#------------------------------------------------------------------------------ #$Date: 2025-07-01 13:39:59 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1111 $ #$URL: svn://localhost/testcod/cif/7/20/00/7200019.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7200019 loop_ _publ_author_name 'Gu\'nka, Piotr A.' 'Hanfland, Michael' 'Chen, Yu-Sheng' 'Zachara, Janusz' _publ_section_title ; High-pressure and low-temperature structural study of claudetite I, a monoclinic layered As2O3 polymorph ; _journal_issue 3 _journal_name_full CrystEngComm _journal_page_first 638 _journal_page_last 644 _journal_paper_doi 10.1039/D0CE01401J _journal_volume 23 _journal_year 2021 _chemical_formula_moiety 'As2 O3' _chemical_formula_sum 'As2 O3' _chemical_formula_weight 197.84 _chemical_name_common 'claudetite I' _chemical_name_systematic ; arsenic(III) oxide ; _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/n 1' _audit_creation_date 2020-10-21T14:51 _audit_creation_method 'created in GSAS-II' _audit_update_record ; 2020-10-22 deposited with the CCDC. 2020-12-10 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 94.803(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.6069(4) _cell_length_b 11.5455(7) _cell_length_c 4.04391(32) _cell_measurement_pressure 2.578e7(5) _cell_measurement_temperature 293 _cell_volume 214.34(3) _computing_data_reduction Fit2D _computing_structure_refinement 'GSAS-II (Toby & Von Dreele, J. Appl. Cryst. 46, 544-549, 2013)' _diffrn_ambient_pressure 2.578e7(5) _diffrn_ambient_temperature 293 _diffrn_detector 'Mar555 flat panel' _diffrn_detector_type 'Mar555 flat panel' _diffrn_measurement_device_type 'ESRF ID09A beamline' _diffrn_radiation_monochromator Si _diffrn_radiation_polarisn_ratio 0.9900 _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 0.41421 _diffrn_source 'ESRF ID09A' _diffrn_source_type synchrotron _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 6.1310 _exptl_crystal_description 'white powder' _pd_block_id 2020-10-21T14:51|clau1_024rietveld||id09a _pd_calc_method 'Rietveld Refinement' _pd_meas_number_of_points 4000 _pd_phase_name claudetiteI _pd_prep_pressure 100.0(1) _pd_prep_temperature 293 _pd_proc_info_datetime 2020-10-21T14:51 _pd_proc_ls_background_function ; Background function: "chebyschev" function with 30 terms: 758.0(7), 525.7(24), -413(6), -14084(15), 23088(14), 421160(21), -432764(5), -6.523837(14)e6, 5.979089(10)e6, 5.7577039(9)e7, -5.6409180(12)e7, -3.13551061(20)e8, 3.41115072(8)e8, 1.114138973(20)e9, -1.350889298(5)e9, -2.664226163(11)e9, 3.615162300(8)e9, 4.318579333(6)e9, -6.663689095(11)e9, -4.642584959(17)e9, 8.483079490(13)e9, 3.058800704(23)e9, -7.333402847(11)e9, -9.07499512(23)e8, 