#------------------------------------------------------------------------------ #$Date: 2025-07-01 16:06:13 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1357 $ #$URL: svn://localhost/testcod/cif/4/50/00/4500032.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4500032 loop_ _publ_author_name 'Saha, Rajat' 'Dey, Sanjoy Kumar' 'Biswas, Susobhan' 'Jana, Atish Dipankar' 'Kumar, Sanjay' _publ_section_title ; Transformation of a Mother Crystal to a Daughter Crystal through Amorphous Phase: De-assembly of Coordination Helices upon Heating and Re-assembly through Aquation ; _journal_issue 5 _journal_name_full 'Crystal Growth & Design' _journal_page_first 2135 _journal_page_last 2142 _journal_paper_doi 10.1021/cg400224a _journal_volume 13 _journal_year 2013 _chemical_formula_sum 'C7 H3 Co N O10' _chemical_formula_weight 320.03 _space_group_IT_number 14 _space_group_name_Hall '-P 2yab' _space_group_name_H-M_alt 'P 1 21/a 1' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 1 21/a 1' _audit_creation_date 2012-05-08T01:38 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2012-05-08T01:38 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 96.009(26) _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 10.8982(32) _cell_length_b 14.146(5) _cell_length_c 9.7303(28) _cell_measurement_temperature 293 _cell_volume 1491.8(8) _computing_structure_refinement GSAS _diffrn_ambient_temperature 293 _diffrn_radiation_polarisn_ratio 0.5 _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 1.5418 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _pd_block_id 2012-05-08T01:38|RAW|raw|bruker_d8 _pd_calc_method 'Rietveld Refinement' _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.02 _pd_meas_2theta_range_max 60.0001 _pd_meas_2theta_range_min 7.9001 _pd_meas_number_of_points 2606 _pd_phase_name 'from C:/Documents and Settings/Sanjoy Dey/Desktop/ntreor/gsas/raw.' _pd_proc_2theta_range_inc 0.02 _pd_proc_2theta_range_max 60.0001 _pd_proc_2theta_range_min 7.9001 _pd_proc_info_datetime 2012-05-08T01:38:47 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 24 terms. Shifted Chebyshev function of 1st kind 1: 69201.6 2: -21032.6 3: 6288.05 4: -231.516 5: -2401.32 6: 4817.90 7: -2791.68 8: 1870.08 9: 747.352 10: -1250.10 11: 1444.91 12: 677.210 13: -476.772 14: -386.697 15: -172.254 16: 278.956 17: 192.372 18: -1352.48 19: -111.988 20: -87.0297 21: 98.2957 22: -348.166 23: -80.9554 24: -179.411 ; _pd_proc_ls_peak_cutoff 0.01000 _pd_proc_ls_pref_orient_corr ; March-Dollase AXIS 1 Ratio= 0.95966 h= 0.000 k= 0.000 l= 1.000 Prefered orientation correction range: Min= -93.86877, Max= 51.89969 ; _pd_proc_ls_profile_function ; CW Profile function number 2 with 18 terms Profile coefficients for Simpson's rule integration of pseudovoigt function C.J. Howard (1982). J. Appl. Cryst.,15,615-620. P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. #1(GU) = 2177.950 #2(GV) = -282.166 #3(GW) = 30.480 #4(LX) = 4.157 #5(LY) = 23.386 #6(trns) = -112.138 #7(asym) = 1.7411 #8(shft) = 1.8405 #9(GP) = 0.000 #10(stec)= 0.00 #11(ptec)= 0.00 #12(sfec)= 0.00 #13(L11) = 0.000 #14(L22) = 0.000 #15(L33) = 0.000 #16(L12) = -0.004 #17(L13) = -0.001 #18(L23) = -0.002 Peak tails are ignored where the intensity is below 0.0100 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0245 _pd_proc_ls_prof_wR_expected 0.0038 _pd_proc_ls_prof_wR_factor 0.0395 _pd_proc_number_of_points 2606 _pd_spec_mounting ' ?' _refine_ls_goodness_of_fit_all 10.51 _refine_ls_matrix_type full _refine_ls_number_parameters 25 _refine_ls_number_restraints 24 _refine_ls_R_Fsqd_factor 1.11552 _refine_ls_shift/su_max 0.00 _refine_ls_shift/su_mean 0.00 _reflns_d_resolution_high 1.565 _reflns_d_resolution_low 9.677 _reflns_limit_h_max 6 _reflns_limit_h_min 0 _reflns_limit_k_max 9 _reflns_limit_k_min 0 _reflns_limit_l_max 6 _reflns_limit_l_min -6 _reflns_number_total 812 _cod_data_source_file cg400224a_si_003.cif _cod_data_source_block RAW_publ _cod_original_cell_volume 1491.9(7) _cod_database_code 4500032 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x+1/2,+y+1/2,-z -1 -x,-y,-z -2 +x+1/2,-y+1/2,+z loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Co CO1 0.56582 0.96326 0.2423 1.0 Uiso 0.04 4 O O1W 0.46191 1.07996 0.13164 1.0 Uiso 0.04 4 O O1 0.70815 0.97685 0.09351 1.0 Uiso 0.04 4 O O4 0.78827 0.74132 0.77036 1.0 Uiso 0.04 4 O O3 0.8677 0.60185 0.66687 1.0 Uiso 0.04 4 O O2 0.92314 0.95559 0.06727 1.0 Uiso 0.04 4 O O2W 0.44772 0.94576 0.41175 1.0 Uiso 0.04 4 C C7 0.8305 0.69398 0.66256 1.0 Uiso 0.04 4 C C2 0.95125 0.82571 0.32738 1.0 Uiso 0.04 4 C C1 0.83314 0.87072 0.26874 1.0 Uiso 0.04 4 N N1 0.71779 0.85809 0.33195 1.0 Uiso 0.04 4 C C5 0.71887 0.7992 0.45285 1.0 Uiso 0.04 4 C C6 0.82251 0.93934 0.13306 1.0 Uiso 0.04 4 C C3 0.95305 0.76843 0.45599 1.0 Uiso 0.04 4 C C4 0.83424 0.753 0.51923 1.0 Uiso 0.04 4 O O5W 0.215 0.213 -0.003 1.0 Uiso 0.04 4 O O6W 0.5047 0.36668 0.16433 1.0 Uiso 0.04 4 O O3W -0.06934 0.1032 0.42179 1.0 Uiso 0.04 4 O O4W 0.789 0.064 0.771 1.0 Uiso 0.04 4 H H2 1.01659 0.83271 0.2878 1.0 Uiso 0.06 4 H H5 0.65161 0.79026 0.48797 1.0 Uiso 0.06 4 H H3 1.02016 0.74478 0.49319 1.0 Uiso 0.06 4 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Co 4.0 0.000 0.000 12.2841 4.27910 7.34090 0.27840 4.00340 13.5359 2.34880 71.1692 1.01180 International_Tables_Vol_C O 40.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C C 28.0 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500 51.6512 0.21560 International_Tables_Vol_C N 4.0 0.000 0.000 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630 0.58260 -11.529 International_Tables_Vol_C H 12.0 0.000 0.000 0.49300 10.5109 0.32291 26.1257 0.14019 3.14236 0.04081 57.7997 0.00304 International_Tables_Vol_C loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 C7 O3 124.636(11) 1_555 . 