#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:05:32 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1184 $
#$URL: svn://crystallography.net/testcod/cif/4/30/00/4300010.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4300010
loop_
_publ_author_name
'Martínez-Casado, Francisco J.'
'Ramos-Riesco, Miguel'
'Rodríguez-Cheda, José A.'
'Cucinotta, Fabio'
'Matesanz, Emilio'
'Miletto, Ivana'
'Gianotti, Enrica'
'Marchese, Leonardo'
'Matěj, Zdeněk'
_publ_section_title
;
 Unraveling the Decomposition Process of Lead(II) Acetate: Anhydrous
 Polymorphs, Hydrates, and Byproducts and Room Temperature Phosphorescence
;
_journal_issue                   17
_journal_name_full               'Inorganic Chemistry'
_journal_page_first              8576
_journal_page_last               8586
_journal_paper_doi               10.1021/acs.inorgchem.6b01116
_journal_volume                  55
_journal_year                    2016
_chemical_formula_moiety         'C40 H60 O40 Pb10'
_chemical_formula_sum            'C40 H60 O40 Pb10'
_chemical_formula_weight         3252.78
_chemical_name_common            'Lead(II) acetate polymorph alpha'
_chemical_name_systematic
catena-poly[[(acetato-O,O')lead(II)]-μ-acetato-O,O':O]_polymorph-alpha
_space_group_IT_number           4
_space_group_name_Hall           'P 2yb'
_space_group_name_H-M_alt        'P 1 21 1'
_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 99.0918(6)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            2
_cell_length_a                   12.5687(2)
_cell_length_b                   7.08687(12)
_cell_length_c                   38.0318(6)
_cell_measurement_reflns_used    12313
_cell_measurement_temperature    285
_cell_measurement_theta_max      90.0
_cell_measurement_theta_min      0.5
_cell_volume                     3345.04(9)
_computing_structure_refinement  FULLPROF
_diffrn_ambient_temperature      285
_diffrn_detector                 'area detector'
_diffrn_detector_area_resol_mean 5.81
_diffrn_detector_type            'Pilatus 100K'
_diffrn_measurement_device_type  'Beamline I711/MAX IV Laboratory'
_diffrn_measurement_method       '2θ scan'
_diffrn_radiation_monochromator  Si(111)
_diffrn_radiation_wavelength     0.9938
_diffrn_source                   Synchrotron
_exptl_absorpt_coefficient_mu    8.01
_exptl_absorpt_correction_type   cylinder
_exptl_absorpt_process_details   muR=2.00
_exptl_crystal_density_diffrn    3.230
_pd_block_diffractogram_id       Pb(Ac)2_polymorph_alpha_1
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.016517
_pd_meas_2theta_range_max        93.98348
_pd_meas_2theta_range_min        0.01652
_pd_meas_number_of_points        5690
_pd_meas_scan_method             cont
_pd_proc_2theta_range_inc        0.016517
_pd_proc_2theta_range_max        93.9600
_pd_proc_2theta_range_min        -0.0070
_pd_proc_ls_background_function  'Interpolation of points'
_pd_proc_ls_pref_orient_corr     ' ?'
_pd_proc_ls_profile_function     Pseudo-Voigt
_pd_proc_ls_prof_R_factor        4.2475
_pd_proc_ls_prof_wR_expected     8.4937
_pd_proc_ls_prof_wR_factor       6.8142
_pd_proc_wavelength              0.993800
_pd_spec_mounting                'borosilicate capillary'
_pd_spec_mount_mode              transmission
_pd_spec_shape                   cylinder
_refine_ls_goodness_of_fit_all   0.80
_refine_ls_number_parameters     89
_refine_ls_number_reflns         12313
_refine_ls_number_restraints     0
_refine_ls_R_I_factor            5.5029
_cod_data_source_file            ic6b01116_si_003.cif
_cod_data_source_block           PbAc2_polymorph_alpha
_cod_original_cell_volume        3345.03(10)
_cod_database_code               4300010
_pd_proc_ls_prof_cr_factor       12.5311
_pd_proc_ls_prof_cwr_factor      14.8074
_pd_proc_ls_prof_cwr_expected    18.4571
_pd_proc_ls_prof_chi2            0.6436
_pd_proc_ls_prof_echi2           0.6479
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,y+1/2,-z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_type_symbol
C1 0.38500 0.42800 0.97060 0.05557 1.00000 Uani C
C2 0.44040 0.41500 1.00860 0.06371 1.00000 Uani C
H2A 0.38760 0.42070 1.02420 0.09200 1.00000 Uiso H
H2B 0.48960 0.51820 1.01370 0.09200 1.00000 Uiso H
H2C 0.47890 0.29870 1.01210 0.09200 1.00000 Uiso H
C3 0.04270 0.47400 0.90560 0.04968 1.00000 Uani C
C4 -0.08170 0.49500 0.90090 0.06713 1.00000 Uani C
H4A -0.09980 0.61610 0.90920 0.10300 1.00000 Uiso H
H4B -0.11070 0.39860 0.91430 0.10300 1.00000 Uiso H
H4C -0.11120 0.48200 0.87630 0.10300 1.00000 Uiso H
C5 0.18140 0.48800 1.07060 0.04562 1.00000 Uani C
C6 0.22900 0.50000 1.10890 0.08995 1.00000 Uani C
H6A 0.30540 0.50080 1.11120 0.14100 1.00000 Uiso H
H6B 0.20580 0.39360 1.12120 0.14100 1.00000 Uiso H
H6C 0.20470 0.61360 1.11880 0.14100 1.00000 Uiso H
C7 0.44590 0.33600 0.69290 0.05224 1.00000 Uani C
C8 0.32750 0.34300 0.69310 0.09815 1.00000 Uani C
H8A 0.30470 0.47190 0.69350 0.14800 1.00000 Uiso H
H8B 0.31110 0.27980 0.71380 0.14800 1.00000 Uiso H
H8C 0.29080 0.28250 0.67230 0.14800 1.00000 Uiso H
C9 -0.05840 0.32100 1.16190 0.05224 1.00000 Uani C
C10 0.01200 0.26400 1.19550 0.09232 1.00000 Uani C
H10A 0.08140 0.31930 1.19630 0.13700 1.00000 Uiso H
H10B 0.01820 0.12960 1.19620 0.13700 1.00000 Uiso H
H10C -0.01970 0.30640 1.21540 0.13700 1.00000 Uiso H
C11 -0.33840 0.48400 1.09530 0.03991 1.00000 Uani C
C12 -0.45360 0.50400 1.10410 0.07217 1.00000 Uani C
H12A -0.49290 0.39000 1.09790 0.10500 1.00000 Uiso H
H12B -0.48920 0.60670 1.09080 0.10500 1.00000 Uiso H
H12C -0.45020 0.52780 1.12900 0.10500 1.00000 Uiso H
C13 0.15200 -0.05000 1.00610 0.05888 1.00000 Uani C
C14 0.27050 -0.06900 1.00730 0.05888 1.00000 Uani C
H14A 0.30140 0.05340 1.00560 0.08800 1.00000 Uiso H
H14B 0.28460 -0.14560 0.98790 0.08800 1.00000 Uiso H
H14C 0.30150 -0.12640 1.02930 0.08800 1.00000 Uiso H
C15 0.54200 0.44400 0.86230 0.05784 1.00000 Uani C
C16 0.60530 0.50200 0.89600 0.07812 1.00000 Uani C
H16A 0.56530 0.59220 0.90740 0.11600 1.00000 Uiso H
H16B 0.67150 0.55730 0.89180 0.11600 1.00000 Uiso H
H16C 0.62030 0.39400 0.91110 0.11600 1.00000 Uiso H
C17 0.55300 0.80100 0.79450 0.05847 1.00000 Uani C
C18 0.66840 0.78100 0.79650 0.05847 1.00000 Uani C
H18A 0.70350 0.89030 0.80760 0.08700 1.00000 Uiso H
H18B 0.68580 0.76820 0.77300 0.08700 1.00000 Uiso H
H18C 0.69220 0.67140 0.81020 0.08700 1.00000 Uiso H
C19 0.21550 0.86600 0.73080 0.06676 1.00000 Uani C
C20 0.16590 0.88900 0.69330 0.09390 1.00000 Uani C
H20A 0.22110 0.90110 0.67880 0.14500 1.00000 Uiso H
H20B 0.12150 0.99890 0.69090 0.14500 1.00000 Uiso H
H20C 0.12280 0.78020 0.68590 0.14500 1.00000 Uiso H
C21 0.25790 0.29700 0.79950 0.04993 1.00000 Uani C
C22 0.14780 0.27600 0.80710 0.06037 1.00000 Uani C
H22A 0.11000 0.39230 0.80250 0.08800 1.00000 Uiso H
H22B 0.15000 0.24200 0.83160 0.08800 1.00000 Uiso H
H22C 0.11160 0.17890 0.79230 0.08800 1.00000 Uiso H
C23 0.77560 0.29000 0.76940 0.05495 1.00000 Uani C
C24 0.81600 0.27900 0.80830 0.07548 1.00000 Uani C
H24A 0.75680 0.28720 0.82120 0.11000 1.00000 Uiso H
H24B 0.86470 0.38160 0.81510 0.11000 1.00000 Uiso H
H24C 0.85300 0.16220 0.81370 0.11000 1.00000 Uiso H