4.112659194(6)e9, -2.01355096(13)e8, -1.350273403(7)e9, 2.41003885(8)e8, 1.97078677(21)e8, -5.476662(4)e7, ; _pd_proc_ls_pref_orient_corr ; Simple spherical harmonic correction Order = 6 Coefficients: 0:0:C(6,6) = -0.055(24); 0:0:C(4,4) = 0.201(22); 0:0:C(6,-2) = -0.113(28); 0:0:C(2,-2) = -0.077(17); 0:0:C(4,-4) = -0.177(20); 0:0:C(2,2) = 0.360(14); 0:0:C(4,0) = 0.090(19); 0:0:C(6,-6) = -0.114(27); 0:0:C(6,4) = -0.138(26); 0:0:C(4,2) = -0.019(19); 0:0:C(6,2) = 0.157(27); 0:0:C(6,-4) = 0.040(19); 0:0:C(6,0) = -0.310(26); 0:0:C(2,0) = -0.436(14); 0:0:C(4,-2) = -0.024(23); ; _pd_proc_ls_profile_function ; Finger-Cox-Jephcoat function parameters U, V, W, X, Y, SH/L: peak variance(Gauss) = Utan(Th)^2^+Vtan(Th)+W: peak HW(Lorentz) = X/cos(Th)+Ytan(Th); SH/L = S/L+H/L U, V, W in (centideg)^2^, X & Y in centideg 4.1(5)e3, -6.3(8)e2, 32(4), 1.8(4), 35(11), 0.002, Crystallite size in microns with "isotropic" model: parameters: Size, G/L mix 1.000, 1.000, Microstrain, "isotropic" model (10^6^ * delta Q/Q) parameters: Mustrain, G/L mix 1000.000, 1.000, ; _pd_proc_ls_prof_R_factor 0.00572 _pd_proc_ls_prof_wR_expected 0.03560 _pd_proc_ls_prof_wR_factor 0.00865 _refine_ls_goodness_of_fit_all 0.247 _refine_ls_matrix_type full _refine_ls_number_parameters 72 _refine_ls_R_Fsqd_factor 0.04210 _refine_ls_shift/su_max 0.0009 _refine_ls_wR_factor_obs 0.00865 _reflns_d_resolution_high 1.110 _reflns_d_resolution_low 5.773 _reflns_limit_h_max 4 _reflns_limit_h_min 0 _reflns_limit_k_max 10 _reflns_limit_k_min 0 _reflns_limit_l_max 3 _reflns_limit_l_min -3 _reflns_number_total 165 _cod_data_source_file d0ce01401j3.cif _cod_data_source_block clau1_024rietveld _cod_original_cell_volume 214.336(14) _cod_database_code 7200019 _refine_ls_r_f_factor 0.01972 _gsas_proc_ls_prof_r_b_factor 0.00935 _gsas_proc_ls_prof_wr_b_factor 0.01732 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 1/2-x,1/2+y,1/2-z 3 -x,-y,-z 4 1/2+x,1/2-y,1/2+z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity As1 As 0.2872(7) 0.08550(29) 0.0840(8) 1.000 Uiso 0.0168(16) 4 As2 As 0.3141(6) 0.3580(4) 0.0369(7) 1.000 Uiso 0.0168 4 O3 O 0.4727(18) 0.2198(3) 0.110(5) 1.000 Uiso 0.0168 4 O4 O 0.6544(20) 0.4225(13) 0.1605(14) 1.000 Uiso 0.0168 4 O5 O -0.0837(14) 0.1167(21) 0.1301(12) 1.000 Uiso 0.0168 4 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_length_neutron _atom_type_scat_source _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_dispersion_source As 8 16.6723 6.0701 3.4313 4.2779 2.6345 0.2647 12.9479 47.7972 2.531 0.658 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.283 0.775 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py O 12 3.0485 2.2868 1.5463 0.867 13.2771 5.7011 