#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:05:32 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1184 $
#$URL: svn://crystallography.net/testcod/cif/4/30/00/4300012.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4300012
loop_
_publ_author_name
'Martínez-Casado, Francisco J.'
'Ramos-Riesco, Miguel'
'Rodríguez-Cheda, José A.'
'Cucinotta, Fabio'
'Matesanz, Emilio'
'Miletto, Ivana'
'Gianotti, Enrica'
'Marchese, Leonardo'
'Matěj, Zdeněk'
_publ_section_title
;
 Unraveling the Decomposition Process of Lead(II) Acetate: Anhydrous
 Polymorphs, Hydrates, and Byproducts and Room Temperature Phosphorescence
;
_journal_issue                   17
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8576
_journal_page_last               8586
_journal_paper_doi               10.1021/acs.inorgchem.6b01116
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C12 H18 O13 Pb4'
_chemical_formula_sum            'C12 H18 O13 Pb4'
_chemical_formula_weight         1199.02
_chemical_name_common            'Tetralead(II) oxo hexaacetate'
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 106.283(2)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   24.5037(5)
_cell_length_b                   6.82814(17)
_cell_length_c                   13.9738(4)
_cell_measurement_reflns_used    1059
_cell_measurement_temperature    298
_cell_measurement_theta_max      85.0
_cell_measurement_theta_min      2.5
_cell_volume                     2244.24(10)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      298
_diffrn_detector_type            X&#x0092;Celerator
_diffrn_measurement_device_type  'PANalytical X Pert Pro Alpha-1'
_diffrn_measurement_method       '2θ scan'
_diffrn_radiation_monochromator  Ge(111)
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54056
_diffrn_source_target            Cu
_exptl_absorpt_coefficient_mu    57.61
_exptl_absorpt_correction_type   cylinder
_exptl_crystal_density_diffrn    3.549
_pd_block_diffractogram_id       Pb4O(Ac)6_profile
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.017000
_pd_meas_2theta_range_max        84.96751
_pd_meas_2theta_range_min        4.99950
_pd_meas_number_of_points        4705
_pd_meas_scan_method             step
_pd_proc_2theta_range_inc        0.017000
_pd_proc_2theta_range_max        85.0297
_pd_proc_2theta_range_min        5.0617
_pd_proc_ls_background_function  'Interpolation of points'
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        5.9774
_pd_proc_ls_prof_wR_expected     5.4392
_pd_proc_ls_prof_wR_factor       8.5620
_pd_proc_wavelength              1.540560
_pd_spec_mounting                'borosilicate capillary'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_goodness_of_fit_all   1.57
_refine_ls_number_parameters     77
_refine_ls_number_reflns         1059
_refine_ls_number_restraints     0
_refine_ls_R_I_factor            7.6853
_cod_data_source_file            ic6b01116_si_003.cif
_cod_data_source_block           Pb4OAc6
_cod_original_cell_volume        2244.24(9)
_cod_original_sg_symbol_H-M      'C 2/c'
_cod_database_code               4300012
_pd_proc_ls_prof_cr_factor       32.6057
_pd_proc_ls_prof_cwr_factor      27.4880
_pd_proc_ls_prof_cwr_expected    17.4624