C25 0.98670 0.37800 0.67330 0.05925 1.00000 Uani C
C26 1.03910 0.38600 0.71100 0.08894 1.00000 Uani C
H26A 0.98510 0.38630 0.72610 0.13600 1.00000 Uiso H
H26B 1.08140 0.49810 0.71490 0.13600 1.00000 Uiso H
H26C 1.08450 0.27790 0.71630 0.13600 1.00000 Uiso H
C27 0.74840 0.83800 0.70320 0.06594 1.00000 Uani C
C28 0.86700 0.83200 0.70630 0.11489 1.00000 Uani C
H28A 0.89410 0.95630 0.70400 0.17400 1.00000 Uiso H
H28B 0.88680 0.75310 0.68790 0.17400 1.00000 Uiso H
H28C 0.89700 0.78110 0.72900 0.17400 1.00000 Uiso H
C29 0.41090 0.82200 0.62610 0.06057 1.00000 Uani C
C30 0.37060 0.81000 0.58790 0.08165 1.00000 Uani C
H30A 0.42980 0.81730 0.57490 0.12100 1.00000 Uiso H
H30B 0.32200 0.91210 0.58110 0.12100 1.00000 Uiso H
H30C 0.33370 0.69270 0.58280 0.12100 1.00000 Uiso H
C31 0.63130 0.34900 0.60200 0.04764 1.00000 Uani C
C32 0.51840 0.33600 0.59830 0.07383 1.00000 Uani C
H32A 0.48670 0.44920 0.58770 0.11300 1.00000 Uiso H
H32B 0.49750 0.31890 0.62120 0.11300 1.00000 Uiso H
H32C 0.49420 0.23060 0.58340 0.11300 1.00000 Uiso H
C33 0.64100 0.96900 0.53540 0.07510 1.00000 Uani C
C34 0.59140 1.03000 0.49840 0.07383 1.00000 Uani C
H34A 0.64660 1.07680 0.48600 0.11300 1.00000 Uiso H
H34B 0.53970 1.12750 0.49990 0.11300 1.00000 Uiso H
H34C 0.55650 0.92470 0.48570 0.11300 1.00000 Uiso H
C35 0.94570 0.84300 0.60620 0.05392 1.00000 Uani C
C36 1.05820 0.81300 0.60170 0.07173 1.00000 Uani C
H36A 1.06630 0.68860 0.59280 0.10400 1.00000 Uiso H
H36B 1.10390 0.82790 0.62410 0.10400 1.00000 Uiso H
H36C 1.07780 0.90350 0.58510 0.10400 1.00000 Uiso H
C37 0.85900 0.85500 0.43570 0.08757 1.00000 Uani C
C38 0.78300 0.80700 0.40130 0.08189 1.00000 Uani C
H38A 0.82160 0.73740 0.38580 0.11800 1.00000 Uiso H
H38B 0.75620 0.92150 0.38970 0.11800 1.00000 Uiso H
H38C 0.72410 0.73330 0.40670 0.11800 1.00000 Uiso H
C39 1.15180 1.00500 0.49610 0.06177 1.00000 Uani C
C40 1.26710 1.03500 0.49270 0.09213 1.00000 Uani C
H40A 1.27570 1.15710 0.48300 0.13900 1.00000 Uiso H
H40B 1.28920 0.94060 0.47740 0.13900 1.00000 Uiso H
H40C 1.31030 1.02540 0.51570 0.13900 1.00000 Uiso H
O1 0.43990 0.42900 0.94650 0.09028 1.00000 Uani O
O2 0.28380 0.43500 0.96460 0.07351 1.00000 Uani O
O3 0.07540 0.32100 0.89470 0.07824 1.00000 Uani O
O4 0.09390 0.60600 0.91640 0.04635 1.00000 Uani O
O5 0.24560 0.49300 1.04950 0.08357 1.00000 Uani O
O6 0.08050 0.48500 1.06080 0.06204 1.00000 Uani O
O7 0.50520 0.48500 0.69470 0.06905 1.00000 Uani O
O8 0.48580 0.18800 0.68790 0.07605 1.00000 Uani O
O9 -0.01090 0.42500 1.14150 0.10008 1.00000 Uani O
O10 -0.15060 0.27200 1.15550 0.06905 1.00000 Uani O
O11 -0.31070 0.32500 1.08360 0.07605 1.00000 Uani O
O12 -0.27930 0.61100 1.09880 0.05692 1.00000 Uani O
O13 0.09840 -0.18000 1.00520 0.12158 1.00000 Uani O
O14 0.10640 0.10800 1.00450 0.09117 1.00000 Uani O
O15 0.44460 0.49900 0.85630 0.09117 1.00000 Uani O
O16 0.58690 0.34700 0.84120 0.10675 1.00000 Uani O
O17 0.51480 0.94500 0.80120 0.06465 1.00000 Uani O
O18 0.49220 0.65900 0.78230 0.06465 1.00000 Uani O
O19 0.16380 0.85400 0.75480 0.07561 1.00000 Uani O
O20 0.31570 0.84600 0.73670 0.07923 1.00000 Uani O
O21 0.28990 0.44200 0.78520 0.06404 1.00000 Uani O
O22 0.32240 0.15900 0.80710 0.06960 1.00000 Uani O
O23 0.67900 0.29400 0.75970 0.07235 1.00000 Uani O
O24 0.83940 0.29800 0.74810 0.09655 1.00000 Uani O
O25 0.88400 0.35700 0.66510 0.07691 1.00000 Uani O
O26 1.04190 0.38500 0.64890 0.06960 1.00000 Uani O
O27 0.70890 0.68700 0.70940 0.07691 1.00000 Uani O
O28 0.69260 0.97600 0.69510 0.05770 1.00000 Uani O
O29 0.35440 0.81400 0.64920 0.09643 1.00000 Uani O
O30 0.51300 0.83100 0.63760 0.06716 1.00000 Uani O
O31 0.68570 0.49000 0.59910 0.08752 1.00000 Uani O
O32 0.69210 0.21400 0.61340 0.08752 1.00000 Uani O
O33 0.73690 0.99900 0.54490 0.09849 1.00000 Uani O
O34 0.58360 0.90300 0.55430 0.08357 1.00000 Uani O
O35 0.90480 0.98800 0.61380 0.08357 1.00000 Uani O
O36 0.88060 0.70100 0.60030 0.09849 1.00000 Uani O
O37 0.80780 0.93600 0.45850 0.10310 1.00000 Uani O
O38 0.95250 0.80100 0.44040 0.10310 1.00000 Uani O
O39 1.08570 1.12700 0.48750 0.06049 1.00000 Uani O
O40 1.12090 0.84800 0.50950 0.06819 1.00000 Uani O
Pb01 0.28103 0.48098 0.90003 0.04875 1.00000 Uani Pb
Pb02 0.10168 0.46647 0.99760 0.04737 1.00000 Uani Pb
Pb03 -0.10645 0.47095 1.08690 0.05688 1.00000 Uani Pb
Pb04 0.49717 0.83318 0.70014 0.04886 1.00000 Uani Pb
Pb05 0.48872 0.30205 0.78612 0.05726 1.00000 Uani Pb
Pb06 0.31902 0.79624 0.80116 0.05259 1.00000 Uani Pb
PbO7 0.69874 0.32998 0.69527 0.04748 1.00000 Uani Pb
Pb08 0.88411 0.34133 0.60147 0.05369 1.00000 Uani Pb
Pb09 0.69711 0.85746 0.60918 0.05987 1.00000 Uani Pb
Pb10 0.92193 0.99835 0.51014 0.06298 1.00000 Uani Pb
loop_
_atom_type_symbol
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
c 2.31000 20.84390 1.02000 10.20750 1.58860 0.56870 0.86500 51.65120 0.21560
0.00200 0.00200
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
h 0.49300 10.51090 0.32291 26.12570 0.14019 3.14236 0.04081 57.79970 0.00304
0.00000 0.00000
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
o 3.04850 13.27710 2.28680 5.70110 1.54630 0.32390 0.86700 32.90890 0.25080
0.00800 0.00600
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
pb 31.06170 0.69020 13.06370 2.35760 18.44200 8.61800 5.96960 47.25790 13.41180
-8.48100 4.23100
International_Tables_for_Crystallography_Vol.C(1991)_Tables_6.1.1.4_and_6.1.1.5
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C2 C1 O1 119.118(3) 1_555 1_555 ?
C2 C1 O2 118.562(2) 1_555 1_555 ?
C2 C1 Pb01 175.847(4) 1_555 1_555 ?
O1 C1 O2 122.313(3) 1_555 1_555 ?
O1 C1 Pb01 61.3422(16) 1_555 1_555 ?
O2 C1 Pb01 61.2076(19) 1_555 1_555 ?
O1 C2 O2 54.7512(13) 1_555 1_555 ?
C4 C3 O3 114.950(2) 1_555 1_555 ?
C4 C3 O4 116.802(3) 1_555 1_555 ?
C4 C3 Pb01 167.690(4) 1_555 1_555 ?
O3 C3 O4 128.009(3) 1_555 1_555 ?
O3 C3 Pb01 67.1883(19) 1_555 1_555 ?
O4 C3 Pb01 61.2178(18) 1_555 1_555 ?
O3 C4 O4 55.2635(12) 1_555 1_555 ?
C6 C5 O5 115.802(3) 1_555 1_555 ?
C6 C5 O6 121.285(3) 1_555 1_555 ?
C6 C5 Pb02 177.256(4) 1_555 1_555 ?
O5 C5 O6 122.766(3) 1_555 1_555 ?
O5 C5 Pb02 61.4534(17) 1_555 1_555 ?
O6 C5 Pb02 61.4530(19) 1_555 1_555 ?
O5 C6 O6 55.3381(13) 1_555 1_555 ?
C8 C7 O7 122.845(3) 1_555 1_555 ?
C8 C7 O8 118.441(2) 1_555 1_555 ?
O7 C7 O8 118.414(3) 1_555 1_555 ?
O7 C8 O8 53.1921(12) 1_555 1_555 ?
C10 C9 O9 113.827(2) 1_555 1_555 ?
C10 C9 O10 121.336(3) 1_555 1_555 ?
C10 C9 Pb03 155.485(4) 1_555 1_555 ?
O9 C9 O10 124.837(2) 1_555 1_555 ?
O10 C9 Pb03 82.364(2) 1_555 1_555 ?
O9 C10 O10 56.1301(12) 1_555 1_555 ?
C12 C11 O11 118.188(2) 1_555 1_555 ?
C12 C11 O12 120.601(3) 1_555 1_555 ?
C12 C11 Pb03 172.766(4) 1_555 1_555 ?
O11 C11 O12 121.203(3) 1_555 1_555 ?
O11 C11 Pb03 67.1344(19) 1_555 1_555 ?
O12 C11 Pb03 54.4211(16) 1_555 1_555 ?
O11 C12 O12 52.7981(12) 1_555 1_555 ?
C14 C13 O13 120.794(3) 1_555 1_555 ?
C14 C13 O14 121.946(2) 1_555 1_555 ?
O13 C13 O14 117.191(3) 1_555 1_555 ?
O13 C14 O14 51.5688(12) 1_555 1_555 ?
C16 C15 O15 116.627(2) 1_555 1_555 ?
C16 C15 O16 118.580(2) 1_555 1_555 ?
C16 C15 Pb05 159.929(4) 1_555 1_555 ?
O15 C15 O16 124.784(2) 1_555 1_555 ?
O15 C15 Pb05 82.499(2) 1_555 1_555 ?
C15 C16 O1 99.912(2) 1_555 1_555 ?