0.3239 32.9089 0.2508 0.5805 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.002 0.002 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O3 As1 O4 103.2(9) 1_555 1_555 4_454 yes O3 As1 O5 106.3(9) 1_555 1_555 1_555 yes O4 As1 O5 81.63(32) 4_454 1_555 1_555 yes O3 As2 O4 89.4(5) 1_555 1_555 1_555 yes O3 As2 O5 99.5(13) 1_555 1_555 4_554 yes O4 As2 O5 84.0(4) 1_555 1_555 4_554 yes As1 O3 As2 126.1(4) 1_555 1_555 1_555 yes As1 O4 As2 118.5(3) 4_555 1_555 1_555 yes As1 O5 As2 117.7(4) 1_555 1_555 4_455 yes loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag As1 O3 1.7692(24) 1_555 1_555 yes As1 O4 1.7719(24) 1_555 4_454 yes As1 O5 1.7710(24) 1_555 1_555 yes As2 O3 1.7692(24) 1_555 1_555 yes As2 O4 1.7698(24) 1_555 1_555 yes As2 O5 1.7729(24) 1_555 4_554 yes loop_ _pd_meas_2theta_scan _pd_meas_intensity_total _pd_calc_intensity_total _pd_proc_intensity_bkg_calc _pd_proc_ls_weight 0.00440 96.739807 0 0 0 0.01321 112.25529 0 0 0 0.02202 114.26134 0 0 0 0.03083 113.05487 0 0 0 0.03963 110.8505 0 0 0 0.04844 109.05149 0 0 0 0.05725 107.2165 0 0 0 0.06605 107.25352 0 0 0 0.07486 106.58575 0 0 0 0.08367 105.65012 0 0 0 0.09248 106.66456 0 0 0 0.10128 107.10622 0 0 0 0.11009 107.33085 0 0 0 0.11890 106.08844 0 0 0 0.12770 105.40874 0 0 0 0.13651 105.26678 0 0 0 0.14532 104.98492 0 0 0 0.15413 104.86152 0 0 0 0.16293 106.12873 0 0 0 0.17174 106.1715 0 0 0 0.18055 106.71881 0 0 0 0.18935 106.2737 0 0 0 0.19816 106.59644 0 0 0 0.20697 105.8675 0 0 0 0.21578 104.99417 0 0 0 0.22458 106.26077 0 0 0 0.23339 107.45352 0 0 0 0.24220 107.50703 0 0 0 0.25100 106.60008 0 0 0 0.25981 106.87082 0 0 0 0.26862 106.73214 0 0 0 0.27743 107.53115 0 0 0 0.28623 107.02901 0 0 0 0.29504 106.62694 0 0 0 0.30385 107.8699 0 0 0 0.31265 110.25418 0 0 0 0.32146 110.24946 0 0 0 0.33027 109.796 0 0 0 0.33908 109.87531 0 0 0 0.34788 111.20074 0 0 0 0.35669 111.07552 0 0 0 0.36550 109.63926 0 0 0 0.37430 108.44827 0 0 0 0.38311 109.30788 0 0 0 0.39192 108.92265 0 0 0 0.40073 108.70267 0 0 0 0.40953 108.68332 0 0 0 0.41834 109.64022 0 0 0 0.42715 109.71897 0 0 0 0.43595 109.99931 0 0 0 0.44476 110.75852 0 0 0 0.45357 110.2117 0 0 0 0.46238 108.89198 0 0 0 0.47118 107.39268 0 0 0 0.47999 107.28155 0 0 0 0.48880 106.965 0 0 0 0.49760 107.2952 0 0 0 0.50641 108.00969 0 0 0 0.51522 108.22432 0 0 0 0.52403 108.30386 0 0 0 0.53283 108.7723 0 0 0 0.54164 110.21205 0 0 0 0.55045 109.39321 0 0 0 0.55926 109.31946 0 0 0 0.56806 109.1412 0 0 0 0.57687 109.29021 0 0 0 0.58568 109.90139 0 0 0 0.59448 109.966 0 0 0 0.60329 109.57433 0 0 0 0.61210 110.15426 0 0 0 0.62091 110.80548 0 0 0 0.62971 111.02052 0 0 0 0.63852 109.9623 0 0 0 0.64733 109.40565 0 0 0 0.65613 111.03379 0 0 0 0.66494 