_pd_proc_ls_prof_chi2            2.4779
_pd_proc_ls_prof_echi2           2.4779
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,y,-z+1/2
-x,-y,-z
x,-y,z+1/2
x+1/2,y+1/2,z
-x+1/2,y+1/2,-z+1/2
-x+1/2,-y+1/2,-z
x+1/2,-y+1/2,z+1/2
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_type_symbol
C1 -0.07710 -0.00800 0.56810 0.07885 1.00000 Uiso C
C2 -0.13510 -0.06600 0.51060 0.07885 1.00000 Uiso C
H2A -0.14630 0.00800 0.44740 0.07885 1.00000 Uiso H
H2B -0.16180 -0.03700 0.54990 0.07885 1.00000 Uiso H
H2C -0.13580 -0.20720 0.49610 0.07885 1.00000 Uiso H
C3 -0.07680 0.52000 0.85650 0.07885 1.00000 Uiso C
C4 -0.13350 0.59000 0.85830 0.07885 1.00000 Uiso C
H4A -0.14690 0.51160 0.90670 0.07885 1.00000 Uiso H
H4B -0.16040 0.57480 0.79130 0.07885 1.00000 Uiso H
H4C -0.13120 0.72860 0.87790 0.07885 1.00000 Uiso H
C5 0.16960 0.33170 0.85710 0.07885 1.00000 Uiso C
C6 0.22110 0.26170 0.83200 0.07885 1.00000 Uiso C
H6A 0.21050 0.16040 0.78020 0.07885 1.00000 Uiso H
H6B 0.24770 0.20590 0.89270 0.07885 1.00000 Uiso H
H6C 0.23930 0.37220 0.80800 0.07885 1.00000 Uiso H
O1 -0.05110 -0.11000 0.64510 0.07885 1.00000 Uiso O
O2 0.05270 0.12100 0.96620 0.07885 1.00000 Uiso O
O3 -0.05040 0.61100 0.80490 0.07885 1.00000 Uiso O
O4 -0.05370 0.38400 0.91460 0.07885 1.00000 Uiso O
O5 0.12370 0.25600 0.81180 0.07885 1.00000 Uiso O
O6 0.17830 0.45780 0.92030 0.07885 1.00000 Uiso O
O1O 0.00000 0.24800 0.75000 0.07885 1.00000 Uiso O
Pb1 0.05030 0.04160 0.67840 0.02945 1.00000 Uiso Pb
Pb2 0.05098 0.45630 0.87140 0.02945 1.00000 Uiso Pb
loop_
_atom_type_symbol
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
c 2.31000 20.84390 1.02000 10.20750 1.58860 0.56870 0.86500 51.65120 0.21560
0.01700 0.00900
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
h 0.49300 10.51090 0.32291 26.12570 0.14019 3.14236 0.04081 57.79970 0.00304
0.00000 0.00000
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
o 3.04850 13.27710 2.28680 5.70110 1.54630 0.32390 0.86700 32.90890 0.25080
0.04700 0.03200
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
pb 31.06170 0.69020 13.06370 2.35760 18.44200 8.61800 5.96960 47.25790 13.41180
-4.81900 8.49700
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 O1 118.932(5) 1_555 1_555 ?
C2 C1 O2 118.489(3) 1_555 2_556 ?
C2 C1 O5 90.374(3) 1_555 2_556 ?
C2 C1 Pb1 169.945(7) 1_555 1_555 ?
O1 C1 O2 121.964(4) 1_555 2_556 ?
O1 C1 O5 92.026(3) 1_555 2_556 ?
O1 C1 Pb1 56.581(3) 1_555 1_555 ?
O2 C1 O5 95.343(4) 2_556 2_556 ?
O2 C1 Pb1 65.396(4) 2_556 1_555 ?
O5 C1 Pb1 98.606(3) 2_556 1_555 ?
O1 C2 O2 55.778(2) 1_555 2_556 ?
C4 C3 O3 119.144(4) 1_555 1_555 ?
C4 C3 O4 118.889(3) 1_555 1_555 ?
C4 C3 O5 93.077(3) 1_555 2_556 ?
O3 C3 O4 121.536(4) 1_555 1_555 ?
O3 C3 O5 89.589(3) 1_555 2_556 ?
O4 C3 O5 93.903(5) 1_555 2_556 ?
O3 C4 O4 55.5046(18) 1_555 1_555 ?
C6 C5 O5 117.156(4) 1_555 1_555 ?
C6 C5 O6 114.557(3) 1_555 1_555 ?
C6 C5 Pb2 169.866(5) 1_555 1_555 ?
O5 C5 O6 128.288(4) 1_555 1_555 ?
O5 C5 Pb2 53.964(2) 1_555 1_555 ?
O6 C5 Pb2 74.507(3) 1_555 1_555 ?
O5 C6 O6 57.3136(19) 1_555 1_555 ?
C1 O1 O3 151.905(6) 1_555 1_545 ?
C1 O1 O3 135.037(5) 1_555 2_546 ?
C1 O1 O1O 90.495(4) 1_555 1_555 ?
C1 O1 Pb1 99.055(4) 1_555 1_555 ?
C1 O1 Pb1 115.796(6) 1_555 2_556 ?