O1 C16 O15 78.5279(18) 1_555 1_555 ?
O1 C16 O16 119.656(3) 1_555 1_555 ?
O15 C16 O16 57.4650(12) 1_555 1_555 ?
C18 C17 O17 121.000(2) 1_555 1_555 ?
C18 C17 O18 117.986(2) 1_555 1_555 ?
C18 C17 Pb06 170.015(4) 1_555 1_555 ?
O17 C17 O18 120.789(3) 1_555 1_555 ?
O17 C17 Pb06 63.2408(19) 1_555 1_555 ?
O18 C17 Pb06 59.5150(16) 1_555 1_555 ?
O17 C18 O18 55.2525(12) 1_555 1_555 ?
C20 C19 O19 123.052(3) 1_555 1_555 ?
C20 C19 O20 116.493(2) 1_555 1_555 ?
C20 C19 Pb06 175.481(4) 1_555 1_555 ?
O19 C19 O20 120.279(3) 1_555 1_555 ?
O19 C19 Pb06 59.5431(16) 1_555 1_555 ?
O20 C19 Pb06 60.7387(19) 1_555 1_555 ?
O19 C20 O20 54.1944(13) 1_555 1_555 ?
C22 C21 O21 123.001(2) 1_555 1_555 ?
C22 C21 O22 117.658(2) 1_555 1_555 ?
C22 C21 Pb05 174.569(4) 1_555 1_555 ?
O21 C21 O22 119.319(2) 1_555 1_555 ?
O21 C21 Pb05 62.4063(18) 1_555 1_555 ?
O22 C21 Pb05 56.9236(15) 1_555 1_555 ?
O21 C22 O22 54.8794(12) 1_555 1_555 ?
C24 C23 O23 118.145(2) 1_555 1_555 ?
C24 C23 O24 120.159(3) 1_555 1_555 ?
C24 C23 PbO7 177.289(4) 1_555 1_555 ?
O23 C23 O24 121.684(3) 1_555 1_555 ?
O23 C23 PbO7 61.925(2) 1_555 1_555 ?
O24 C23 PbO7 59.7842(17) 1_555 1_555 ?
O23 C24 O24 54.1800(13) 1_555 1_555 ?
C26 C25 O25 120.941(2) 1_555 1_555 ?
C26 C25 O26 120.351(3) 1_555 1_555 ?
C26 C25 Pb08 176.876(4) 1_555 1_555 ?
O25 C25 O26 118.663(3) 1_555 1_555 ?
O25 C25 Pb08 58.1013(19) 1_555 1_555 ?
O26 C25 Pb08 60.5694(16) 1_555 1_555 ?
O25 C26 O26 54.2196(13) 1_555 1_555 ?
C28 C27 O27 113.341(2) 1_555 1_555 ?
C28 C27 O28 125.340(3) 1_555 1_555 ?
O27 C27 O28 121.317(3) 1_555 1_555 ?
O27 C28 O28 54.1565(12) 1_555 1_555 ?
C30 C29 O29 124.394(3) 1_555 1_555 ?
C30 C29 O30 120.600(2) 1_555 1_555 ?
C30 C29 Pb04 177.333(4) 1_555 1_555 ?
O29 C29 O30 114.885(3) 1_555 1_555 ?
O29 C29 Pb04 57.4726(16) 1_555 1_555 ?
O30 C29 Pb04 57.4355(19) 1_555 1_555 ?
O29 C30 O30 52.6096(13) 1_555 1_555 ?
C32 C31 O31 127.786(3) 1_555 1_555 ?
C32 C31 O32 122.202(3) 1_555 1_555 ?
O31 C31 O32 109.508(2) 1_555 1_555 ?
O31 C32 O32 51.1408(12) 1_555 1_555 ?
C34 C33 O33 117.966(2) 1_555 1_555 ?
C34 C33 O34 118.331(3) 1_555 1_555 ?
C34 C33 Pb09 169.698(4) 1_555 1_555 ?
O33 C33 O34 123.594(3) 1_555 1_555 ?
O33 C33 Pb09 71.4971(20) 1_555 1_555 ?
O34 C33 Pb09 52.0998(16) 1_555 1_555 ?
O33 C34 O34 54.1691(12) 1_555 1_555 ?
C36 C35 O35 127.422(2) 1_555 1_555 ?
C36 C35 O36 117.513(3) 1_555 1_555 ?
O35 C35 O36 115.021(3) 1_555 1_555 ?
O35 C36 O36 52.5758(12) 1_555 1_555 ?
C38 C37 O37 111.236(2) 1_555 1_555 ?
C38 C37 O38 120.737(3) 1_555 1_555 ?
C38 C37 Pb10 156.800(3) 1_555 1_555 ?
O37 C37 O38 127.590(2) 1_555 1_555 ?
O37 C37 Pb10 45.6032(14) 1_555 1_555 ?
O38 C37 Pb10 82.165(2) 1_555 1_555 ?
O37 C38 O38 56.9359(12) 1_555 1_555 ?
C40 C39 O39 120.733(3) 1_555 1_555 ?
C40 C39 O40 120.515(2) 1_555 1_555 ?
C40 C39 Pb10 171.106(4) 1_555 1_555 ?
O39 C39 O40 118.719(2) 1_555 1_555 ?
O39 C39 Pb10 54.7451(15) 1_555 1_555 ?
O40 C39 Pb10 64.3198(18) 1_555 1_555 ?
O39 C40 O40 53.8256(12) 1_555 1_555 ?
C1 O1 C16 167.225(3) 1_555 1_555 ?
C1 O1 Pb01 92.786(2) 1_555 1_555 ?
C2 O1 C16 137.124(3) 1_555 1_555 ?
C2 O1 O2 62.9706(14) 1_555 1_555 ?
C2 O1 Pb01 126.452(3) 1_555 1_555 ?
C16 O1 O2 157.058(3) 1_555 1_555 ?
C16 O1 Pb01 94.436(2) 1_555 1_555 ?
O2 O1 Pb01 63.7654(15) 1_555 1_555 ?
C1 O2 O4 143.598(3) 1_555 1_555 ?
C1 O2 Pb01 92.324(2) 1_555 1_555 ?
C1 O2 Pb02 143.180(4) 1_555 1_555 ?
C2 O2 O1 62.2782(14) 1_555 1_555 ?
C2 O2 O4 159.537(3) 1_555 1_555 ?
C2 O2 Pb01 125.955(3) 1_555 1_555 ?
C2 O2 Pb02 109.583(3) 1_555 1_555 ?
O1 O2 O4 118.685(3) 1_555 1_555 ?
O1 O2 Pb01 63.9577(14) 1_555 1_555 ?
O1 O2 Pb02 171.003(3) 1_555 1_555 ?
O4 O2 Pb01 57.2524(13) 1_555 1_555 ?
O4 O2 Pb02 67.3727(14) 1_555 1_555 ?
Pb01 O2 Pb02 123.572(3) 1_555 1_555 ?
C3 O3 O12 137.502(3) 1_555 2_547 ?
C3 O3 Pb01 88.448(2) 1_555 1_555 ?
C3 O3 Pb03 141.498(4) 1_555 2_547 ?
C4 O3 O4 61.3981(13) 1_555 1_555 ?
C4 O3 O12 169.556(3) 1_555 2_547 ?
C4 O3 Pb01 123.768(3) 1_555 1_555 ?
C4 O3 Pb03 124.296(2) 1_555 2_547 ?
O4 O3 O12 113.434(2) 1_555 2_547 ?
O4 O3 Pb01 63.6096(14) 1_555 1_555 ?
O4 O3 Pb03 141.481(3) 1_555 2_547 ?
O12 O3 Pb01 54.3056(13) 2_547 1_555 ?
O12 O3 Pb03 53.1569(12) 2_547 2_547 ?
Pb01 O3 Pb03 105.681(2) 1_555 2_547 ?
C3 O4 O2 103.274(3) 1_555 1_555 ?
C3 O4 Pb01 96.213(3) 1_555 1_555 ?
C3 O4 Pb03 144.332(4) 1_555 2_557 ?
C4 O4 O2 130.063(3) 1_555 1_555 ?
C4 O4 O3 63.3384(13) 1_555 1_555 ?
C4 O4 Pb01 131.411(3) 1_555 1_555 ?
C4 O4 Pb03 112.748(2) 1_555 2_557 ?
O2 O4 O3 83.3943(16) 1_555 1_555 ?
O2 O4 Pb01 50.9521(12) 1_555 1_555 ?
O2 O4 Pb03 112.366(2) 1_555 2_557 ?
O3 O4 Pb01 69.5412(15) 1_555 1_555 ?
O3 O4 Pb03 155.295(4) 1_555 2_557 ?
Pb01 O4 Pb03 104.845(2) 1_555 2_557 ?
C5 O5 Pb02 92.657(2) 1_555 1_555 ?
C6 O5 O6 64.6222(15) 1_555 1_555 ?
C6 O5 Pb02 128.224(3) 1_555 1_555 ?
O6 O5 Pb02 63.6402(15) 1_555 1_555 ?
C5 O6 Pb02 91.750(2) 1_555 1_555 ?
C5 O6 Pb03 141.713(4) 1_555 1_555 ?
C6 O6 O5 60.0397(14) 1_555 1_555 ?
C6 O6 Pb02 123.716(3) 1_555 1_555 ?
C6 O6 Pb03 109.837(3) 1_555 1_555 ?
O5 O6 Pb02 63.7113(14) 1_555 1_555 ?
O5 O6 Pb03 169.829(3) 1_555 1_555 ?
Pb02 O6 Pb03 126.354(2) 1_555 1_555 ?
C7 O7 O27 153.876(3) 1_555 1_555 ?
C7 O7 Pb04 142.130(4) 1_555 1_555 ?
C7 O7 PbO7 100.496(3) 1_555 1_555 ?
C8 O7 O8 60.1964(13) 1_555 1_555 ?
C8 O7 O27 168.903(3) 1_555 1_555 ?
C8 O7 Pb04 111.290(2) 1_555 1_555 ?
C8 O7 PbO7 131.315(3) 1_555 1_555 ?
O8 O7 O27 126.154(2) 1_555 1_555 ?
O8 O7 Pb04 171.169(4) 1_555 1_555 ?
O8 O7 PbO7 71.3721(16) 1_555 1_555 ?
O27 O7 Pb04 62.6446(14) 1_555 1_555 ?
O27 O7 PbO7 55.0484(12) 1_555 1_555 ?
Pb04 O7 PbO7 117.291(2) 1_555 1_555 ?