111.28878 0 0 0 0.67375 110.5419 0 0 0 0.68256 109.92633 0 0 0 0.69136 110.28226 0 0 0 0.70017 109.97292 0 0 0 0.70898 109.54668 0 0 0 0.71778 108.94254 0 0 0 0.72659 110.1424 0 0 0 0.73540 110.51723 0 0 0 0.74421 110.9437 0 0 0 0.75301 111.62019 0 0 0 0.76182 111.55706 0 0 0 0.77063 110.73966 0 0 0 0.77943 111.111 0 0 0 0.78824 112.52538 0 0 0 0.79705 112.31589 0 0 0 0.80586 112.24283 0 0 0 0.81466 112.48872 0 0 0 0.82347 113.48581 0 0 0 0.83228 113.63159 0 0 0 0.84108 114.20537 0 0 0 0.84989 114.55666 0 0 0 0.85870 114.19318 0 0 0 0.86751 114.02644 0 0 0 0.87631 114.89771 0 0 0 0.88512 116.15537 0 0 0 0.89393 116.93578 0 0 0 0.90273 118.88908 0 0 0 0.91154 121.64653 0 0 0 0.92035 125.03921 0 0 0 0.92916 127.37435 0 0 0 0.93796 126.10452 0 0 0 0.94677 123.48441 0 0 0 0.95558 123.04789 0 0 0 0.96438 126.63132 0 0 0 0.97319 128.17552 0 0 0 0.98200 127.42065 0 0 0 0.99081 127.49585 0 0 0 0.99961 131.89859 0 0 0 1.00842 137.17023 0 0 0 1.01723 141.31296 0 0 0 1.02604 142.11555 0 0 0 1.03484 150.23773 0 0 0 1.04365 159.5518 0 0 0 1.05246 167.90385 0 0 0 1.06126 172.68312 0 0 0 1.07007 184.35747 0 0 0 1.07888 190.55777 0 0 0 1.08769 194.91699 0 0 0 1.09649 200.86444 0 0 0 1.10530 210.98232 0 0 0 1.11411 219.32271 0 0 0 1.12291 225.39804 0 0 0 1.13172 231.99782 0 0 0 1.14053 236.42398 0 0 0 1.14934 238.71082 0 0 0 1.15814 240.7039 0 0 0 1.16695 243.53514 0 0 0 1.17576 246.87746 0 0 0 1.18456 248.92326 0 0 0 1.19337 249.79184 0 0 0 1.20218 250.15233 0 0 0 1.21099 251.64711 0 0 0 1.21979 254.65517 0 0 0 1.22860 257.66885 0 0 0 1.23741 259.75226 0 0 0 1.24621 261.31625 0 0 0 1.25502 262.51599 0 0 0 1.26383 263.84576 0 0 0 1.27264 264.93341 0 0 0 1.28144 267.03638 0 0 0 1.29025 270.14401 0 0 0 1.29906 272.41605 0 0 0 1.30786 272.9501 0 0 0 1.31667 273.69727 0 0 0 1.32548 274.3967 0 0 0 1.33429 276.30978 0 0 0 1.34309 278.99957 0 0 0 1.35190 281.43161 0 0 0 1.36071 283.49301 0 0 0 1.36951 284.38562 0 0 0 1.37832 285.29654 0 0 0 1.38713 286.16083 0 0 0 1.39594 287.02539 0 0 0 1.40474 287.60025 0 0 0 1.41355 287.91245 0 0 0 1.42236 287.81738 0 0 0 1.43116 289.06891 0 0 0 1.43997 290.70898 0 0 0 1.44878 292.52206 0 0 0 1.45759 293.7395 0 0 0 1.46639 294.76077 0 0 0 1.47520 296.38208 0 0 0 1.48401 297.48257 0 0 0 1.49281 298.81461 0 0 0 1.50162 299.95657 0 0 0 1.51043 300.11142 0 0 0 1.51924 301.18607 0 0 0 1.52804 301.28018 0 0 0 1.53685 301.08746 0 0 0 1.54566 302.21091 0 0 0 1.55446 304.5188 0 0 0 1.56327 305.51526 0 0 0 1.57208 306.94226 0 0 0 1.58089 307.80768 0 0 0 1.58969 308.28763 0 0 0 1.59850 308.44083 0 0 0 1.60731 309.9827 0 0 0 1.61612 311.40787 0 0 0 1.62492 311.12247 0 0 0 1.63373 310.54309 0 0 0 1.64254 311.03653 0 0 0 1.65134 313.10999 0 0 0 1.66015 