C1 O1 Pb2 118.979(6) 1_555 2_546 ?
C2 O1 O2 60.921(2) 1_555 2_556 ?
C2 O1 O3 120.098(5) 1_555 1_545 ?
C2 O1 O3 136.570(5) 1_555 2_546 ?
C2 O1 O1O 116.131(4) 1_555 1_555 ?
C2 O1 Pb1 131.183(5) 1_555 1_555 ?
C2 O1 Pb1 117.404(5) 1_555 2_556 ?
C2 O1 Pb2 94.808(3) 1_555 2_546 ?
O2 O1 O3 174.882(5) 2_556 1_545 ?
O2 O1 O3 117.339(4) 2_556 2_546 ?
O2 O1 O1O 71.248(3) 2_556 1_555 ?
O2 O1 Pb1 70.747(3) 2_556 1_555 ?
O2 O1 Pb1 111.584(5) 2_556 2_556 ?
O2 O1 Pb2 131.132(5) 2_556 2_546 ?
O3 O1 O3 65.792(2) 1_545 2_546 ?
O3 O1 O1O 104.450(4) 1_545 1_555 ?
O3 O1 Pb1 108.659(3) 1_545 1_555 ?
O3 O1 Pb1 63.342(2) 1_545 2_556 ?
O3 O1 Pb2 53.938(2) 1_545 2_546 ?
O3 O1 O1O 101.460(4) 2_546 1_555 ?
O3 O1 Pb1 62.174(2) 2_546 1_555 ?
O3 O1 Pb1 103.646(3) 2_546 2_556 ?
O3 O1 Pb2 51.498(2) 2_546 2_546 ?
O1O O1 Pb1 48.0157(17) 1_555 1_555 ?
O1O O1 Pb1 47.6223(19) 1_555 2_556 ?
O1O O1 Pb2 148.996(5) 1_555 2_546 ?
Pb1 O1 Pb1 85.497(3) 1_555 2_556 ?
Pb1 O1 Pb2 112.805(4) 1_555 2_546 ?
Pb1 O1 Pb2 117.280(4) 2_556 2_546 ?
C1 O2 O4 142.697(4) 2_556 1_555 ?
C1 O2 O1O 86.280(4) 2_556 1_555 ?
C1 O2 Pb1 91.048(4) 2_556 2_556 ?
C1 O2 Pb2 111.431(5) 2_556 1_555 ?
C2 O2 O1 63.301(2) 2_556 2_556 ?
C2 O2 O4 173.800(4) 2_556 1_555 ?
C2 O2 O1O 113.673(4) 2_556 1_555 ?
C2 O2 Pb1 124.220(5) 2_556 2_556 ?
C2 O2 Pb2 115.836(4) 2_556 1_555 ?
O1 O2 O4 113.887(3) 2_556 1_555 ?
O1 O2 O1O 65.646(2) 2_556 1_555 ?
O1 O2 Pb1 61.337(2) 2_556 2_556 ?
O1 O2 Pb2 105.754(4) 2_556 1_555 ?
O4 O2 O1O 60.552(2) 1_555 1_555 ?
O4 O2 Pb1 54.069(2) 1_555 2_556 ?
O4 O2 Pb2 58.8998(19) 1_555 1_555 ?
O1O O2 Pb1 45.480(2) 1_555 2_556 ?
O1O O2 Pb2 46.811(2) 1_555 1_555 ?
Pb1 O2 Pb2 85.508(3) 2_556 1_555 ?
C3 O3 O1 149.596(5) 1_555 1_565 ?
C3 O3 O1 133.854(4) 1_555 2_566 ?
C3 O3 O1O 93.082(3) 1_555 1_555 ?
C3 O3 Pb1 115.831(5) 1_555 2_566 ?
C3 O3 Pb2 100.736(4) 1_555 1_555 ?
C3 O3 Pb2 117.464(6) 1_555 2_556 ?
C4 O3 O1 117.308(4) 1_555 1_565 ?
C4 O3 O1 133.207(4) 1_555 2_566 ?
C4 O3 O4 62.1628(19) 1_555 1_555 ?
C4 O3 O1O 119.322(3) 1_555 1_555 ?
C4 O3 Pb1 90.985(3) 1_555 2_566 ?