C7 O8 O28 144.433(3) 1_555 1_545 ?
C7 O8 Pb04 148.203(4) 1_555 1_545 ?
C7 O8 PbO7 94.964(3) 1_555 1_555 ?
C8 O8 O7 66.6116(14) 1_555 1_555 ?
C8 O8 O28 169.755(3) 1_555 1_545 ?
C8 O8 Pb04 118.455(2) 1_555 1_545 ?
C8 O8 PbO7 129.527(3) 1_555 1_555 ?
O7 O8 O28 113.954(2) 1_555 1_545 ?
O7 O8 Pb04 161.370(4) 1_555 1_545 ?
O7 O8 PbO7 63.1613(14) 1_555 1_555 ?
O28 O8 Pb04 57.5980(13) 1_545 1_545 ?
O28 O8 PbO7 51.1246(12) 1_545 1_555 ?
Pb04 O8 PbO7 107.858(2) 1_545 1_555 ?
C9 O9 Pb03 114.149(3) 1_555 1_555 ?
C10 O9 O10 62.4064(12) 1_555 1_555 ?
C10 O9 Pb03 149.110(3) 1_555 1_555 ?
O10 O9 Pb03 87.9773(17) 1_555 1_555 ?
C9 O10 Pb03 75.067(2) 1_555 1_555 ?
C9 O10 Pb06 129.812(3) 1_555 2_547 ?
C10 O10 O9 61.4634(12) 1_555 1_555 ?
C10 O10 Pb03 107.690(2) 1_555 1_555 ?
C10 O10 Pb06 105.860(2) 1_555 2_547 ?
O9 O10 Pb03 46.7139(11) 1_555 1_555 ?
O9 O10 Pb06 142.609(3) 1_555 2_547 ?
Pb03 O10 Pb06 134.457(3) 1_555 2_547 ?
C11 O11 Pb01 143.201(4) 1_555 2_547 ?
C11 O11 Pb03 87.494(2) 1_555 1_555 ?
C12 O11 O12 61.9311(13) 1_555 1_555 ?
C12 O11 Pb01 120.849(2) 1_555 2_547 ?
C12 O11 Pb03 121.429(3) 1_555 1_555 ?
O12 O11 Pb01 146.894(3) 1_555 2_547 ?
O12 O11 Pb03 59.8603(13) 1_555 1_555 ?
Pb01 O11 Pb03 104.528(2) 2_547 1_555 ?
C11 O12 O3 159.285(3) 1_555 2_557 ?
C11 O12 Pb01 140.357(4) 1_555 2_557 ?
C11 O12 Pb03 103.329(3) 1_555 1_555 ?
C12 O12 O3 164.880(3) 1_555 2_557 ?
C12 O12 O11 65.2707(13) 1_555 1_555 ?
C12 O12 Pb01 108.055(2) 1_555 2_557 ?
C12 O12 Pb03 137.357(3) 1_555 1_555 ?
O3 O12 O11 128.825(2) 2_557 1_555 ?
O3 O12 Pb01 60.1269(14) 2_557 2_557 ?
O3 O12 Pb03 56.2193(12) 2_557 1_555 ?
O11 O12 Pb01 162.836(4) 1_555 2_557 ?
O11 O12 Pb03 72.6062(15) 1_555 1_555 ?
Pb01 O12 Pb03 114.252(2) 2_557 1_555 ?
C13 O13 O14 156.260(3) 1_555 2_547 ?
C13 O13 Pb02 141.867(4) 1_555 1_545 ?
C13 O13 Pb02 103.442(3) 1_555 2_547 ?
C14 O13 O14 67.0131(14) 1_555 1_555 ?
C14 O13 O14 168.127(3) 1_555 2_547 ?
C14 O13 Pb02 108.210(2) 1_555 1_545 ?
C14 O13 Pb02 137.371(3) 1_555 2_547 ?
O14 O13 O14 123.379(2) 1_555 2_547 ?
O14 O13 Pb02 171.256(4) 1_555 1_545 ?
O14 O13 Pb02 70.3594(16) 1_555 2_547 ?
O14 O13 Pb02 60.6691(14) 2_547 1_545 ?
O14 O13 Pb02 53.4259(12) 2_547 2_547 ?
Pb02 O13 Pb02 114.088(2) 1_545 2_547 ?
C13 O14 O13 147.400(3) 1_555 2_557 ?
C13 O14 Pb02 153.586(4) 1_555 1_555 ?
C13 O14 Pb02 95.708(3) 1_555 2_547 ?
C14 O14 O13 61.4181(14) 1_555 1_555 ?
C14 O14 O13 175.374(3) 1_555 2_557 ?
C14 O14 Pb02 122.000(2) 1_555 1_555 ?
C14 O14 Pb02 127.439(3) 1_555 2_547 ?
O13 O14 O13 117.776(2) 1_555 2_557 ?
O13 O14 Pb02 173.918(4) 1_555 1_555 ?
O13 O14 Pb02 66.0215(15) 1_555 2_547 ?
O13 O14 Pb02 58.3555(13) 2_557 1_555 ?
O13 O14 Pb02 52.0279(12) 2_557 2_547 ?
Pb02 O14 Pb02 110.377(2) 1_555 2_547 ?
C15 O15 O21 124.811(3) 1_555 1_555 ?
C15 O15 Pb01 130.253(3) 1_555 1_555 ?
C16 O15 O16 61.5350(12) 1_555 1_555 ?
C16 O15 O21 158.440(3) 1_555 1_555 ?
C16 O15 Pb01 104.770(2) 1_555 1_555 ?
O16 O15 O21 97.471(2) 1_555 1_555 ?
O16 O15 Pb01 143.983(3) 1_555 1_555 ?
O21 O15 Pb01 95.313(2) 1_555 1_555 ?
C15 O16 Pb05 115.527(3) 1_555 1_555 ?
C16 O16 O15 61.0000(12) 1_555 1_555 ?
C16 O16 Pb05 148.101(3) 1_555 1_555 ?
O15 O16 Pb05 87.9695(17) 1_555 1_555 ?
C17 O17 O22 148.090(3) 1_555 1_565 ?
C17 O17 Pb05 147.070(4) 1_555 1_565 ?
C17 O17 Pb06 93.728(3) 1_555 1_555 ?
C18 O17 O18 64.1340(13) 1_555 1_555 ?
C18 O17 O22 178.965(3) 1_555 1_565 ?
C18 O17 Pb05 123.760(2) 1_555 1_565 ?
C18 O17 Pb06 125.995(3) 1_555 1_555 ?
O18 O17 O22 116.829(2) 1_555 1_565 ?
O18 O17 Pb05 146.662(3) 1_555 1_565 ?
O18 O17 Pb06 63.6747(13) 1_555 1_555 ?
O22 O17 Pb05 55.2474(12) 1_565 1_565 ?
O22 O17 Pb06 55.0349(13) 1_565 1_555 ?
Pb05 O17 Pb06 107.391(2) 1_565 1_555 ?
C17 O18 O20 102.082(2) 1_555 1_555 ?
C17 O18 O21 146.962(3) 1_555 1_555 ?
C17 O18 Pb05 139.853(4) 1_555 1_555 ?
C17 O18 Pb06 94.741(2) 1_555 1_555 ?
C18 O18 O17 60.6135(13) 1_555 1_555 ?
C18 O18 O20 124.689(3) 1_555 1_555 ?
C18 O18 O21 162.464(3) 1_555 1_555 ?
C18 O18 Pb05 112.131(2) 1_555 1_555 ?
C18 O18 Pb06 126.820(3) 1_555 1_555 ?
O17 O18 O20 79.5312(15) 1_555 1_555 ?
O17 O18 O21 122.679(2) 1_555 1_555 ?
O17 O18 Pb05 157.286(4) 1_555 1_555 ?
O17 O18 Pb06 68.0436(14) 1_555 1_555 ?
O20 O18 O21 71.5451(13) 1_555 1_555 ?
O20 O18 Pb05 118.048(2) 1_555 1_555 ?
O20 O18 Pb06 53.0193(12) 1_555 1_555 ?
O21 O18 Pb05 57.4388(13) 1_555 1_555 ?
O21 O18 Pb06 54.9107(12) 1_555 1_555 ?
Pb05 O18 Pb06 109.661(2) 1_555 1_555 ?
C19 O19 Pb06 95.374(2) 1_555 1_555 ?
C20 O19 O20 62.0198(14) 1_555 1_555 ?
C20 O19 Pb06 126.852(3) 1_555 1_555 ?
O20 O19 Pb06 64.8763(15) 1_555 1_555 ?
C19 O20 O18 143.989(3) 1_555 1_555 ?
C19 O20 Pb04 140.807(3) 1_555 1_555 ?
C19 O20 Pb06 93.026(2) 1_555 1_555 ?
C20 O20 O18 160.136(3) 1_555 1_555 ?
C20 O20 O19 63.7858(14) 1_555 1_555 ?
C20 O20 Pb04 106.189(2) 1_555 1_555 ?
C20 O20 Pb06 127.547(3) 1_555 1_555 ?
O18 O20 O19 117.212(3) 1_555 1_555 ?
O18 O20 Pb04 71.5322(14) 1_555 1_555 ?
O18 O20 Pb06 56.7639(12) 1_555 1_555 ?
O19 O20 Pb04 169.846(3) 1_555 1_555 ?
O19 O20 Pb06 63.8063(14) 1_555 1_555 ?
Pb04 O20 Pb06 126.112(3) 1_555 1_555 ?
C21 O21 O15 85.9049(19) 1_555 1_555 ?
C21 O21 O18 140.201(3) 1_555 1_555 ?
C21 O21 Pb05 93.046(2) 1_555 1_555 ?
C21 O21 Pb06 137.053(4) 1_555 1_555 ?
C22 O21 O15 99.2172(19) 1_555 1_555 ?
C22 O21 O18 162.000(3) 1_555 1_555 ?
C22 O21 O22 61.4102(13) 1_555 1_555 ?
C22 O21 Pb05 123.909(3) 1_555 1_555 ?
C22 O21 Pb06 118.628(2) 1_555 1_555 ?
O15 O21 O18 62.9173(13) 1_555 1_555 ?
O15 O21 O22 74.5264(14) 1_555 1_555 ?
O15 O21 Pb05 65.2936(14) 1_555 1_555 ?
O15 O21 Pb06 67.8996(13) 1_555 1_555 ?
O18 O21 O22 112.177(2) 1_555 1_555 ?