1_555 N O4 C7 C4 116.559(22) 1_555 . 1_555 N O3 C7 C4 118.801(14) 1_555 . 1_555 N C1 C2 C3 119.184(19) 1_555 . 1_555 N C2 C1 N1 121.972(18) 1_555 . 1_555 N C2 C1 C6 123.178(18) 1_555 . 1_555 N N1 C1 C6 114.833(18) 1_555 . 1_555 N C1 N1 C5 118.600(18) 1_555 . 1_555 N N1 C5 C4 122.537(18) 1_555 . 1_555 N O1 C6 O2 124.187(17) 1_555 . 1_555 N O1 C6 C1 116.237(19) 1_555 . 1_555 N O2 C6 C1 119.576(17) 1_555 . 1_555 N C2 C3 C4 119.069(18) 1_555 . 1_555 N C7 C4 C5 119.752(19) 1_555 . 1_555 N C7 C4 C3 121.562(18) 1_555 . 1_555 N C5 C4 C3 118.547(18) 1_555 . 1_555 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag CO1 O1W 2.2163(5) . 1_555 N CO1 O1 2.2381(6) . 1_555 N CO1 O3 2.2396(6) . 2_656 N CO1 O2W 2.2093(6) . 1_555 N CO1 N1 2.3269(5) . 1_555 N O1W CO1 2.2163(5) . 1_555 N O1 CO1 2.2381(6) . 1_555 N O1 C6 1.3721(4) . 1_555 N O4 C7 1.36436(32) . 1_555 N O3 CO1 2.2396(6) . 2_646 N O3 C7 1.3642(4) . 1_555 N O2 C6 1.3462(4) . 1_555 N O2W CO1 2.2093(6) . 1_555 N C7 O4 1.36436(32) . 1_555 N C7 O3 1.3642(4) . 1_555 N C7 C4 1.6296(4) . 1_555 N C2 C1 1.4947(4) . 1_555 N C2 C3 1.48925(35) . 1_555 N C1 C2 1.4947(4) . 1_555 N C1 N1 1.4671(4) . 1_555 N C1 C6 1.6330(4) . 1_555 N N1 CO1 2.3269(5) . 1_555 N N1 C1 1.4671(4) . 1_555 N N1 C5 1.44053(33) . 1_555 N C5 N1 1.44053(33) . 1_555 N C5 C4 1.5018(4) . 1_555 N C6 O1 1.3721(4) . 1_555 N C6 O2 1.3462(4) . 1_555 N C6 C1 1.6330(4) . 1_555 N C3 C2 1.48925(35) . 1_555 N C3 C4 1.5065(4) . 1_555 N C4 C7 1.6296(4) . 1_555 N C4 C5 1.5018(4) . 1_555 N C4 C3 1.5065(4) . 1_555 N loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 87438.0 0.0000114 89161.46875 89161.46875 87453.0 0.0000114 88804.48438 88804.48438 87431.0 0.0000114 88489.03125 88489.03125 87072.0 0.0000115 88212.70313 88212.70313 88146.0 0.0000113 87973.17969 87973.17969 87914.0 0.0000114 87768.26563 87768.26563 87870.0 0.0000114 87595.85938 87595.85938 87369.0 0.0000114 87453.92188 87453.92188 88278.0 0.0000113 87340.54688 87340.54688 88079.0 0.0000114 87253.89844 87253.89844 88043.0 0.0000114 87192.21875 87192.21875 88596.0 0.0000113 87153.82813 87153.82813 88650.0 0.0000113 87137.14063 87137.14063 87468.0 0.0000114 87140.64063 87140.64063 87825.0 0.0000114 87162.86719 87162.86719 88662.0 0.0000113 87202.45313 87202.45313 88529.0 0.0000113 87258.07813 87258.07813 88469.0 0.0000113 87328.50781 87328.50781 87892.0 0.0000114 87412.54688 87412.54688 88520.0 0.0000113 87509.07813 87509.07813 88428.0 0.0000113 87617.02344 87617.02344 87916.0 0.0000114 87735.38281 87735.38281 88605.0 0.0000113 87863.18750 87863.18750 88894.0 0.0000112 87999.53125 87999.53125 88322.0 