C4 O3 Pb2 132.824(4) 1_555 1_555 ?
C4 O3 Pb2 118.969(4) 1_555 2_556 ?
O1 O3 O1 66.384(3) 1_565 2_566 ?
O1 O3 O4 175.043(5) 1_565 1_555 ?
O1 O3 O1O 105.076(4) 1_565 1_555 ?
O1 O3 Pb1 53.996(2) 1_565 2_566 ?
O1 O3 Pb2 109.562(4) 1_565 1_555 ?
O1 O3 Pb2 63.771(2) 1_565 2_556 ?
O1 O3 O4 117.857(3) 2_566 1_555 ?
O1 O3 O1O 102.070(4) 2_566 1_555 ?
O1 O3 Pb1 51.5049(20) 2_566 2_566 ?
O1 O3 Pb2 62.598(2) 2_566 1_555 ?
O1 O3 Pb2 104.508(3) 2_566 2_556 ?
O4 O3 O1O 71.955(2) 1_555 1_555 ?
O4 O3 Pb1 130.344(5) 1_555 2_566 ?
O4 O3 Pb2 71.619(2) 1_555 1_555 ?
O4 O3 Pb2 111.835(5) 1_555 2_556 ?
O1O O3 Pb1 149.632(5) 1_555 2_566 ?
O1O O3 Pb2 48.0816(18) 1_555 1_555 ?
O1O O3 Pb2 47.7020(20) 1_555 2_556 ?
Pb1 O3 Pb2 113.230(4) 2_566 1_555 ?
Pb1 O3 Pb2 117.767(4) 2_566 2_556 ?
Pb2 O3 Pb2 85.820(4) 1_555 2_556 ?
C3 O4 O2 141.186(5) 1_555 1_555 ?
C3 O4 O1O 87.135(3) 1_555 1_555 ?
C3 O4 Pb1 113.531(5) 1_555 2_556 ?
C3 O4 Pb2 90.245(4) 1_555 1_555 ?
C4 O4 O2 173.894(4) 1_555 1_555 ?
C4 O4 O3 62.3326(19) 1_555 1_555 ?
C4 O4 O1O 114.622(3) 1_555 1_555 ?
C4 O4 Pb1 119.533(4) 1_555 2_556 ?
C4 O4 Pb2 122.663(4) 1_555 1_555 ?
O2 O4 O3 112.350(4) 1_555 1_555 ?
O2 O4 O1O 59.388(2) 1_555 1_555 ?
O2 O4 Pb1 57.795(2) 1_555 2_556 ?
O2 O4 Pb2 52.7788(18) 1_555 1_555 ?
O3 O4 O1O 65.593(2) 1_555 1_555 ?
O3 O4 Pb1 105.314(4) 1_555 2_556 ?
O3 O4 Pb2 61.100(2) 1_555 1_555 ?
O1O O4 Pb1 45.7669(18) 1_555 2_556 ?
O1O O4 Pb2 45.2778(18) 1_555 1_555 ?
Pb1 O4 Pb2 84.035(2) 2_556 1_555 ?
C1 O5 C3 135.723(4) 2_556 2_556 ?
C1 O5 C5 114.288(4) 2_556 1_555 ?
C1 O5 C6 119.786(3) 2_556 1_555 ?
C1 O5 O6 104.583(3) 2_556 1_555 ?
C1 O5 O1O 67.324(2) 2_556 1_555 ?
C1 O5 Pb1 76.327(3) 2_556 1_555 ?
C1 O5 Pb2 73.850(2) 2_556 1_555 ?
C3 O5 C5 104.424(5) 2_556 1_555 ?
C3 O5 C6 104.213(4) 2_556 1_555 ?
C3 O5 O6 101.156(5) 2_556 1_555 ?
C3 O5 O1O 68.400(2) 2_556 1_555 ?
C3 O5 Pb1 74.826(3) 2_556 1_555 ?
C3 O5 Pb2 77.326(3) 2_556 1_555 ?
C5 O5 O1O 151.721(6) 1_555 1_555 ?
C5 O5 Pb1 158.980(6) 1_555 1_555 ?
C5 O5 Pb2 103.041(4) 1_555 1_555 ?
C6 O5 O6 60.0574(20) 1_555 1_555 ?