O18 O21 Pb05 52.7515(12) 1_555 1_555 ?
O18 O21 Pb06 54.6511(12) 1_555 1_555 ?
O22 O21 Pb05 62.4998(13) 1_555 1_555 ?
O22 O21 Pb06 141.973(3) 1_555 1_555 ?
Pb05 O21 Pb06 104.943(2) 1_555 1_555 ?
C21 O22 O17 153.447(3) 1_555 1_545 ?
C21 O22 Pb05 98.446(2) 1_555 1_555 ?
C21 O22 Pb06 138.057(4) 1_555 1_545 ?
C22 O22 O17 168.146(3) 1_555 1_545 ?
C22 O22 O21 63.7104(13) 1_555 1_555 ?
C22 O22 Pb05 132.034(3) 1_555 1_555 ?
C22 O22 Pb06 110.467(2) 1_555 1_545 ?
O17 O22 O21 124.038(2) 1_545 1_555 ?
O17 O22 Pb05 56.6345(12) 1_545 1_555 ?
O17 O22 Pb06 58.2207(13) 1_545 1_545 ?
O21 O22 Pb05 68.3241(14) 1_555 1_555 ?
O21 O22 Pb06 151.820(4) 1_555 1_545 ?
Pb05 O22 Pb06 111.714(2) 1_555 1_545 ?
C23 O23 Pb05 141.259(4) 1_555 1_555 ?
C23 O23 PbO7 92.902(3) 1_555 1_555 ?
C24 O23 O24 63.7925(15) 1_555 1_555 ?
C24 O23 Pb05 106.853(2) 1_555 1_555 ?
C24 O23 PbO7 127.277(3) 1_555 1_555 ?
O24 O23 Pb05 170.340(3) 1_555 1_555 ?
O24 O23 PbO7 63.5545(14) 1_555 1_555 ?
Pb05 O23 PbO7 125.598(2) 1_555 1_555 ?
C23 O24 PbO7 94.753(3) 1_555 1_555 ?
C24 O24 O23 62.0275(14) 1_555 1_555 ?
C24 O24 PbO7 127.773(3) 1_555 1_555 ?
O23 O24 PbO7 65.8167(15) 1_555 1_555 ?
C25 O25 O32 149.205(3) 1_555 1_555 ?
C25 O25 PbO7 141.854(4) 1_555 1_555 ?
C25 O25 Pb08 95.074(2) 1_555 1_555 ?
C26 O25 O26 61.8674(14) 1_555 1_555 ?
C26 O25 O32 165.073(3) 1_555 1_555 ?
C26 O25 PbO7 110.093(3) 1_555 1_555 ?
C26 O25 Pb08 126.801(3) 1_555 1_555 ?
O26 O25 O32 120.897(3) 1_555 1_555 ?
O26 O25 PbO7 171.922(3) 1_555 1_555 ?
O26 O25 Pb08 64.9928(14) 1_555 1_555 ?
O32 O25 PbO7 67.0414(14) 1_555 1_555 ?
O32 O25 Pb08 57.5488(13) 1_555 1_555 ?
PbO7 O25 Pb08 123.072(2) 1_555 1_555 ?
C25 O26 Pb08 93.522(2) 1_555 1_555 ?
C26 O26 O25 63.9131(14) 1_555 1_555 ?
C26 O26 Pb08 126.131(3) 1_555 1_555 ?
O25 O26 Pb08 62.2758(14) 1_555 1_555 ?
C27 O27 O7 140.189(3) 1_555 1_555 ?
C27 O27 Pb04 93.349(3) 1_555 1_555 ?
C27 O27 PbO7 145.851(4) 1_555 1_555 ?
C28 O27 O7 165.798(3) 1_555 1_555 ?
C28 O27 O28 66.2343(14) 1_555 1_555 ?
C28 O27 Pb04 130.265(3) 1_555 1_555 ?
C28 O27 PbO7 116.726(2) 1_555 1_555 ?
O7 O27 O28 112.303(2) 1_555 1_555 ?
O7 O27 Pb04 51.2109(12) 1_555 1_555 ?
O7 O27 PbO7 57.6895(13) 1_555 1_555 ?
O28 O27 Pb04 64.0875(14) 1_555 1_555 ?
O28 O27 PbO7 153.149(4) 1_555 1_555 ?
Pb04 O27 PbO7 108.559(2) 1_555 1_555 ?
C27 O28 O8 152.937(3) 1_555 1_565 ?
C27 O28 O30 104.001(3) 1_555 1_555 ?
C27 O28 Pb04 100.140(3) 1_555 1_555 ?
C27 O28 PbO7 141.995(4) 1_555 1_565 ?
C28 O28 O8 173.172(3) 1_555 1_565 ?
C28 O28 O27 59.6092(13) 1_555 1_555 ?
C28 O28 O30 122.341(3) 1_555 1_555 ?
C28 O28 Pb04 130.333(3) 1_555 1_555 ?
C28 O28 PbO7 113.494(2) 1_555 1_565 ?
O8 O28 O27 123.955(2) 1_565 1_555 ?
O8 O28 O30 64.4838(12) 1_565 1_555 ?
O8 O28 Pb04 53.3423(12) 1_565 1_555 ?
O8 O28 PbO7 61.4358(14) 1_565 1_565 ?
O27 O28 O30 83.6543(17) 1_555 1_555 ?
O27 O28 Pb04 70.7799(15) 1_555 1_555 ?
O27 O28 PbO7 164.362(4) 1_555 1_565 ?
O30 O28 Pb04 49.1907(12) 1_555 1_555 ?
O30 O28 PbO7 110.8682(20 1_555 1_565 ?
Pb04 O28 PbO7 113.813(2) 1_555 1_565 ?
C29 O29 Pb04 97.565(3) 1_555 1_555 ?
C30 O29 O30 64.2139(15) 1_555 1_555 ?
C30 O29 Pb04 128.139(3) 1_555 1_555 ?
O30 O29 Pb04 63.9259(15) 1_555 1_555 ?
C29 O30 O28 147.168(3) 1_555 1_555 ?
C29 O30 Pb04 95.839(3) 1_555 1_555 ?
C29 O30 Pb09 137.240(4) 1_555 1_555 ?
C30 O30 O28 163.706(3) 1_555 1_555 ?
C30 O30 O29 63.1766(15) 1_555 1_555 ?
C30 O30 Pb04 127.569(3) 1_555 1_555 ?
C30 O30 Pb09 105.564(2) 1_555 1_555 ?
O28 O30 O29 118.923(3) 1_555 1_555 ?
O28 O30 Pb04 57.4002(13) 1_555 1_555 ?
O28 O30 Pb09 71.4639(15) 1_555 1_555 ?
O29 O30 Pb04 64.3935(15) 1_555 1_555 ?
O29 O30 Pb09 168.680(3) 1_555 1_555 ?
Pb04 O30 Pb09 126.861(3) 1_555 1_555 ?
C31 O31 O36 155.804(3) 1_555 1_555 ?
C31 O31 Pb08 101.808(3) 1_555 1_555 ?
C31 O31 Pb09 144.261(4) 1_555 1_555 ?
C32 O31 O32 63.6382(14) 1_555 1_555 ?
C32 O31 O36 176.005(3) 1_555 1_555 ?
C32 O31 Pb08 129.496(3) 1_555 1_555 ?
C32 O31 Pb09 119.090(2) 1_555 1_555 ?
O32 O31 O36 120.106(2) 1_555 1_555 ?
O32 O31 Pb08 67.4699(15) 1_555 1_555 ?
O32 O31 Pb09 156.324(4) 1_555 1_555 ?
O36 O31 Pb08 54.4890(13) 1_555 1_555 ?
O36 O31 Pb09 56.9421(13) 1_555 1_555 ?
Pb08 O31 Pb09 110.666(2) 1_555 1_555 ?
C31 O32 O25 110.280(3) 1_555 1_555 ?
C31 O32 Pb08 101.519(3) 1_555 1_555 ?
C31 O32 Pb09 139.161(4) 1_555 1_545 ?
C32 O32 O25 130.723(3) 1_555 1_555 ?
C32 O32 O31 65.2210(14) 1_555 1_555 ?
C32 O32 Pb08 131.726(3) 1_555 1_555 ?
C32 O32 Pb09 112.678(2) 1_555 1_545 ?
O25 O32 O31 81.1124(16) 1_555 1_555 ?
O25 O32 Pb08 49.6787(12) 1_555 1_555 ?
O25 O32 Pb09 110.4215(20 1_555 1_545 ?
O31 O32 Pb08 68.2067(15) 1_555 1_555 ?
O31 O32 Pb09 160.940(4) 1_555 1_545 ?
Pb08 O32 Pb09 107.031(2) 1_555 1_545 ?
C33 O33 O35 139.051(3) 1_555 1_555 ?
C33 O33 Pb09 83.700(2) 1_555 1_555 ?
C33 O33 Pb10 134.583(3) 1_555 1_555 ?
C34 O33 O34 62.4392(13) 1_555 1_555 ?
C34 O33 O35 170.801(3) 1_555 1_555 ?
C34 O33 Pb09 118.241(3) 1_555 1_555 ?
C34 O33 Pb10 104.273(2) 1_555 1_555 ?
O34 O33 O35 111.368(2) 1_555 1_555 ?
O34 O33 Pb09 55.8743(13) 1_555 1_555 ?
O34 O33 Pb10 154.788(3) 1_555 1_555 ?
O35 O33 Pb09 55.6454(13) 1_555 1_555 ?
O35 O33 Pb10 84.0034(19) 1_555 1_555 ?
Pb09 O33 Pb10 133.262(2) 1_555 1_555 ?
C33 O34 Pb09 104.389(3) 1_555 1_555 ?
C34 O34 O33 63.3917(13) 1_555 1_555 ?
C34 O34 Pb09 139.088(3) 1_555 1_555 ?
O33 O34 Pb09 75.8121(16) 1_555 1_555 ?
C35 O35 O33 94.478(2) 1_555 1_555 ?
C35 O35 Pb08 145.851(4) 1_555 1_565 ?
C35 O35 Pb09 97.731(3) 1_555 1_555 ?
C36 O35 O33 108.177(2) 1_555 1_555 ?
C36 O35 O36 62.8436(14) 1_555 1_555 ?
C36 O35 Pb08 122.258(2) 1_555 1_565 ?
C36 O35 Pb09 126.729(3) 1_555 1_555 ?
O33 O35 O36 76.4226(15) 1_555 1_555 ?
