8519 0 0 0 2.58342 369.91156 0 0 0 2.59222 370.45007 0 0 0 2.60103 370.45523 0 0 0 2.60983 370.2814 0 0 0 2.61863 370.8537 0 0 0 2.62743 371.92194 0 0 0 2.63624 372.01144 0 0 0 2.64504 372.08722 0 0 0 2.65384 372.50247 0 0 0 2.66264 373.09836 0 0 0 2.67144 373.06079 0 0 0 2.68025 373.99829 0 0 0 2.68905 375.24313 0 0 0 2.69785 375.57312 0 0 0 2.70665 374.76337 0 0 0 2.71545 375.38739 0 0 0 2.72426 376.1723 0 0 0 2.73306 376.43173 0 0 0 2.74186 376.37943 0 0 0 2.75066 377.78748 0 0 0 2.75946 378.42441 0 0 0 2.76827 378.50864 0 0 0 2.77707 377.07449 0 0 0 2.78587 377.79294 0 0 0 2.79467 378.1481 0 0 0 2.80348 379.30728 0 0 0 2.81228 379.83392 0 0 0 2.82108 380.55316 0 0 0 2.82988 380.22522 0 0 0 2.83868 381.42203 0 0 0 2.84749 381.45258 0 0 0 2.85629 381.18805 0 0 0 2.86509 381.45239 0 0 0 2.87389 382.17755 385.487246 385.288692 0.002616585 2.88269 382.76813 383.865079 383.665675 0.002612548 2.89150 382.9874 382.816395 382.616134 0.002611052 2.90030 383.90112 382.228765 382.027637 0.002604837 2.90910 384.50302 382.00601 381.804007 0.00260076 2.91790 384.62671 382.06675 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34.54392 195.65782 0 0 0 34.55272 190.10387 0 0 0 34.56152 194.74112 0 0 0 34.57033 197.37115 0 0 0 34.57913 201.54312 0 0 0 34.58793 215.02277 0 0 0 34.59673 214.12973 0 0 0 34.60553 205.19069 0 0 0 34.61434 210.00069 0 0 0 34.62314 215.90138 0 0 0 34.63194 207.30507 0 0 0 34.64074 195.69063 0 0 0 34.64954 195.91153 0 0 0 34.65835 209.77116 0 0 0 34.66715 210.21878 0 0 0 34.67595 188.38269 0 0 0 34.68475 190.89735 0 0 0 34.69355 204.92308 0 0 0 34.70236 207.0542 0 0 0 34.71116 214.17574 0 0 0 34.71996 203.55858 0 0 0 34.72876 203.06569 0 0 0 34.73757 208.05182 0 0 0 34.74637 216.24327 0 0 0 34.75517 223.93819 0 0 0 34.76397 220.11116 0 0 0 34.77277 219.65604 0 0 0 34.78158 211.99571 0 0 0 34.79038 196.54306 0 0 0 34.79918 179.97951 0 0 0 34.80798 168.56584 0 0 0 34.81678 182.50827 0 0 0 34.82559 200.12892 0 0 0 34.83439 211.4817 0 0 0 34.84319 220.47322 0 0 0 34.85199 230.73355 0 0 0 34.86079 234.78317 0 0 0 34.86960 222.97697 0 0 0 34.87840 209.53673 0 0 0 34.88720 201.68233 0 0 0 34.89600 205.96439 0 0 0 34.90481 208.05948 0 0 0 34.91361 203.67928 0 0 0 34.92241 218.79433 0 0 0 34.93121 226.70595 0 0 0 34.94001 203.14096 0 0 0 34.94882 201.90343 0 0 0 34.95762 211.11951 0 0 0 34.96642 208.40532 0 0 0 34.97522 209.04749 0 0 0 34.98402 210.66565 0 0 0 34.99283 206.87105 0 0 0 35.00163 198.50122 0 0 0 35.01043 194.78697 0 0 0 35.01923 198.51407 0 0 0 35.02804 205.24524 0 0 0 35.03684 212.14853 0 0 0 35.04564 207.08427 0 0 0 35.05444 203.80879 0 0 0 35.06324 207.41878 0 0 0 35.07205 223.89673 0 0 0 35.08085 226.45137 0 0 0 35.08965 221.94684 0 0 0 35.09845 222.71918 0 0 0 35.10725 234.50301 0 0 0 35.11606 233.50781 0 0 0 35.12486 222.64684 0 0 0 35.13366 215.61691 0 0 0 35.14246 216.37581 0 0 0 35.15126 226.50261 0 0 0 35.16007 230.56009 0 0 0 35.16887 227.40791 0 0 0 35.17767 215.53613 0 0 0 35.18647 217.58089 0 0 0 35.19528 223.66962 0 0 0 35.20408 219.01569 0 0 0 loop_ _gsas_i100_meas 2.02 8.14 3.26 0.00 6.72 0.70 100.00 4.09 95.05 21.00 69.06 22.90 2.46 0.15 45.55 48.62 3.34 36.32 31.05 22.09 0.27 5.17 1.32 8.66 3.91 21.90 3.36 34.71 7.06 0.73 1.25 0.11 0.75 4.13 1.79 0.04 8.61 6.01 5.05 14.15 25.66 5.82 6.41 0.10 3.29 1.90 0.36 0.61 10.55 0.31 3.08 9.42 0.72 12.84 5.17 12.00 0.18 2.32 4.94 15.63 0.12 4.71 0.04 0.38 0.37 1.61 1.22 2.72 3.74 0.86 2.12 6.41 0.11 0.05 18.53 0.88 0.00 4.29 3.93 1.11 0.06 0.11 12.41 12.39 0.46 8.26 12.71 1.68 1.82 23.47 5.46 0.99 2.71 0.34 0.84 2.54 0.02 2.41 0.28 3.33 0.33 0.63 1.29 0.27 0.00 11.84 0.57 2.33 0.45 3.08 2.14 14.21 8.30 1.65 0.17 2.53 1.08 0.04 0.04 0.03 0.75 0.33 0.47 0.01 0.07 4.72 14.02 1.49 1.43 0.01 0.23 0.03 0.01 0.00 0.83 2.46 0.12 0.49 0.32 0.54 3.53 0.08 0.14 0.02 5.11 8.38 4.90 1.62 0.03 0.33 1.34 0.15 3.01 0.39 0.03 1.03 1.19 2.80 2.43 0.26 2.41