C6 O5 O1O 170.145(5) 1_555 1_555 ?
C6 O5 Pb1 124.619(4) 1_555 1_555 ?
C6 O5 Pb2 137.343(4) 1_555 1_555 ?
O6 O5 O1O 126.671(5) 1_555 1_555 ?
O6 O5 Pb1 174.244(5) 1_555 1_555 ?
O6 O5 Pb2 77.641(3) 1_555 1_555 ?
O1O O5 Pb1 48.2020(19) 1_555 1_555 ?
O1O O5 Pb2 49.1083(18) 1_555 1_555 ?
Pb1 O5 Pb2 97.309(3) 1_555 1_555 ?
C5 O6 Pb2 82.651(3) 1_555 1_555 ?
C6 O6 O5 62.629(2) 1_555 1_555 ?
C6 O6 Pb2 118.950(4) 1_555 1_555 ?
O5 O6 Pb2 56.5617(20) 1_555 1_555 ?
O1 O1O O1 67.692(3) 1_555 2_556 ?
O1 O1O O2 105.025(4) 1_555 1_555 ?
O1 O1O O3 132.327(5) 1_555 1_555 ?
O1 O1O O3 135.679(5) 1_555 2_556 ?
O1 O1O O4 114.150(4) 1_555 1_555 ?
O1 O1O O4 95.118(3) 1_555 2_556 ?
O1 O1O O5 115.192(4) 1_555 1_555 ?
O1 O1O O5 66.767(2) 1_555 2_556 ?
O1 O1O Pb1 58.3235(19) 1_555 1_555 ?
O1 O1O Pb1 59.888(2) 1_555 2_556 ?
O1 O1O Pb2 161.751(5) 1_555 1_555 ?
O1 O1O Pb2 94.540(4) 1_555 2_556 ?
O1 O1O O2 105.025(4) 2_556 2_556 ?
O1 O1O O3 135.679(5) 2_556 1_555 ?
O1 O1O O3 132.327(5) 2_556 2_556 ?
O1 O1O O4 95.118(3) 2_556 1_555 ?
O1 O1O O4 114.150(4) 2_556 2_556 ?
O1 O1O O5 66.767(2) 2_556 1_555 ?
O1 O1O O5 115.192(4) 2_556 2_556 ?
O1 O1O Pb1 59.888(2) 2_556 1_555 ?
O1 O1O Pb1 58.3235(19) 2_556 2_556 ?
O1 O1O Pb2 94.540(4) 2_556 1_555 ?
O1 O1O Pb2 161.751(5) 2_556 2_556 ?
O2 O1O O2 147.066(7) 1_555 2_556 ?
O2 O1O O3 94.162(3) 1_555 1_555 ?
O2 O1O O3 113.667(4) 1_555 2_556 ?
O2 O1O O4 60.060(2) 1_555 1_555 ?
O2 O1O O4 132.003(5) 1_555 2_556 ?
O2 O1O O5 66.179(3) 1_555 1_555 ?
O2 O1O O5 114.489(5) 1_555 2_556 ?
O2 O1O Pb1 97.337(4) 1_555 1_555 ?
O2 O1O Pb1 61.435(3) 1_555 2_556 ?
O2 O1O Pb2 56.938(2) 1_555 1_555 ?
O2 O1O Pb2 153.727(6) 1_555 2_556 ?
O2 O1O O3 113.667(4) 2_556 1_555 ?
O2 O1O O3 94.162(3) 2_556 2_556 ?
O2 O1O O4 132.003(5) 2_556 1_555 ?
O2 O1O O4 60.060(2) 2_556 2_556 ?
O2 O1O O5 114.489(5) 2_556 1_555 ?
O2 O1O O5 66.179(3) 2_556 2_556 ?
O2 O1O Pb1 61.435(3) 2_556 1_555 ?
O2 O1O Pb1 97.337(4) 2_556 2_556 ?
O2 O1O Pb2 153.727(6) 2_556 1_555 ?
O2 O1O Pb2 56.938(2) 2_556 2_556 ?
O3 O1O O3 66.541(2) 1_555 2_556 ?
O3 O1O O4 103.661(3) 1_555 2_556 ?
O3 O1O O5 112.478(3) 1_555 1_555 ?