O33 O35 Pb08 77.5117(15) 1_555 1_565 ?
O33 O35 Pb09 55.9972(13) 1_555 1_555 ?
O36 O35 Pb08 153.500(4) 1_555 1_565 ?
O36 O35 Pb09 63.9397(14) 1_555 1_555 ?
Pb08 O35 Pb09 104.489(2) 1_565 1_555 ?
C35 O36 O31 157.598(3) 1_555 1_555 ?
C35 O36 Pb08 139.972(4) 1_555 1_555 ?
C35 O36 Pb09 101.142(3) 1_555 1_555 ?
C36 O36 O31 168.163(3) 1_555 1_555 ?
C36 O36 O35 64.5806(14) 1_555 1_555 ?
C36 O36 Pb08 108.778(2) 1_555 1_555 ?
C36 O36 Pb09 134.482(3) 1_555 1_555 ?
O31 O36 O35 126.709(2) 1_555 1_555 ?
O31 O36 Pb08 59.3845(13) 1_555 1_555 ?
O31 O36 Pb09 57.0912(13) 1_555 1_555 ?
O35 O36 Pb08 163.523(4) 1_555 1_555 ?
O35 O36 Pb09 69.9664(15) 1_555 1_555 ?
Pb08 O36 Pb09 115.634(2) 1_555 1_555 ?
C37 O37 Pb10 110.545(3) 1_555 1_555 ?
C38 O37 O38 62.9442(13) 1_555 1_555 ?
C38 O37 Pb10 148.205(3) 1_555 1_555 ?
O38 O37 Pb10 85.2630(16) 1_555 1_555 ?
C37 O38 Pb08 131.186(3) 1_555 2_756 ?
C37 O38 Pb10 74.659(2) 1_555 1_555 ?
C38 O38 O37 60.1199(13) 1_555 1_555 ?
C38 O38 Pb08 107.729(2) 1_555 2_756 ?
C38 O38 Pb10 107.872(2) 1_555 1_555 ?
O37 O38 Pb08 145.851(3) 1_555 2_756 ?
O37 O38 Pb10 47.7527(11) 1_555 1_555 ?
Pb08 O38 Pb10 130.212(3) 2_756 1_555 ?
C39 O39 O40 155.602(3) 1_555 2_756 ?
C39 O39 Pb10 102.251(3) 1_555 1_555 ?
C39 O39 Pb10 137.118(4) 1_555 2_756 ?
C40 O39 O40 65.0232(13) 1_555 1_555 ?
C40 O39 O40 163.732(3) 1_555 2_756 ?
C40 O39 Pb10 134.745(3) 1_555 1_555 ?
C40 O39 Pb10 108.318(2) 1_555 2_756 ?
O40 O39 O40 125.285(2) 1_555 2_756 ?
O40 O39 Pb10 70.4970(14) 1_555 1_555 ?
O40 O39 Pb10 154.824(4) 1_555 2_756 ?
O40 O39 Pb10 55.0864(12) 2_756 1_555 ?
O40 O39 Pb10 56.6452(13) 2_756 2_756 ?
Pb10 O39 Pb10 108.245(2) 1_555 2_756 ?
C39 O40 O39 139.315(3) 1_555 2_746 ?
C39 O40 Pb10 90.016(2) 1_555 1_555 ?
C39 O40 Pb10 138.927(4) 1_555 2_746 ?
C40 O40 O39 61.1512(13) 1_555 1_555 ?
C40 O40 O39 166.640(3) 1_555 2_746 ?
C40 O40 Pb10 121.502(3) 1_555 1_555 ?
C40 O40 Pb10 124.784(2) 1_555 2_746 ?
O39 O40 O39 111.112(2) 1_555 2_746 ?
O39 O40 Pb10 60.9273(13) 1_555 1_555 ?
O39 O40 Pb10 137.176(3) 1_555 2_746 ?
O39 O40 Pb10 53.9740(12) 2_746 1_555 ?
O39 O40 Pb10 52.1968(12) 2_746 2_746 ?
Pb10 O40 Pb10 103.0123(20 1_555 2_746 ?
C1 Pb01 C3 104.208(2) 1_555 1_555 ?
C1 Pb01 O3 107.383(2) 1_555 1_555 ?
C1 Pb01 O4 96.5926(19) 1_555 1_555 ?
C1 Pb01 O11 82.2917(16) 1_555 2_557 ?
C1 Pb01 O12 81.6334(16) 1_555 2_547 ?
C1 Pb01 O15 107.074(2) 1_555 1_555 ?
C3 Pb01 O1 129.861(3) 1_555 1_555 ?
C3 Pb01 O2 77.7459(17) 1_555 1_555 ?
C3 Pb01 O11 96.1557(19) 1_555 2_557 ?
C3 Pb01 O12 88.3734(17) 1_555 2_547 ?
C3 Pb01 O15 148.615(3) 1_555 1_555 ?
O1 Pb01 O2 52.2769(13) 1_555 1_555 ?
O1 Pb01 O3 128.494(3) 1_555 1_555 ?
O1 Pb01 O4 121.484(3) 1_555 1_555 ?
O1 Pb01 O11 84.0771(16) 1_555 2_557 ?
O1 Pb01 O12 81.2027(15) 1_555 2_547 ?
O1 Pb01 O15 81.2663(18) 1_555 1_555 ?
O2 Pb01 O3 83.4828(17) 1_555 1_555 ?
O2 Pb01 O4 71.7955(14) 1_555 1_555 ?
O2 Pb01 O11 84.4998(17) 1_555 2_557 ?
O2 Pb01 O12 81.3852(17) 1_555 2_547 ?
O2 Pb01 O15 133.534(3) 1_555 1_555 ?
O3 Pb01 O4 46.8492(11) 1_555 1_555 ?
O3 Pb01 O11 120.438(2) 1_555 2_557 ?
O3 Pb01 O12 65.5674(14) 1_555 2_547 ?
O3 Pb01 O15 136.057(3) 1_555 1_555 ?
O4 Pb01 O11 74.0097(15) 1_555 2_557 ?
O4 Pb01 O12 108.481(2) 1_555 2_547 ?
O4 Pb01 O15 149.756(3) 1_555 1_555 ?
O11 Pb01 O12 163.914(4) 2_557 2_547 ?
O11 Pb01 O15 90.4912(15) 2_557 1_555 ?
O12 Pb01 O15 93.6413(16) 2_547 1_555 ?
C5 Pb02 O2 105.061(2) 1_555 1_555 ?
C5 Pb02 O13 80.9223(16) 1_555 1_565 ?
C5 Pb02 O13 104.141(2) 1_555 2_557 ?
C5 Pb02 O14 87.3350(17) 1_555 1_555 ?
C5 Pb02 O14 101.275(2) 1_555 2_557 ?
O2 Pb02 O5 79.3822(17) 1_555 1_555 ?
O2 Pb02 O6 131.802(3) 1_555 1_555 ?
O2 Pb02 O13 99.2329(17) 1_555 1_565 ?
O2 Pb02 O13 140.834(3) 1_555 2_557 ?
O2 Pb02 O14 87.6665(15) 1_555 1_555 ?
O2 Pb02 O14 148.035(3) 1_555 2_557 ?
O5 Pb02 O6 52.6485(13) 1_555 1_555 ?
O5 Pb02 O13 81.7045(15) 1_555 1_565 ?
O5 Pb02 O13 128.345(3) 1_555 2_557 ?
O5 Pb02 O14 89.5072(17) 1_555 1_555 ?
O5 Pb02 O14 124.155(3) 1_555 2_557 ?
O6 Pb02 O13 80.1562(16) 1_555 1_565 ?
O6 Pb02 O13 79.3898(16) 1_555 2_557 ?
O6 Pb02 O14 87.5413(17) 1_555 1_555 ?
O6 Pb02 O14 76.3171(16) 1_555 2_557 ?
O13 Pb02 O13 110.694(2) 1_565 2_557 ?
O13 Pb02 O14 167.580(4) 1_565 1_555 ?
O13 Pb02 O14 67.3030(14) 1_565 2_557 ?
O13 Pb02 O14 68.2186(14) 2_557 1_555 ?
O14 Pb02 O14 111.529(2) 1_555 2_557 ?
C9 Pb03 C11 87.8602(18) 1_555 1_555 ?
C9 Pb03 O3 94.7546(19) 1_555 2_557 ?
C9 Pb03 O4 71.9299(16) 1_555 2_547 ?
C9 Pb03 O6 107.806(2) 1_555 1_555 ?
C9 Pb03 O11 87.5139(18) 1_555 1_555 ?
C9 Pb03 O12 91.0658(16) 1_555 1_555 ?
C11 Pb03 O3 92.8333(18) 1_555 2_557 ?
C11 Pb03 O4 95.9657(18) 1_555 2_547 ?
C11 Pb03 O6 164.228(3) 1_555 1_555 ?
C11 Pb03 O9 107.063(2) 1_555 1_555 ?
C11 Pb03 O10 67.3658(13) 1_555 1_555 ?
O3 Pb03 O4 163.680(4) 2_557 2_547 ?
O3 Pb03 O6 87.7757(15) 2_557 1_555 ?
O3 Pb03 O9 81.5912(17) 2_557 1_555 ?
O3 Pb03 O10 104.372(2) 2_557 1_555 ?
O3 Pb03 O11 118.157(2) 2_557 1_555 ?
O3 Pb03 O12 70.6239(14) 2_557 1_555 ?
O4 Pb03 O6 87.4661(16) 2_547 1_555 ?
O4 Pb03 O9 82.6963(16) 2_547 1_555 ?
O4 Pb03 O10 66.8446(14) 2_547 1_555 ?
O4 Pb03 O11 71.7389(15) 2_547 1_555 ?
O4 Pb03 O12 117.819(2) 2_547 1_555 ?
O6 Pb03 O9 88.6249(19) 1_555 1_555 ?
O6 Pb03 O10 127.677(2) 1_555 1_555 ?
O6 Pb03 O11 149.198(3) 1_555 1_555 ?
O6 Pb03 O12 152.607(3) 1_555 1_555 ?
O9 Pb03 O10 45.3088(11) 1_555 1_555 ?
O9 Pb03 O11 110.204(2) 1_555 1_555 ?
O9 Pb03 O12 104.069(2) 1_555 1_555 ?
O10 Pb03 O11 64.9515(13) 1_555 1_555 ?
O10 Pb03 O12 75.5659(13) 1_555 1_555 ?
O11 Pb03 O12 47.5335(12) 1_555 1_555 ?
