#------------------------------------------------------------------------------
#$Date: 2025-07-01 13:39:17 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1110 $
#$URL: svn://crystallography.net/testcod/cif/7/20/00/7200001.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7200001
loop_
_publ_author_name
'Ferdov, Stanislav'
'Shivachev, Boris'
'Titorenkova, Rositsa'
'Petrova, Nadia'
'Tarassov, Mihail'
'Nikolova, Rositsa'
_publ_section_title
;
 Indium silicate with an imandrite-type structure
;
_journal_issue                   20
_journal_name_full               'RSC Advances'
_journal_page_first              12531
_journal_page_last               12536
_journal_paper_doi               10.1039/D2RA00864E
_journal_volume                  12
_journal_year                    2022
_chemical_formula_sum            'Ca3.16 In1.36 Na12.53 O36 Si12'
_chemical_formula_weight         1483.72
_chemical_name_common            MS-2
_space_group_IT_number           58
_space_group_name_Hall           '-P 2 2n'
_space_group_name_H-M_alt        'P n n m'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n n m'
_audit_creation_date             2022-02-04T14:15
_audit_creation_method           'created in GSAS-II'
_audit_update_record
;
2022-02-09 deposited with the CCDC.	2022-04-14 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            1
_cell_length_a                   7.459427
_cell_length_b                   10.620756
_cell_length_c                   10.375741
_cell_measurement_temperature    300
_cell_volume                     822.016
_computing_structure_refinement
'GSAS-II (Toby & Von Dreele, J. Appl. Cryst. 46, 544-549, 2013)'
_diffrn_ambient_pressure         100
_diffrn_ambient_temperature      300
_diffrn_measurement_device_type  'Empyrean, Panalytical'
_diffrn_radiation_polarisn_ratio 0.7000
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_exptl_crystal_density_diffrn    2.9973
_pd_block_id
2022-02-04T14:15|imandritev2a_OK|noname|Empyrean
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  colourless
_pd_meas_2theta_range_inc        0.01313
_pd_meas_2theta_range_max        99.99343
_pd_meas_2theta_range_min        3.01317
_pd_meas_number_of_points        7387
_pd_phase_name                   'Ca3.25 In1.37 Na12.46 O36 Si12'
_pd_proc_info_datetime           2022-02-04T14:15
_pd_proc_ls_background_function
;
Background function: "chebyschev-1" function with 20 terms:
    57.97(22), -78.2(4), 51.7(4), -26.0(4), 10.2(4), -1.2(4), 
    -1.7(3), 1.3(3), -0.8(3), 0.5(3), 0.1(3), -0.15(31), 0.91(30), 