O3 O1O O5 65.561(2) 1_555 2_556 ?
O3 O1O Pb1 161.100(4) 1_555 1_555 ?
O3 O1O Pb1 95.025(4) 1_555 2_556 ?
O3 O1O Pb2 58.046(2) 1_555 1_555 ?
O3 O1O Pb2 59.569(2) 1_555 2_556 ?
O3 O1O O4 103.661(3) 2_556 1_555 ?
O3 O1O O5 65.561(2) 2_556 1_555 ?
O3 O1O O5 112.478(3) 2_556 2_556 ?
O3 O1O Pb1 95.025(4) 2_556 1_555 ?
O3 O1O Pb1 161.100(4) 2_556 2_556 ?
O3 O1O Pb2 59.569(2) 2_556 1_555 ?
O3 O1O Pb2 58.046(2) 2_556 2_556 ?
O4 O1O O4 145.084(5) 1_555 2_556 ?
O4 O1O O5 113.470(4) 1_555 1_555 ?
O4 O1O O5 65.824(3) 1_555 2_556 ?
O4 O1O Pb1 154.998(5) 1_555 1_555 ?
O4 O1O Pb1 57.630(2) 1_555 2_556 ?
O4 O1O Pb2 61.430(2) 1_555 1_555 ?
O4 O1O Pb2 96.119(4) 1_555 2_556 ?
O4 O1O O5 65.824(3) 2_556 1_555 ?
O4 O1O O5 113.470(4) 2_556 2_556 ?
O4 O1O Pb1 57.630(2) 2_556 1_555 ?
O4 O1O Pb1 154.998(5) 2_556 2_556 ?
O4 O1O Pb2 96.119(4) 2_556 1_555 ?
O4 O1O Pb2 61.430(2) 2_556 2_556 ?
O5 O1O O5 177.849(6) 1_555 2_556 ?
O5 O1O Pb1 59.706(2) 1_555 1_555 ?
O5 O1O Pb1 121.847(4) 1_555 2_556 ?
O5 O1O Pb2 57.556(2) 1_555 1_555 ?
O5 O1O Pb2 120.879(5) 1_555 2_556 ?
O5 O1O Pb1 121.847(4) 2_556 1_555 ?
O5 O1O Pb1 59.706(2) 2_556 2_556 ?
O5 O1O Pb2 120.879(5) 2_556 1_555 ?
O5 O1O Pb2 57.556(2) 2_556 2_556 ?
Pb1 O1O Pb1 103.636(3) 1_555 2_556 ?
Pb1 O1O Pb2 117.261(4) 1_555 1_555 ?
Pb1 O1O Pb2 107.923(3) 1_555 2_556 ?
Pb1 O1O Pb2 107.923(3) 2_556 1_555 ?
Pb1 O1O Pb2 117.261(4) 2_556 2_556 ?
Pb2 O1O Pb2 103.456(5) 1_555 2_556 ?
C1 Pb1 O1 99.387(4) 1_555 2_556 ?
C1 Pb1 O3 84.748(3) 1_555 2_546 ?
C1 Pb1 O4 91.038(3) 1_555 2_556 ?
C1 Pb1 O5 143.729(5) 1_555 1_555 ?
C1 Pb1 O1O 72.038(3) 1_555 1_555 ?
O1 Pb1 O1 76.761(3) 1_555 2_556 ?
O1 Pb1 O2 47.916(2) 1_555 2_556 ?
O1 Pb1 O3 66.322(2) 1_555 2_546 ?
O1 Pb1 O4 114.571(3) 1_555 2_556 ?
O1 Pb1 O5 140.498(4) 1_555 1_555 ?
O1 Pb1 O1O 73.661(2) 1_555 1_555 ?
O1 Pb1 O2 120.788(5) 2_556 2_556 ?
O1 Pb1 O3 62.662(2) 2_556 2_546 ?
O1 Pb1 O4 142.262(4) 2_556 2_556 ?
O1 Pb1 O5 74.674(2) 2_556 1_555 ?
O1 Pb1 O1O 72.489(2) 2_556 1_555 ?
O2 Pb1 O3 103.298(3) 2_556 2_546 ?
O2 Pb1 O4 68.136(2) 2_556 2_556 ?