0.0000113 88143.56250 88143.56250 88551.0 0.0000113 88294.45313 88294.45313 88655.0 0.0000113 88451.44531 88451.44531 88956.0 0.0000112 88613.80469 88613.80469 88392.0 0.0000113 88780.85156 88780.85156 88675.0 0.0000113 88951.94531 88951.94531 89125.0 0.0000112 89126.47656 89126.47656 88696.0 0.0000113 89303.87500 89303.87500 88716.0 0.0000113 89483.61719 89483.61719 89982.0 0.0000111 89665.17969 89665.17969 89336.0 0.0000112 89848.10156 89848.10156 88724.0 0.0000113 90031.95313 90031.95313 89109.0 0.0000112 90216.30469 90216.30469 88791.0 0.0000113 90400.78906 90400.78906 89382.0 0.0000112 90585.04688 90585.04688 89540.0 0.0000112 90768.75000 90768.75000 89383.0 0.0000112 90951.58594 90951.58594 88899.0 0.0000112 91133.28125 91133.28125 89019.0 0.0000112 91313.56250 91313.56250 89300.0 0.0000112 91492.20313 91492.20313 89815.0 0.0000111 91668.96875 91668.96875 89500.0 0.0000112 91843.67188 91843.67188 89634.0 0.0000112 92016.11719 92016.11719 89845.0 0.0000111 92186.14844 92324.51563 89820.0 0.0000111 92353.60156 92574.11719 89799.0 0.0000111 92518.35938 92762.41406 90502.0 0.0000110 92680.29688 92951.89063 90308.0 0.0000111 92839.30469 93143.43750 91200.0 0.0000110 92995.28906 93338.40625 91911.0 0.0000109 93148.17969 93539.07031 91655.0 0.0000109 93297.89844 93749.36719 92009.0 0.0000109 93444.39063 93976.58594 92721.0 0.0000108 93587.60938 94233.83594 93290.0 0.0000107 93727.51563 94543.27344 93923.0 0.0000106 93864.08594 94939.17188 95623.0 0.0000105 93997.28906 95469.43750 97068.0 0.0000103 94127.13281 96194.43750 98610.0 0.0000101 94253.59375 97181.67969 100891.0 9.91e-6 94376.69531 98492.61719 103977.0 9.62e-6 94496.42969 100153.78125 107119.0 9.34e-6 94612.82813 102122.94531 111495.0 8.97e-6 94725.89844 104295.92188 116229.0 8.60e-6 94835.67969 106526.34375 121453.0 8.23e-6 94942.19531 108541.32031 126360.0 7.91e-6 95045.49219 109847.15625 128467.0 7.78e-6 95145.60156 109927.78906 126580.0 7.90e-6 95242.57813 108675.97656 120999.0 8.26e-6 95336.46094 106500.56250 113981.0 8.77e-6 95427.30469 104016.07813 107231.0 9.33e-6 95515.17188 101719.53125 101826.0 9.82e-6 95600.10938 99877.78906 98290.0 0.0000102 95682.17969 98557.49219 96620.0 0.0000103 95761.45313 97698.21875 95344.0 0.0000105 95837.97656 97184.44531 93534.0 0.0000107 95911.82813 96898.75000 92588.0 0.0000108 95983.07031 96749.29688 93073.0 0.0000107 96051.78125 96675.77344 93235.0 0.0000107 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150052.0 6.66e-6 97666.60156 162702.70313 127948.0 7.82e-6 97686.13281 144341.10938 114451.0 8.74e-6 97705.73438 127360.14844 106476.0 9.39e-6 97725.41406 114604.75000 102375.0 9.77e-6 97745.18750 106546.77344 100327.0 9.97e-6 97765.07031 102172.16406 98993.0 0.0000101 97785.07813 100083.32031 98598.0 0.0000101 97805.22656 99171.09375 98416.0 