    -0.97(30), 0.15(29), 0.42(28), -0.38(25), 0.33(24), -0.27(20), 
    -1.18(18), 
;
_pd_proc_ls_pref_orient_corr     none
_pd_proc_ls_profile_function
;
Finger-Cox-Jephcoat function parameters U, V, W, X, Y, SH/L:
  peak variance(Gauss) = Utan(Th)^2^+Vtan(Th)+W:
  peak HW(Lorentz) = X/cos(Th)+Ytan(Th); SH/L = S/L+H/L
  U, V, W in (centideg)^2^, X & Y in centideg
    2.000, -2.000, 5.000, 0.000, 0.000, 0.002, 

;
_pd_proc_ls_prof_R_factor        0.11371
_pd_proc_ls_prof_wR_expected     0.11625
_pd_proc_ls_prof_wR_factor       0.15318
_refine_ls_goodness_of_fit_all   1.320
_refine_ls_matrix_type           full
_refine_ls_number_parameters     21
_refine_ls_R_factor_all          0.0569
_refine_ls_R_Fsqd_factor         0.10910
_refine_ls_shift/su_max          0.0000
_refine_ls_wR_factor_obs         0.15318
_reflns_d_resolution_high        1.006
_reflns_d_resolution_low         7.422
_reflns_limit_h_max              7
_reflns_limit_h_min              0
_reflns_limit_k_max              10
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_total             460
_cod_data_source_file            d2ra00864e2.cif
_cod_data_source_block           imandritev2a_OK
_cod_database_code               7200001
_refine_ls_r_f_factor            0.05698
_gsas_proc_ls_prof_r_b_factor    0.12215
_gsas_proc_ls_prof_wr_b_factor   0.15222
_publcif_funding_html
;
;
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 x,y,z
2 1/2-x,1/2+y,1/2+z
3 1/2+x,1/2-y,1/2+z
4 -x,-y,z
5 -x,-y,-z
6 1/2+x,1/2-y,1/2-z
7 1/2-x,1/2+y,1/2-z
8 x,y,-z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_adp_type
_atom_site_U_iso_or_equiv
_atom_site_site_symmetry_multiplicity
Na1 Na 0.52054 0.26263 0.73882 1.0000 Uani 0.0271 8
Na2 Na 0.50000 0.50000 1.00000 0.9673 Uani 0.0453 2
Ca1 Ca 0.50000 1.00000 1.00000 0.7185 Uani 0.0140 2
Na11 Na 0.50000 1.00000 1.00000 0.2559 Uani 0.0148 2
Ca2 Ca 0.26023 0.25289 1.00000 0.4296 Uani 0.0163 4
Na21 Na 0.25970 0.25165 1.00000 0.5207 Uani 0.0122 4
Si1 Si 0.21431 0.50953 0.78097 1.0000 Uani 0.0287 8
Si2 Si 0.24335 0.71446 1.00000 1.0000 Uani 0.0203 4
In In 0.50000 0.50000 0.50000 0.6803 Uani 0.0179 2
O1 O 0.42313 0.79459 1.00000 1.0000 Uani 0.0320 4
O2 O 0.05855 0.78976 1.00000 1.0000 Uani 0.0279 4
O3 O 0.00000 0.50000 0.75110 1.0000 Uani 0.0463 4
O4 O 0.24394 0.62414 0.88415 1.0000 Uani 0.0237 8
O5 O 0.29324 0.55920 0.63863 1.0000 Uani 0.0224 8
O6 O 0.27628 0.38310 0.82737 1.0000 Uani 0.0444 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_length_neutron
_atom_type_scat_source