O2 Pb1 O5 134.244(6) 2_556 1_555 ?
O2 Pb1 O1O 73.085(3) 2_556 1_555 ?
O3 Pb1 O4 154.964(6) 2_546 2_556 ?
O3 Pb1 O5 120.766(4) 2_546 1_555 ?
O3 Pb1 O1O 124.755(5) 2_546 1_555 ?
O4 Pb1 O5 75.625(3) 2_556 1_555 ?
O4 Pb1 O1O 76.604(2) 2_556 1_555 ?
O5 Pb1 O1O 72.092(2) 1_555 1_555 ?
C5 Pb2 O1 104.371(3) 1_555 2_566 ?
C5 Pb2 O2 84.873(2) 1_555 1_555 ?
C5 Pb2 O3 154.776(4) 1_555 1_555 ?
C5 Pb2 O3 79.129(3) 1_555 2_556 ?
C5 Pb2 O4 152.737(5) 1_555 1_555 ?
C5 Pb2 O1O 96.228(3) 1_555 1_555 ?
O1 Pb2 O2 154.620(6) 2_566 1_555 ?
O1 Pb2 O3 65.905(2) 2_566 1_555 ?
O1 Pb2 O3 62.291(2) 2_566 2_556 ?
O1 Pb2 O4 102.154(3) 2_566 1_555 ?
O1 Pb2 O5 119.392(4) 2_566 1_555 ?
O1 Pb2 O6 89.466(3) 2_566 1_555 ?
O1 Pb2 O1O 124.914(5) 2_566 1_555 ?
O2 Pb2 O3 114.085(4) 1_555 1_555 ?
O2 Pb2 O3 143.071(4) 1_555 2_556 ?
O2 Pb2 O4 68.321(2) 1_555 1_555 ?
O2 Pb2 O5 77.616(2) 1_555 1_555 ?
O2 Pb2 O6 91.111(3) 1_555 1_555 ?
O2 Pb2 O1O 76.252(3) 1_555 1_555 ?
O3 Pb2 O3 75.788(3) 1_555 2_556 ?
O3 Pb2 O4 47.2811(18) 1_555 1_555 ?
O3 Pb2 O5 140.956(4) 1_555 1_555 ?
O3 Pb2 O6 154.393(5) 1_555 1_555 ?
O3 Pb2 O1O 73.873(2) 1_555 1_555 ?
O3 Pb2 O4 119.503(4) 2_556 1_555 ?
O3 Pb2 O5 74.713(2) 2_556 1_555 ?
O3 Pb2 O6 86.854(4) 2_556 1_555 ?
O3 Pb2 O1O 72.729(2) 2_556 1_555 ?
O4 Pb2 O5 136.741(4) 1_555 1_555 ?
O4 Pb2 O6 153.641(5) 1_555 1_555 ?
O4 Pb2 O1O 73.292(2) 1_555 1_555 ?
O5 Pb2 O6 45.7977(17) 1_555 1_555 ?
O5 Pb2 O1O 73.336(2) 1_555 1_555 ?
O6 Pb2 O1O 119.067(4) 1_555 1_555 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.47712(4) 1_555 ?
C1 O1 1.29007(3) 1_555 ?
C1 O2 1.23440(2) 2_556 ?
C1 O5 2.90593(5) 2_556 ?
C1 Pb1 3.08827(8) 1_555 ?
C2 C1 1.47712(4) 1_555 ?
C2 O1 2.38535(7) 1_555 ?
C2 O2 2.33348(4) 2_556 ?
C3 C4 1.47613(3) 1_555 ?
C3 O3 1.25937(2) 1_555 ?
C3 O4 1.25864(3) 1_555 ?
C3 O5 2.93009(6) 2_556 ?
C4 C3 1.47613(3) 1_555 ?
C4 O3 2.36128(5) 1_555 ?
C4 O4 2.35760(4) 1_555 ?
C5 C6 1.48058(3) 1_555 ?
C5 O5 1.23839(3) 1_555 ?
C5 O6 1.20879(2) 1_555 ?
C5 Pb2 3.08832(6) 1_555 ?
C6 C5 1.48058(3) 1_555 ?
C6 O5 2.32367(5) 1_555 ?