C29 Pb04 O7 84.5015(17) 1_555 1_555 ?
C29 Pb04 O8 81.1474(16) 1_555 1_565 ?
C29 Pb04 O20 105.858(2) 1_555 1_555 ?
C29 Pb04 O27 108.439(2) 1_555 1_555 ?
C29 Pb04 O28 98.5627(19) 1_555 1_555 ?
O7 Pb04 O8 164.843(4) 1_555 1_565 ?
O7 Pb04 O20 96.8069(17) 1_555 1_555 ?
O7 Pb04 O27 66.1444(14) 1_555 1_555 ?
O7 Pb04 O28 108.582(2) 1_555 1_555 ?
O7 Pb04 O29 84.9739(15) 1_555 1_555 ?
O7 Pb04 O30 84.3071(17) 1_555 1_555 ?
O8 Pb04 O20 91.7999(16) 1_565 1_555 ?
O8 Pb04 O27 114.059(2) 1_565 1_555 ?
O8 Pb04 O28 69.0598(14) 1_565 1_555 ?
O8 Pb04 O29 84.0754(16) 1_565 1_555 ?
O8 Pb04 O30 80.6847(16) 1_565 1_555 ?
O20 Pb04 O27 139.499(3) 1_555 1_555 ?
O20 Pb04 O28 146.234(3) 1_555 1_555 ?
O20 Pb04 O29 81.0097(18) 1_555 1_555 ?
O20 Pb04 O30 132.510(3) 1_555 1_555 ?
O27 Pb04 O28 45.1326(12) 1_555 1_555 ?
O27 Pb04 O29 129.929(3) 1_555 1_555 ?
O27 Pb04 O30 84.1451(17) 1_555 1_555 ?
O28 Pb04 O29 122.146(3) 1_555 1_555 ?
O28 Pb04 O30 73.4091(15) 1_555 1_555 ?
O29 Pb04 O30 51.6807(13) 1_555 1_555 ?
C15 Pb05 C21 85.1957(17) 1_555 1_555 ?
C15 Pb05 O17 96.3474(19) 1_555 1_545 ?
C15 Pb05 O18 73.8090(16) 1_555 1_555 ?
C15 Pb05 O21 87.3959(18) 1_555 1_555 ?
C15 Pb05 O22 84.3648(15) 1_555 1_555 ?
C15 Pb05 O23 106.445(2) 1_555 1_555 ?
C21 Pb05 O16 103.974(2) 1_555 1_555 ?
C21 Pb05 O17 92.4168(18) 1_555 1_545 ?
C21 Pb05 O18 92.7034(18) 1_555 1_555 ?
C21 Pb05 O23 168.160(3) 1_555 1_555 ?
O16 Pb05 O17 84.3965(17) 1_555 1_545 ?
O16 Pb05 O18 84.3446(16) 1_555 1_555 ?
O16 Pb05 O21 109.154(2) 1_555 1_555 ?
O16 Pb05 O22 96.8333(19) 1_555 1_555 ?
O16 Pb05 O23 87.8648(19) 1_555 1_555 ?
O17 Pb05 O18 168.470(4) 1_545 1_555 ?
O17 Pb05 O21 116.525(2) 1_545 1_555 ?
O17 Pb05 O22 68.1182(14) 1_545 1_555 ?
O17 Pb05 O23 88.4938(16) 1_545 1_555 ?
O18 Pb05 O21 69.8098(15) 1_555 1_555 ?
O18 Pb05 O22 115.797(2) 1_555 1_555 ?
O18 Pb05 O23 88.6114(16) 1_555 1_555 ?
O21 Pb05 O22 49.1761(11) 1_555 1_555 ?
O21 Pb05 O23 150.312(3) 1_555 1_555 ?
O22 Pb05 O23 155.437(3) 1_555 1_555 ?
C17 Pb06 C19 103.260(2) 1_555 1_555 ?
C17 Pb06 O10 150.292(3) 1_555 2_557 ?
C17 Pb06 O19 128.259(3) 1_555 1_555 ?
C17 Pb06 O20 77.1185(17) 1_555 1_555 ?
C17 Pb06 O21 95.4688(18) 1_555 1_555 ?
C17 Pb06 O22 89.6203(17) 1_555 1_565 ?
C19 Pb06 O10 106.350(2) 1_555 2_557 ?
C19 Pb06 O17 102.541(2) 1_555 1_555 ?
C19 Pb06 O18 94.8664(18) 1_555 1_555 ?
C19 Pb06 O21 85.4687(17) 1_555 1_555 ?
C19 Pb06 O22 84.6882(17) 1_555 1_565 ?
O10 Pb06 O17 141.282(3) 2_557 1_555 ?
O10 Pb06 O18 149.450(3) 2_557 1_555 ?
O10 Pb06 O19 81.2786(18) 2_557 1_555 ?
O10 Pb06 O20 132.554(3) 2_557 1_555 ?
O10 Pb06 O21 89.2518(15) 2_557 1_555 ?
O10 Pb06 O22 90.7285(16) 2_557 1_565 ?
O17 Pb06 O18 48.2817(11) 1_555 1_555 ?
O17 Pb06 O19 124.218(3) 1_555 1_555 ?
O17 Pb06 O20 79.3818(16) 1_555 1_555 ?
O17 Pb06 O21 118.476(2) 1_555 1_555 ?
O17 Pb06 O22 66.7443(14) 1_555 1_565 ?
O18 Pb06 O19 118.215(2) 1_555 1_555 ?
O18 Pb06 O20 70.2169(14) 1_555 1_555 ?
O18 Pb06 O21 70.4382(14) 1_555 1_555 ?
O18 Pb06 O22 113.323(2) 1_555 1_565 ?
O19 Pb06 O20 51.3173(13) 1_555 1_555 ?
O19 Pb06 O21 85.7803(17) 1_555 1_555 ?
O19 Pb06 O22 84.0714(15) 1_555 1_565 ?
O20 Pb06 O21 85.7758(17) 1_555 1_555 ?
O20 Pb06 O22 86.6825(17) 1_555 1_565 ?
O21 Pb06 O22 169.735(4) 1_555 1_565 ?
C23 PbO7 O7 102.4449(20 1_555 1_555 ?
C23 PbO7 O8 103.311(2) 1_555 1_555 ?
C23 PbO7 O25 104.010(2) 1_555 1_555 ?
C23 PbO7 O27 83.8951(17) 1_555 1_555 ?
C23 PbO7 O28 84.7522(17) 1_555 1_545 ?
O7 PbO7 O8 45.4666(12) 1_555 1_555 ?
O7 PbO7 O23 79.5906(15) 1_555 1_555 ?
O7 PbO7 O24 125.432(3) 1_555 1_555 ?
O7 PbO7 O25 142.801(3) 1_555 1_555 ?
O7 PbO7 O27 67.2622(14) 1_555 1_555 ?
O7 PbO7 O28 112.595(2) 1_555 1_545 ?
O8 PbO7 O23 79.8144(16) 1_555 1_555 ?
O8 PbO7 O24 126.317(3) 1_555 1_555 ?
O8 PbO7 O25 146.074(3) 1_555 1_555 ?
O8 PbO7 O27 112.532(2) 1_555 1_555 ?
O8 PbO7 O28 67.4395(15) 1_555 1_545 ?
O23 PbO7 O24 50.6288(13) 1_555 1_555 ?
O23 PbO7 O25 129.176(3) 1_555 1_555 ?
O23 PbO7 O27 84.6021(17) 1_555 1_555 ?
O23 PbO7 O28 83.8821(17) 1_555 1_545 ?
O24 PbO7 O25 78.5793(17) 1_555 1_555 ?
O24 PbO7 O27 85.1330(16) 1_555 1_555 ?
O24 PbO7 O28 85.8763(16) 1_555 1_545 ?
O25 PbO7 O27 90.0751(16) 1_555 1_555 ?
O25 PbO7 O28 95.5022(17) 1_555 1_545 ?
O27 PbO7 O28 168.278(4) 1_555 1_545 ?
C25 Pb08 O31 105.853(2) 1_555 1_555 ?
C25 Pb08 O32 98.7346(20) 1_555 1_555 ?
C25 Pb08 O35 84.0063(16) 1_555 1_545 ?
C25 Pb08 O36 85.9482(17) 1_555 1_555 ?
C25 Pb08 O38 107.055(2) 1_555 2_746 ?
O25 Pb08 O26 52.7313(13) 1_555 1_555 ?
O25 Pb08 O31 82.4693(17) 1_555 1_555 ?
O25 Pb08 O32 72.7725(15) 1_555 1_555 ?
O25 Pb08 O35 82.9703(17) 1_555 1_545 ?
O25 Pb08 O36 88.2160(18) 1_555 1_555 ?
O25 Pb08 O38 133.451(3) 1_555 2_746 ?
O26 Pb08 O31 127.208(3) 1_555 1_555 ?
O26 Pb08 O32 123.813(3) 1_555 1_555 ?
O26 Pb08 O35 86.6906(16) 1_555 1_545 ?
O26 Pb08 O36 84.1222(15) 1_555 1_555 ?
O26 Pb08 O38 81.5242(18) 1_555 2_746 ?
O31 Pb08 O35 117.149(2) 1_555 1_545 ?
O31 Pb08 O36 66.1265(14) 1_555 1_555 ?
O31 Pb08 O38 141.011(3) 1_555 2_746 ?
O32 Pb08 O35 72.9719(15) 1_555 1_545 ?
O32 Pb08 O36 109.016(2) 1_555 1_555 ?
O32 Pb08 O38 145.183(3) 1_555 2_746 ?
O35 Pb08 O36 169.949(4) 1_545 1_555 ?
O35 Pb08 O38 86.6682(15) 1_545 2_746 ?
O36 Pb08 O38 95.9789(17) 1_555 2_746 ?
C33 Pb09 O30 108.240(2) 1_555 1_555 ?
C33 Pb09 O31 97.4523(19) 1_555 1_555 ?
C33 Pb09 O32 77.5398(17) 1_555 1_565 ?
C33 Pb09 O35 93.0684(19) 1_555 1_555 ?
C33 Pb09 O36 94.3013(17) 1_555 1_555 ?
O30 Pb09 O31 87.6702(16) 1_555 1_555 ?
O30 Pb09 O32 90.7108(17) 1_555 1_565 ?
O30 Pb09 O33 131.591(2) 1_555 1_555 ?
O30 Pb09 O34 85.8232(18) 1_555 1_555 ?