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_dispersion_source
Ca 3.155 8.6266 7.3873 1.5899 1.0211 10.4421 0.6599 85.7484 178.437 1.3751 0.47
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.364 1.285
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py
In 1.361 19.1624 18.5596 4.2948 2.0396 0.5476 6.3776 25.8499 92.8029 4.9391
0.4065 https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.077 5.044
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py
Na 12.529 4.7626 3.1736 1.2674 1.1128 3.285 8.8422 0.3136 129.424 0.676 0.363
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.135 0.124
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py
O 36 3.0485 2.2868 1.5463 0.867 13.2771 5.7011 0.3239 32.9089 0.2508 0.5805
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.049 0.032
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py
Si 12 6.2915 3.0353 1.9891 1.541 2.4386 32.3337 0.6785 81.6937 1.1407 0.4151
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py 0.254 0.330
https://subversion.xray.aps.anl.gov/pyGSAS/trunk/atmdata.py
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_wavelength_id
1.54051 1.0 1
1.54433 0.5000 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ca2 Na1 Na21 0.252 3_554 1_555 3_554 yes
Ca2 Na2 Ca2 180 1_555 1_555 4_665 yes
Ca2 Na2 Na21 0.075 1_555 1_555 1_555 yes
Ca2 Na2 Na21 179.925 4_665 1_555 1_555 yes
Ca2 Na2 Na21 179.925 1_555 1_555 4_665 yes
Ca2 Na2 Na21 0.075 4_665 1_555 4_665 yes
Na21 Na2 Na21 180 1_555 1_555 4_665 yes
Ca2 Ca1 Ca2 180 1_565 1_555 4_665 yes
Ca2 Ca1 Na21 0.189 1_565 1_555 1_565 yes
Ca2 Ca1 Na21 179.811 4_665 1_555 1_565 yes
Ca2 Ca1 Na21 179.811 1_565 1_555 4_665 yes
Ca2 Ca1 Na21 0.189 4_665 1_555 4_665 yes
Na21 Ca1 Na21 180 1_565 1_555 4_665 yes
Ca2 Ca1 O1 131.614 1_565 1_555 1_555 yes
Ca2 Ca1 O1 48.386 4_665 1_555 1_555 yes
Na21 Ca1 O1 131.425 1_565 1_555 1_555 yes
Na21 Ca1 O1 48.575 4_665 1_555 1_555 yes
Ca2 Ca1 O1 48.386 1_565 1_555 4_675 yes
Ca2 Ca1 O1 131.614 4_665 1_555 4_675 yes
Na21 Ca1 O1 48.575 1_565 1_555 4_675 yes
Na21 Ca1 O1 131.425 4_665 1_555 4_675 yes
O1 Ca1 O1 180 1_555 1_555 4_675 yes
Ca2 Na11 Ca2 180 1_565 1_555 4_665 yes
Ca2 Na11 Na21 0.189 1_565 1_555 1_565 yes
Ca2 Na11 Na21 179.811 4_665 1_555 1_565 yes
Ca2 Na11 Na21 179.811 1_565 1_555 4_665 yes
Ca2 Na11 Na21 0.189 4_665 1_555 4_665 yes
Na21 Na11 Na21 180 1_565 1_555 4_665 yes
Ca2 Na11 O1 131.614 1_565 1_555 1_555 yes
Ca2 Na11 O1 48.386 4_665 1_555 1_555 yes
Na21 Na11 O1 131.425 1_565 1_555 1_555 yes
Na21 Na11 O1 48.575 4_665 1_555 1_555 yes