0.0000102 97825.52344 98778.75000 97921.0 0.0000102 97845.97656 98593.01563 97656.0 0.0000102 97866.60156 98487.93750 96726.0 0.0000103 97887.40625 98418.55469 96763.0 0.0000103 97908.39063 98369.10156 96829.0 0.0000103 97929.57031 98333.21875 96689.0 0.0000103 97950.94531 98307.50781 96574.0 0.0000104 97972.51563 98088.89844 96338.0 0.0000104 97994.28906 98093.53125 96909.0 0.0000103 98016.27344 98011.40625 96836.0 0.0000103 98038.46094 98030.75781 96879.0 0.0000103 98060.85938 98052.34375 96985.0 0.0000103 98083.46094 98074.00781 96718.0 0.0000103 98106.27344 98095.70313 97209.0 0.0000103 98129.29688 98117.40625 97298.0 0.0000103 98152.51563 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0.0000187 55243.21484 54752.48828 53704.0 0.0000186 55393.97656 54767.98828 53333.0 0.0000188 55541.88281 54784.41016 53058.0 0.0000188 55686.27734 54750.47656 53621.0 0.0000186 55826.44141 54756.67578 53803.0 0.0000186 55961.62500 54733.55859 53272.0 0.0000188 56091.02344 54738.68359 53403.0 0.0000187 56213.79297 54738.45703 53812.0 0.0000186 56329.01953 54750.55078 54247.0 0.0000184 56435.72656 54763.54297 54072.0 0.0000185 56532.94141 54794.60938 53285.0 0.0000188 56619.56641 54812.51563 53829.0 0.0000186 56694.46484 54825.26563 53725.0 0.0000186 56756.43359 54836.35156 53117.0 0.0000188 56804.20313 54823.41797 53275.0 0.0000188 56836.43359 54822.60938 53691.0 0.0000186 56851.71875 54815.91016 53135.0 0.0000188 56848.57031 54786.12500 53167.0 0.0000188 56825.41797 54755.33984 53715.0 0.0000186 56780.61719 54711.35547 53997.0 0.0000185 56712.43359 54644.06641 53490.0 0.0000187 56619.03906 54556.33203 53550.0 0.0000187 56498.52344 54378.85547 53563.0 0.0000187 56348.87891 54246.70313 53533.0 0.0000187 56167.99219 54079.67188 53770.0 0.0000186 55953.69141 53883.83594 53398.0 0.0000187 55703.58203 53666.91797 53830.0 0.0000186 55415.25781 53403.53906 53706.0 0.0000186 55086.18359 53100.90234 53920.0 0.0000185 54713.69531 52718.78125 53862.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 0 0 1 1 o 822.277 561.683 180.00 9.67684 23.86 0 0 1 2 o 778.881 561.683 180.00 9.67684 11.26 1 1 0 1 o 6479.201 5242.715 180.00 8.60348 91.35 1 1 0 2 o 5626.604 5242.715 180.00 8.60348 38.40 0 1 1 1 o 37.307 133.410 0.00 7.98696 0.01 0 1 1 2 o 38.944 133.410 0.00 7.98696 0.00 0 2 0 1 o 6179.954 6615.918 0.00 7.07320 3.43 0 2 0 2 o 5286.344 6615.918 0.00 7.07320 1.41 1 1 -1 1 o 5843.994 5453.605 180.00 6.71267 63.78 1 1 -1 2 o 5279.917 5453.605 180.00 6.71267 28.36 1 1 1 1 o 13547.186 13582.769 0.00 6.17976 81.28 1 1 1 2 o 15031.708 13582.769 0.00 6.17976 45.08 1 2 0 1 o 158.772 2785.950 180.00 5.92340 0.00 1 2 0 2 o 158.772 2785.950 180.00 5.92340 0.00 0 2 1 1 o 6815.562 7078.578 0.00 5.71037 61.07 0 2 1 2 o 6616.694 7078.578 0.00 5.71037 29.49 2 0 0 1 o 153.716 492.504 