315.17801 0 0 0 1.66896 314.97235 0 0 0 1.67777 314.98529 0 0 0 1.68657 314.82568 0 0 0 1.69538 315.63489 0 0 0 1.70419 317.79868 0 0 0 1.71299 320.34509 0 0 0 1.72180 320.9375 0 0 0 1.73061 321.13654 0 0 0 1.73942 321.57101 0 0 0 1.74822 322.97443 0 0 0 1.75703 324.0889 0 0 0 1.76584 324.68958 0 0 0 1.77464 325.15308 0 0 0 1.78345 324.86127 0 0 0 1.79226 324.96884 0 0 0 1.80107 325.46979 0 0 0 1.80987 325.793 0 0 0 1.81868 326.41437 0 0 0 1.82749 327.17093 0 0 0 1.83629 328.82941 0 0 0 1.84510 329.55289 0 0 0 1.85391 330.17639 0 0 0 1.86272 330.01611 0 0 0 1.87152 330.61987 0 0 0 1.88033 331.64871 0 0 0 1.88914 333.45126 0 0 0 1.89794 334.59955 0 0 0 1.90675 334.27484 0 0 0 1.91556 332.93323 0 0 0 1.92437 332.31076 0 0 0 1.93317 333.73309 0 0 0 1.94198 335.35449 0 0 0 1.95079 336.99625 0 0 0 1.95959 337.71518 0 0 0 1.96840 338.55695 0 0 0 1.97721 338.56372 0 0 0 1.98602 338.21249 0 0 0 1.99482 339.20786 0 0 0 2.00363 340.13971 0 0 0 2.01244 340.97 0 0 0 2.02124 341.36084 0 0 0 2.03005 342.73523 0 0 0 2.03886 343.74997 0 0 0 2.04767 343.50778 0 0 0 2.05647 343.50531 0 0 0 2.06528 345.22922 0 0 0 2.07409 346.18375 0 0 0 2.08289 346.69446 0 0 0 2.09170 346.47815 0 0 0 2.10051 346.82846 0 0 0 2.10932 347.27551 0 0 0 2.11812 348.15518 0 0 0 2.12693 349.17349 0 0 0 2.13574 350.07663 0 0 0 2.14455 351.11896 0 0 0 2.15335 351.00772 0 0 0 2.16216 350.1886 0 0 0 2.17097 350.31299 0 0 0 2.17977 351.80042 0 0 0 2.18858 351.91299 0 0 0 2.19739 351.12677 0 0 0 2.20620 352.32852 0 0 0 2.21500 353.68591 0 0 0 2.22381 354.77426 0 0 0 2.23262 355.8176 0 0 0 2.24142 356.82663 0 0 0 2.25023 357.22351 0 0 0 2.25904 357.4664 0 0 0 2.26785 357.46814 0 0 0 2.27665 357.39951 0 0 0 2.28546 356.65298 0 0 0 2.29427 357.38239 0 0 0 2.30307 359.17435 0 0 0 2.31188 360.51266 0 0 0 2.32069 360.26947 0 0 0 2.32950 359.76367 0 0 0 2.33830 359.2244 0 0 0 2.34711 359.46732 0 0 0 2.35592 360.45773 0 0 0 2.36472 361.96167 0 0 0 2.37353 363.19568 0 0 0 2.38234 364.0394 0 0 0 2.39115 363.20151 0 0 0 2.39995 362.91592 0 0 0 2.40876 363.89404 0 0 0 2.41757 363.78766 0 0 0 2.42637 363.96603 0 0 0 2.43518 364.02866 0 0 0 2.44399 365.33795 0 0 0 2.45280 366.46179 0 0 0 2.46160 366.90051 0 0 0 2.47041 366.44138 0 0 0 2.47922 365.96628 0 0 0 2.48802 366.21744 0 0 0 2.49683 367.59796 0 0 0 2.50564 368.7764 0 0 0 2.51445 369.1759 0 0 0 2.52325 369.47137 0 0 0 2.53206 369.74707 0 0 0 2.54087 369.65222 0 0 0 2.54967 369.42609 0 0 0 2.55848 369.95389 0 0 0 2.56729 371.23621 0 0 0 2.57610 372.01105 0 0 0 2.58490 372.31183 0 0 0 2.59371 372.36957 0 0 0 2.60252 372.7038 0 0 0 2.61132 373.39127 0 0 0 2.62013 373.99442 0 0 0 2.62894 373.61493 0 0 0 2.63775 373.74933 0 0 0 2.64655 374.32623 0 0 0 2.65536 