Ca2 Na11 O1 48.386 1_565 1_555 4_675 yes
Ca2 Na11 O1 131.614 4_665 1_555 4_675 yes
Na21 Na11 O1 48.575 1_565 1_555 4_675 yes
Na21 Na11 O1 131.425 4_665 1_555 4_675 yes
O1 Na11 O1 180 1_555 1_555 4_675 yes
Na1 Ca2 Na1 108.145 3_455 1_555 6_567 yes
Na1 Ca2 Na2 111.934 3_455 1_555 1_555 yes
Na1 Ca2 Na2 111.934 6_567 1_555 1_555 yes
Na1 Ca2 Ca1 106.202 3_455 1_555 1_545 yes
Na1 Ca2 Ca1 106.202 6_567 1_555 1_545 yes
Na2 Ca2 Ca1 112.067 1_555 1_555 1_545 yes
Na1 Ca2 O1 124.067 3_455 1_555 4_665 yes
Na1 Ca2 O1 124.067 6_567 1_555 4_665 yes
Na2 Ca2 O1 67.778 1_555 1_555 4_665 yes
Ca1 Ca2 O1 44.288 1_545 1_555 4_665 yes
Na1 Ca2 O2 54.265 3_455 1_555 4_565 yes
Na1 Ca2 O2 54.265 6_567 1_555 4_565 yes
Na2 Ca2 O2 135.058 1_555 1_555 4_565 yes
Ca1 Ca2 O2 112.875 1_545 1_555 4_565 yes
O1 Ca2 O2 157.164 4_665 1_555 4_565 yes
Na1 Ca2 O6 134.731 3_455 1_555 1_555 yes
Na1 Ca2 O6 54.807 6_567 1_555 1_555 yes
Na2 Ca2 O6 57.721 1_555 1_555 1_555 yes
Ca1 Ca2 O6 118.599 1_545 1_555 1_555 yes
O1 Ca2 O6 94.345 4_665 1_555 1_555 yes
O2 Ca2 O6 99.56 4_565 1_555 1_555 yes
Na1 Ca2 O6 54.807 3_455 1_555 8_557 yes
Na1 Ca2 O6 134.731 6_567 1_555 8_557 yes
Na2 Ca2 O6 57.721 1_555 1_555 8_557 yes
Ca1 Ca2 O6 118.599 1_545 1_555 8_557 yes
O1 Ca2 O6 94.345 4_665 1_555 8_557 yes
O2 Ca2 O6 99.56 4_565 1_555 8_557 yes
O6 Ca2 O6 104.451 1_555 1_555 8_557 yes
Na1 Na21 Na1 108.3 3_455 1_555 6_567 yes
Na1 Na21 Na2 111.655 3_455 1_555 1_555 yes
Na1 Na21 Na2 111.655 6_567 1_555 1_555 yes
Na1 Na21 Ca1 106.491 3_455 1_555 1_545 yes
Na1 Na21 Ca1 106.491 6_567 1_555 1_545 yes
Na2 Na21 Ca1 111.952 1_555 1_555 1_545 yes
Na1 Na21 O6 134.468 3_455 1_555 1_555 yes
Na1 Na21 O6 54.817 6_567 1_555 1_555 yes
Na2 Na21 O6 57.434 1_555 1_555 1_555 yes
Ca1 Na21 O6 118.654 1_545 1_555 1_555 yes
Na1 Na21 O6 54.817 3_455 1_555 8_557 yes
Na1 Na21 O6 134.468 6_567 1_555 8_557 yes
Na2 Na21 O6 57.434 1_555 1_555 8_557 yes
Ca1 Na21 O6 118.654 1_545 1_555 8_557 yes
O6 Na21 O6 103.914 1_555 1_555 8_557 yes
O3 Si1 O4 107.625 1_555 1_555 1_555 yes
O3 Si1 O5 101.327 1_555 1_555 1_555 yes
O4 Si1 O5 107.165 1_555 1_555 1_555 yes
O3 Si1 O6 107.908 1_555 1_555 1_555 yes
O4 Si1 O6 114.491 1_555 1_555 1_555 yes
O5 Si1 O6 117.177 1_555 1_555 1_555 yes
O1 Si2 O2 117.479 1_555 1_555 1_555 yes
O1 Si2 O4 109.379 1_555 1_555 1_555 yes
O2 Si2 O4 108.392 1_555 1_555 1_555 yes
O1 Si2 O4 109.379 1_555 1_555 8_557 yes
O2 Si2 O4 108.392 1_555 1_555 8_557 yes
O4 Si2 O4 102.814 1_555 1_555 8_557 yes
Ca1 O1 Ca2 87.325 1_555 1_555 4_665 yes
Ca1 O1 Si2 137.126 1_555 1_555 1_555 yes