0.00 5.41915 0.00 2 0 0 2 o 153.716 492.504 0.00 5.41915 0.00 1 2 -1 1 o -261.226 719.728 180.00 5.18590 0.00 1 2 -1 2 o -261.226 719.728 180.00 5.18590 0.00 2 1 0 1 o 5059.999 4917.708 180.00 5.06055 40.85 2 1 0 2 o 6866.380 4917.708 180.00 5.06055 27.20 2 0 -1 1 o 2861.805 2819.144 0.00 4.95450 6.60 2 0 -1 2 o 2715.410 2819.144 0.00 4.95450 3.07 1 2 1 1 o 306.191 2407.445 180.00 4.92807 0.00 1 2 1 2 o 306.191 2407.445 180.00 4.92807 0.00 0 0 2 1 o 8321.804 8934.434 180.00 4.83842 47.46 0 0 2 2 o 8252.750 8934.434 180.00 4.83842 23.37 2 1 -1 1 o 590.149 311.491 0.00 4.67601 10.19 2 1 -1 2 o 756.188 311.491 0.00 4.67601 6.37 0 1 2 1 o -20.183 807.876 180.00 4.57805 0.00 0 1 2 2 o -20.183 807.876 180.00 4.57805 0.00 2 0 1 1 o 10384.241 9640.948 180.00 4.53035 51.51 2 0 1 2 o 10001.041 9640.948 180.00 4.53035 24.57 1 1 -2 1 o 9113.844 6918.288 0.00 4.37548 8.71 1 1 -2 2 o 9135.435 6918.288 0.00 4.37548 4.34 1 3 0 1 o 1196.752 11787.632 180.00 4.32395 0.00 1 3 0 2 o 1196.752 11787.632 180.00 4.32395 0.00 2 1 1 1 o 39.629 220.315 0.00 4.31451 0.00 2 2 0 1 o 11311.677 12034.101 0.00 4.30174 41.25 2 1 1 2 o 39.629 220.315 0.00 4.31451 0.00 2 2 0 2 o 8329.504 12034.101 0.00 4.30174 14.57 0 3 1 1 o 1024.432 10405.759 0.00 4.23896 0.00 0 3 1 2 o 1024.432 10405.759 0.00 4.23896 0.00 1 1 2 1 o 6882.053 6944.496 0.00 4.07506 47.10 1 1 2 2 o 6808.973 6944.496 0.00 4.07506 23.13 2 2 -1 1 o 219.767 749.905 0.00 4.05800 0.00 2 2 -1 2 o 219.767 749.905 0.00 4.05800 0.00 1 3 -1 1 o 1529.910 1478.912 0.00 4.01065 35.32 1 3 -1 2 o 1484.493 1478.912 0.00 4.01065 17.13 0 2 2 1 o 1281.992 8659.800 180.00 3.99348 0.00 0 2 2 2 o 1281.992 8659.800 180.00 3.99348 0.00 1 3 1 1 o -64.627 71.162 180.00 3.88775 0.00 1 3 1 2 o -64.627 71.162 180.00 3.88775 0.00 1 2 -2 1 o 586.785 382.954 180.00 3.85688 17.30 1 2 -2 2 o 362.047 382.954 180.00 3.85688 5.80 2 0 -2 1 o 472.727 2030.872 180.00 3.81294 0.05 2 2 1 1 o 367.777 1698.655 180.00 3.81493 0.00 2 0 -2 2 o 431.333 2030.872 180.00 3.81294 0.01 2 2 1 2 o 366.378 1698.655 180.00 3.81493 0.00 2 1 -2 1 o -91.577 497.103 0.00 3.68156 0.00 2 1 -2 2 o -91.577 497.103 0.00 3.68156 0.00 1 2 2 1 o -50.348 14.608 0.00 3.64639 0.69 1 2 2 2 o -34.043 14.608 0.00 3.64639 0.24 2 3 0 1 o 3995.734 4063.639 0.00 3.55729 35.26 2 3 0 2 o 5485.524 4063.639 0.00 3.55729 24.92 0 4 0 1 o 4313.350 2529.424 0.00 3.53660 0.62 0 4 0 2 o 4549.910 2529.424 0.00 3.53660 0.33 3 1 0 1 o 378.346 477.404 180.00 3.50042 2.46 3 1 0 2 o 99.249 477.404 180.00 3.50042 0.00 2 0 2 1 o -27.127 72.650 180.00 3.43497 0.00 2 0 2 2 o -27.127 72.650 180.00 3.43497 0.00 2 3 -1 1 o -12042.911 1721.937 0.00 3.41572 21.01 2 3 -1 2 o -7635.756 1721.937 0.00 3.41572 6.49 3 1 -1 1 o -25546.359 9853.469 180.00 3.40398 7.79 3 1 -1 2 o 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