374.61526 0 0 0 2.66417 374.0386 0 0 0 2.67298 373.96805 0 0 0 2.68178 374.20212 0 0 0 2.69059 374.60272 0 0 0 2.69940 375.35428 0 0 0 2.70820 374.83011 0 0 0 2.71701 375.19678 0 0 0 2.72582 375.99225 0 0 0 2.73463 377.5824 0 0 0 2.74343 377.82452 0 0 0 2.75224 377.25769 0 0 0 2.76105 377.46182 0 0 0 2.76985 378.9715 386.024017 385.846856 0.00263872 2.77866 379.87149 383.517798 383.339892 0.00263247 2.78747 380.22607 381.600125 381.421466 0.00263001 2.79628 380.72809 380.192135 380.012077 0.00262655 2.80508 380.98944 379.220898 379.040073 0.00262474 2.81389 381.45834 378.622647 378.441047 0.00262152 2.82270 381.97238 378.339636 378.157255 0.00261799 2.83150 381.65366 378.320285 378.137115 0.00262018 2.84031 381.49997 378.518645 378.33468 0.00262123 2.84912 381.93771 378.893945 378.709176 0.00261823 2.85793 382.37076 379.410167 379.224587 0.00261526 2.86673 382.6405 380.044755 379.849209 0.00261342 2.87554 382.71039 380.751726 380.555332 0.00261294 2.88435 384.00241 381.516075 381.318825 0.00260415 2.89315 384.51163 382.316929 382.118813 0.0026007 2.90196 383.83527 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205.81499 0 0 0 34.99528 209.24017 0 0 0 35.00409 208.24417 0 0 0 35.01289 206.17682 0 0 0 35.02170 200.99599 0 0 0 35.03051 202.99979 0 0 0 35.03931 202.10872 0 0 0 35.04812 204.61475 0 0 0 35.05693 210.61545 0 0 0 35.06573 213.5984 0 0 0 35.07454 209.99805 0 0 0 35.08335 212.81131 0 0 0 35.09215 220.74205 0 0 0 35.10096 221.68649 0 0 0 35.10977 217.4294 0 0 0 35.11858 209.85643 0 0 0 35.12738 206.45421 0 0 0 35.13619 212.35965 0 0 0 35.14500 221.2728 0 0 0 35.15380 222.23476 0 0 0 35.16261 221.46591 0 0 0 35.17142 212.37271 0 0 0 35.18023 209.26486 0 0 0 35.18903 212.81624 0 0 0 35.19784 210.18991 0 0 0 35.20665 207.22572 0 0 0 35.21545 206.48766 0 0 0 35.22426 214.95766 0 0 0 loop_ _gsas_i100_meas 2.63 10.93 4.12 0.04 6.35 0.88 100.00 5.08 83.55 28.51 66.28 21.81 1.65 0.14 52.08 38.47 2.65 40.06 37.46 27.30 6.11 0.10 1.49 9.21 4.59 31.73 3.92 43.55 7.24 0.64 1.37 0.03 0.67 5.69 1.47 0.05 7.03 8.08 4.99 17.10 24.76 6.60 6.75 0.09 4.85 1.93 0.12 0.40 11.74 0.24 3.55 7.28 0.98 13.57 4.56 13.67 0.34 2.85 4.49 18.67 0.07 5.15 0.03 0.49 0.49 1.81 1.40 3.59 2.91 1.49 1.08 7.18 0.42 16.79 0.13 1.43 0.00 4.81 3.96 0.09 1.01 14.75 0.07 10.11 0.69 10.28 13.68 1.81 20.90 1.91 4.41 1.13 3.14 0.49 1.33 4.06 0.02 2.64 0.33 5.45 0.60 1.11 1.15 0.52 0.00 10.37 0.65 2.66 0.49 4.12 2.29 15.03 10.64 0.49 2.43 1.67 1.88 0.06 0.01 0.04 0.46 0.82 0.65 0.00 0.09 4.57 13.41 1.51 1.19 0.51 0.00 0.01 0.02 0.00 0.78 2.91 0.16 0.56 0.27 0.52 3.11 0.06 0.04 8.88 6.59 0.01 4.69 1.46 0.03 0.43 1.24 3.24 0.11 0.46 0.05 1.39 1.45 3.13 2.26 0.36 2.86 0.99 0.69 1.85 0.08