Ca2 O1 Si2 135.548 4_665 1_555 1_555 yes
Ca2 O2 Si2 139.094 4_565 1_555 1_555 yes
Si1 O3 Si1 158.098 1_555 1_555 4_565 yes
Si1 O4 Si2 167.204 1_555 1_555 1_555 yes
Ca2 O6 Na21 0.278 1_555 1_555 1_555 yes
Ca2 O6 Si1 141.626 1_555 1_555 1_555 yes
Na21 O6 Si1 141.793 1_555 1_555 1_555 yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Na1 Ca2 3.33545 1_555 1_555 yes
Na1 Ca2 3.06003 1_555 3_554 yes
Na1 Na21 3.33819 1_555 1_555 yes
Na1 Na21 3.05704 1_555 3_554 yes
Na1 O2 2.56341 1_555 2_544 yes
Na1 O4 2.609 1_555 4_665 yes
Na1 O5 2.56729 1_555 4_665 yes
Na1 O6 2.40859 1_555 1_555 yes
Na1 O6 2.55069 1_555 6_556 yes
Na2 Ca2 3.176 1_555 1_555 yes
Na2 Ca2 3.176 1_555 4_665 yes
Na2 Na21 3.18914 1_555 1_555 yes
Na2 Na21 3.18914 1_555 4_665 yes
Na2 Si2 2.97544 1_555 1_555 yes
Na2 Si2 2.97544 1_555 4_665 yes
Na2 O4 2.6137 1_555 1_555 yes
Na2 O4 2.6137 1_555 4_665 yes
Na2 O4 2.6137 1_555 5_667 yes
Na2 O4 2.6137 1_555 8_557 yes
Ca1 Ca2 3.22688 1_555 1_565 yes
Ca1 Ca2 3.22688 1_555 4_665 yes
Ca1 Na21 3.2181 1_555 1_565 yes
Ca1 Na21 3.2181 1_555 4_665 yes
Ca1 O1 2.25569 1_555 1_555 yes
Ca1 O1 2.25569 1_555 4_675 yes
Ca1 O3 2.60535 1_555 2_555 yes
Ca1 O3 2.60535 1_555 6_566 yes
Ca1 O5 2.6924 1_555 2_555 yes
Ca1 O5 2.6924 1_555 3_565 yes
Ca1 O5 2.6924 1_555 6_566 yes
Ca1 O5 2.6924 1_555 7_556 yes
Na11 Ca2 3.22688 1_555 1_565 yes
Na11 Ca2 3.22688 1_555 4_665 yes
Na11 Na21 3.2181 1_555 1_565 yes
Na11 Na21 3.2181 1_555 4_665 yes
Na11 O1 2.25569 1_555 1_555 yes
Na11 O1 2.25569 1_555 4_675 yes
Na11 O3 2.60535 1_555 2_555 yes
Na11 O3 2.60535 1_555 6_566 yes
Na11 O5 2.6924 1_555 2_555 yes
Na11 O5 2.6924 1_555 3_565 yes
Na11 O5 2.6924 1_555 6_566 yes
Na11 O5 2.6924 1_555 7_556 yes
Ca2 Na1 3.33545 1_555 1_555 yes
Ca2 Na1 3.06003 1_555 3_455 yes
Ca2 Na1 3.06003 1_555 6_456 yes
Ca2 Na1 3.33545 1_555 8_557 yes
Ca2 Na2 3.176 1_555 1_555 yes
Ca2 Ca1 3.22688 1_555 1_545 yes
Ca2 In 3.31391 1_555 2_545 yes
Ca2 O1 2.41517 1_555 4_665 yes
Ca2 O2 2.42068 1_555 4_565 yes
Ca2 O5 2.54159 1_555 2_545 yes
Ca2 O5 2.54159 1_555 7_546 yes
Ca2 O6 2.26608 1_555 1_555 yes
Ca2 O6 2.26608 1_555 8_557 yes
Na21 Na1 3.33819 1_555 1_555 yes
Na21 Na1 3.05704 1_555 3_455 yes
Na21 Na1 3.05704 1_555 6_456 yes
Na21 Na1 3.33819 1_555 8_557 yes
Na21 Na2 3.18914 1_555 1_555 yes
Na21 Ca1 3.2181 1_555 1_545 yes
Na21 In 3.3009 1_555 2_545 yes
Na21 O1 2.41633 1_555 4_665 yes
Na21 O2 2.41435 1_555 4_565 yes
Na21 O5 2.53029 1_555 2_545 yes
Na21 O5 2.53029 1_555 7_546 yes
Na21 O6 2.27437 1_555 1_555 yes
Na21 O6 2.27437 1_555 8_557 yes