C6 O6 2.26735(4) 1_555 ?
O1 C1 1.29007(3) 1_555 ?
O1 C2 2.38535(7) 1_555 ?
O1 O2 2.20774(4) 2_556 ?
O1 O3 2.93161(6) 1_545 ?
O1 O3 3.05427(5) 2_546 ?
O1 O1O 2.94325(6) 1_555 ?
O1 Pb1 2.61021(5) 1_555 ?
O1 Pb1 2.66978(7) 2_556 ?
O1 Pb2 2.97040(8) 2_546 ?
O2 C1 1.23440(2) 2_556 ?
O2 C2 2.33348(4) 2_556 ?
O2 O1 2.20774(4) 2_556 ?
O2 O4 3.08025(5) 1_555 ?
O2 O1O 3.05924(9) 1_555 ?
O2 Pb1 2.80835(8) 2_556 ?
O2 Pb2 2.63951(6) 1_555 ?
O3 C3 1.25937(2) 1_555 ?
O3 C4 2.36128(5) 1_555 ?
O3 O1 2.93161(6) 1_565 ?
O3 O1 3.05427(5) 2_566 ?
O3 O4 2.19735(4) 1_555 ?
O3 O1O 2.96454(6) 1_555 ?
O3 Pb1 2.94939(8) 2_566 ?
O3 Pb2 2.61837(5) 1_555 ?
O3 Pb2 2.67685(7) 2_556 ?
O4 C3 1.25864(3) 1_555 ?
O4 C4 2.35760(4) 1_555 ?
O4 O2 3.08025(5) 1_555 ?
O4 O3 2.19735(4) 1_555 ?
O4 O1O 3.09536(7) 1_555 ?
O4 Pb1 2.68748(6) 2_556 ?
O4 Pb2 2.83826(5) 1_555 ?
O5 C1 2.90593(5) 2_556 ?
O5 C3 2.93009(6) 2_556 ?
O5 C5 1.23839(3) 1_555 ?
O5 C6 2.32367(5) 1_555 ?
O5 O6 2.20223(5) 1_555 ?
O5 O1O 2.91003(7) 1_555 ?
O5 Pb1 2.64059(6) 1_555 ?
O5 Pb2 2.56349(4) 1_555 ?
O6 C5 1.20879(2) 1_555 ?
O6 C6 2.26735(4) 1_555 ?
O6 O5 2.20223(5) 1_555 ?
O6 Pb2 3.00076(7) 1_555 ?
O1O O1 2.94325(6) 1_555 ?
O1O O1 2.94325(6) 2_556 ?
O1O O2 3.05924(9) 1_555 ?
O1O O2 3.05924(9) 2_556 ?
O1O O3 2.96454(6) 1_555 ?
O1O O3 2.96454(6) 2_556 ?
O1O O4 3.09536(7) 1_555 ?
O1O O4 3.09536(7) 2_556 ?
O1O O5 2.91003(7) 1_555 ?
O1O O5 2.91003(7) 2_556 ?
O1O Pb1 2.27988(4) 1_555 ?
O1O Pb1 2.27988(4) 2_556 ?
O1O Pb2 2.29627(5) 1_555 ?
O1O Pb2 2.29627(5) 2_556 ?
Pb1 C1 3.08827(8) 1_555 ?
Pb1 O1 2.61021(5) 1_555 ?
Pb1 O1 2.66978(7) 2_556 ?
Pb1 O2 2.80835(8) 2_556 ?
Pb1 O3 2.94939(8) 2_546 ?
Pb1 O4 2.68748(6) 2_556 ?
Pb1 O5 2.64059(6) 1_555 ?
Pb1 O1O 2.27988(4) 1_555 ?
Pb2 C5 3.08832(6) 1_555 ?
Pb2 O1 2.97040(8) 2_566 ?
Pb2 O2 2.63951(6) 1_555 ?
Pb2 O3 2.61837(5) 1_555 ?
Pb2 O3 2.67685(7) 2_556 ?
Pb2 O4 2.83826(5) 1_555 ?
Pb2 O5 2.56349(4) 1_555 ?
Pb2 O6 3.00076(7) 1_555 ?
Pb2 O1O 2.29627(5) 1_555 ?

_cod_database_fobs_code 4300009