Si1 O3 1.63156 1_555 1_555 yes
Si1 O4 1.63607 1_555 1_555 yes
Si1 O5 1.6752 1_555 1_555 yes
Si1 O6 1.49947 1_555 1_555 yes
Si2 Na2 2.97544 1_555 1_555 yes
Si2 O1 1.58835 1_555 1_555 yes
Si2 O2 1.59368 1_555 1_555 yes
Si2 O4 1.53785 1_555 1_555 yes
Si2 O4 1.53785 1_555 8_557 yes
In Ca2 3.31391 1_555 2_554 yes
In Ca2 3.31391 1_555 3_554 yes
In Na21 3.3009 1_555 2_554 yes
In Na21 3.3009 1_555 3_554 yes
In O2 2.27522 1_555 2_544 yes
In O2 2.27522 1_555 3_564 yes
In O5 2.20067 1_555 1_555 yes
In O5 2.20067 1_555 4_665 yes
In O5 2.20067 1_555 5_666 yes
In O5 2.20067 1_555 8_556 yes
O1 Ca1 2.25569 1_555 1_555 yes
O1 Ca2 2.41517 1_555 4_665 yes
O1 Na21 2.41633 1_555 4_665 yes
O1 Si2 1.58835 1_555 1_555 yes
O2 Na1 2.56341 1_555 2_555 yes
O2 Na1 2.56341 1_555 7_556 yes
O2 Ca2 2.42068 1_555 4_565 yes
O2 Na21 2.41435 1_555 4_565 yes
O2 Si2 1.59368 1_555 1_555 yes
O2 In 2.27522 1_555 2_555 yes
O3 Ca1 2.60535 1_555 2_544 yes
O3 Si1 1.63156 1_555 1_555 yes
O3 Si1 1.63156 1_555 4_565 yes
O4 Na1 2.609 1_555 4_665 yes
O4 Na2 2.6137 1_555 1_555 yes
O4 Si1 1.63607 1_555 1_555 yes
O4 Si2 1.53785 1_555 1_555 yes
O5 Na1 2.56729 1_555 4_665 yes
O5 Ca1 2.6924 1_555 2_544 yes
O5 Ca2 2.54159 1_555 2_554 yes
O5 Na21 2.53029 1_555 2_554 yes
O5 Si1 1.6752 1_555 1_555 yes
O5 In 2.20067 1_555 1_555 yes
O6 Na1 2.40859 1_555 1_555 yes
O6 Na1 2.55069 1_555 6_456 yes
O6 Ca2 2.26608 1_555 1_555 yes
O6 Na21 2.27437 1_555 1_555 yes
O6 Si1 1.49947 1_555 1_555 yes
loop_
_pd_meas_intensity_total
_pd_calc_intensity_total
_pd_proc_intensity_bkg_calc
_pd_proc_ls_weight
399 0 0 0
368 0 0 0
362 0 0 0
353 0 0 0
373 0 0 0
381 0 0 0
404 0 0 0
323 0 0 0
341 0 0 0
378 0 0 0
350 0 0 0
349 0 0 0
390 0 0 0
381 0 0 0
346 0 0 0
337 0 0 0
323 0 0 0
344 0 0 0
350 0 0 0
297 0 0 0
322 0 0 0
335 0 0 0
341 0 0 0
331 0 0 0
314 0 0 0
349 0 0 0
330 0 0 0
325 0 0 0
319 0 0 0
302 0 0 0
339 0 0 0
317 0 0 0
310 0 0 0
309 0 0 0
325 0 0 0
279 0 0 0
307 0 0 0
323 0 0 0
310 0 0 0
293 0 0 0
274 0 0 0
307 0 0 0
305 0 0 0
291 0 0 0
279 0 0 0
246 0 0 0
289 0 0 0
261 0 0 0
304 0 0 0
301 0 0 0
290 0 0 0
289 0 0 0
271 0 0 0
271 0 0 0
292 0 0 0
271 0 0 0
281 0 0 0
270 0 0 0
271 0 0 0
279 0 0 0
257 0 0 0
275 0 0 0
266 0 0 0
290 0 0 0
286 0 0 0
277 0 0 0
245 0 0 0
285 0 0 0
275 0 0 0
239 0 0 0
263 0 0 0
256 0 0 0
280 0 0 0
265 0 0 0
243 0 0 0
264 0 0 0
263 0 0 0
273 0 0 0
277 0 0 0
269 0 0 0
262 0 0 0
272 0 0 0
241 0 0 0
276 0 0 0
249 0 0 0
250 0 0 0
269 0 0 0
279 0 0 0
262 0 0 0
262 0 0 0
234 0 0 0
279 0 0 0
248 0 0 0
241 0 0 0
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