O30 Pb09 O35 149.277(3) 1_555 1_555 ?
O30 Pb09 O36 147.529(3) 1_555 1_555 ?
O31 Pb09 O32 173.970(4) 1_555 1_565 ?
O31 Pb09 O33 104.111(2) 1_555 1_555 ?
O31 Pb09 O34 89.7176(17) 1_555 1_555 ?
O31 Pb09 O35 111.810(2) 1_555 1_555 ?
O31 Pb09 O36 65.9667(14) 1_555 1_555 ?
O32 Pb09 O33 72.7492(15) 1_565 1_555 ?
O32 Pb09 O34 84.3700(16) 1_565 1_555 ?
O32 Pb09 O35 72.1288(15) 1_565 1_555 ?
O32 Pb09 O36 117.388(2) 1_565 1_555 ?
O33 Pb09 O34 48.3136(12) 1_555 1_555 ?
O33 Pb09 O35 68.3574(14) 1_555 1_555 ?
O33 Pb09 O36 75.7624(13) 1_555 1_555 ?
O34 Pb09 O35 116.511(2) 1_555 1_555 ?
O34 Pb09 O36 111.384(2) 1_555 1_555 ?
O35 Pb09 O36 46.0939(12) 1_555 1_555 ?
C37 Pb10 C39 87.4370(18) 1_555 1_555 ?
C37 Pb10 O33 109.028(2) 1_555 1_555 ?
C37 Pb10 O39 84.7108(15) 1_555 1_555 ?
C37 Pb10 O39 71.8081(16) 1_555 2_746 ?
C37 Pb10 O40 87.9674(18) 1_555 1_555 ?
C37 Pb10 O40 92.2730(19) 1_555 2_756 ?
C39 Pb10 O33 162.777(3) 1_555 1_555 ?
C39 Pb10 O37 109.831(3) 1_555 1_555 ?
C39 Pb10 O38 66.5041(13) 1_555 1_555 ?
C39 Pb10 O39 93.5876(18) 1_555 2_746 ?
C39 Pb10 O40 95.3969(18) 1_555 2_756 ?
O33 Pb10 O37 87.2234(19) 1_555 1_555 ?
O33 Pb10 O38 128.521(2) 1_555 1_555 ?
O33 Pb10 O39 157.919(3) 1_555 1_555 ?
O33 Pb10 O39 87.0814(16) 1_555 2_746 ?
O33 Pb10 O40 145.356(3) 1_555 1_555 ?
O33 Pb10 O40 89.1266(15) 1_555 2_756 ?
O37 Pb10 O38 46.9843(11) 1_555 1_555 ?
O37 Pb10 O39 102.224(2) 1_555 1_555 ?
O37 Pb10 O39 79.3311(15) 1_555 2_746 ?
O37 Pb10 O40 111.687(2) 1_555 1_555 ?
O37 Pb10 O40 82.2412(17) 1_555 2_756 ?
O38 Pb10 O39 69.5324(12) 1_555 1_555 ?
O38 Pb10 O39 65.5116(14) 1_555 2_746 ?
O38 Pb10 O40 64.7964(13) 1_555 1_555 ?
O38 Pb10 O40 103.433(2) 1_555 2_756 ?
O39 Pb10 O39 114.103(2) 1_555 2_746 ?
O39 Pb10 O40 48.5757(11) 1_555 1_555 ?
O39 Pb10 O40 72.7168(14) 1_555 2_756 ?
O39 Pb10 O40 69.3808(15) 2_746 1_555 ?
O39 Pb10 O40 161.339(4) 2_746 2_756 ?
O40 Pb10 O40 121.030(2) 1_555 2_756 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C2 1.5047(2) 1_555 ?
C1 O1 1.23133(15 1_555 ?
C1 O2 1.25729(19 1_555 ?
C1 Pb01 2.8185(4) 1_555 ?
C2 C1 1.5047(2) 1_555 ?
C2 O1 2.3629(4) 1_555 ?
C2 O2 2.3778(3) 1_555 ?
C3 C4 1.5526(2) 1_555 ?
C3 O3 1.25312(15 1_555 ?
C3 O4 1.17236(13 1_555 ?
C3 Pb01 3.0367(5) 1_555 ?
C4 C3 1.5526(2) 1_555 ?
C4 O3 2.3712(3) 1_555 ?
C4 O4 2.3295(3) 1_555 ?
C5 C6 1.4871(2) 1_555 ?
C5 O5 1.22514(14 1_555 ?
C5 O6 1.26424(19 1_555 ?
C5 Pb02 2.8030(4) 1_555 ?
C6 C5 1.4871(2) 1_555 ?
C6 O5 2.3019(4) 1_555 ?
C6 O6 2.4006(3) 1_555 ?
C7 C8 1.4902(2) 1_555 ?
C7 O7 1.28812(15 1_555 ?
C7 O8 1.19085(15 1_555 ?
C8 C7 1.4902(2) 1_555 ?
C8 O7 2.4417(3) 1_555 ?
C8 O8 2.3085(3) 1_555 ?
C9 C10 1.49063(18 1_555 ?
C9 O9 1.28371(12 1_555 ?
C9 O10 1.19737(17 1_555 ?
C9 Pb03 3.0143(4) 1_555 ?
C10 C9 1.49063(18 1_555 ?
C10 O9 2.3272(3) 1_555 ?
C10 O10 2.3477(3) 1_555 ?
C11 C12 1.5433(2) 1_555 ?
C11 O11 1.27983(16 1_555 ?
C11 O12 1.16123(13 1_555 ?
C11 Pb03 2.9840(4) 1_555 ?
C12 C11 1.5433(2) 1_555 ?
C12 O11 2.4261(3) 1_555 ?
C12 O12 2.3568(3) 1_555 ?
C13 C14 1.4890(2) 1_555 ?
C13 O13 1.13866(13 1_555 ?
C13 O14 1.25505(16 1_555 ?
C14 C13 1.4890(2) 1_555 ?
C14 O13 2.2912(3) 1_555 ?
C14 O14 2.4020(3) 1_555 ?
C15 C16 1.45689(18 1_555 ?
C15 O15 1.27069(18 1_555 ?
C15 O16 1.25623(12 1_555 ?
C15 Pb05 3.0401(4) 1_555 ?
C16 C15 1.45689(18 1_555 ?
C16 O1 3.0888(4) 1_555 ?
C16 O15 2.3230(3) 1_555 ?
C16 O16 2.3349(3) 1_555 ?
C17 C18 1.4473(2) 1_555 ?
C17 O17 1.17282(14 1_555 ?
C17 O18 1.30384(14 1_555 ?
C17 Pb06 2.9916(4) 1_555 ?
C18 C17 1.4473(2) 1_555 ?
C18 O17 2.2845(3) 1_555 ?
C18 O18 2.3592(3) 1_555 ?
C19 C20 1.4725(2) 1_555 ?
C19 O19 1.20427(15 1_555 ?
C19 O20 1.25194(19 1_555 ?
C19 Pb06 2.8281(4) 1_555 ?
C20 C19 1.4725(2) 1_555 ?
C20 O19 2.3564(4) 1_555 ?
C20 O20 2.3196(3) 1_555 ?
C21 C22 1.4653(2) 1_555 ?
C21 O21 1.25801(14 1_555 ?
C21 O22 1.27409(14 1_555 ?
C21 Pb05 3.0239(4) 1_555 ?
C22 C21 1.4653(2) 1_555 ?
C22 O21 2.3954(3) 1_555 ?
C22 O22 2.3460(3) 1_555 ?
C23 C24 1.4884(2) 1_555 ?
C23 O23 1.21229(18 1_555 ?
C23 O24 1.22796(14 1_555 ?
C23 PbO7 2.8464(4) 1_555 ?
C24 C23 1.4884(2) 1_555 ?
C24 O23 2.3210(3) 1_555 ?
C24 O24 2.3579(4) 1_555 ?
C25 C26 1.4813(2) 1_555 ?
C25 O25 1.28781(19 1_555 ?
C25 O26 1.24449(15 1_555 ?
C25 Pb08 2.8426(4) 1_555 ?
C26 C25 1.4813(2) 1_555 ?
C26 O25 2.4113(3) 1_555 ?
C26 O26 2.3677(4) 1_555 ?
C27 C28 1.4772(2) 1_555 ?
C27 O27 1.21832(15 1_555 ?
C27 O28 1.21450(14 1_555 ?
C28 C27 1.4772(2) 1_555 ?
C28 O27 2.2567(3) 1_555 ?
C28 O28 2.3943(3) 1_555 ?
C29 C30 1.4635(2) 1_555 ?
C29 O29 1.21512(15 1_555 ?
C29 O30 1.29038(19 1_555 ?
C29 Pb04 2.8542(4) 1_555 ?
C30 C29 1.4635(2) 1_555 ?
C30 O29 2.3723(4) 1_555 ?
C30 O30 2.3936(3) 1_555 ?
C31 C32 1.4067(2) 1_555 ?
C31 O31 1.22562(14 1_555 ?
C31 O32 1.25807(13 1_555 ?
C32 C31 1.4067(2) 1_555 ?
C32 O31 2.3651(3) 1_555 ?
C32 O32 2.3340(3) 1_555 ?
C33 C34 1.5095(2) 1_555 ?
C33 O33 1.22107(18 1_555 ?
C33 O34 1.19164(12 1_555 ?
C33 Pb09 2.8933(4) 1_555 ?
C34 C33 1.5095(2) 1_555 ?
C34 O33 2.3448(3) 1_555 ?
C34 O34 2.3250(3) 1_555 ?
C35 C36 1.4664(2) 1_555 ?
C35 O35 1.20450(14 1_555 ?
C35 O36 1.29403(14 1_555 ?
C36 C35 1.4664(2) 1_555 ?
C36 O35 2.3975(3) 1_555 ?
C36 O36 2.3618(3) 1_555 ?
C37 C38 1.53132(19 1_555 ?
C37 O37 1.29301(13 1_555 ?
C37 O38 1.22197(17 1_555 ?
C37 Pb10 2.9943(4) 1_555 ?
C38 C37 1.53132(19 1_555 ?
C38 O37 2.3348(3) 1_555 ?
C38 O38 2.3981(3) 1_555 ?
C39 C40 1.4904(2) 1_555 ?
C39 O39 1.20780(13 1_555 ?
C39 O40 1.30816(15 1_555 ?
C39 Pb10 3.0204(4) 1_555 ?
C40 C39 1.4904(2) 1_555 ?
C40 O39 2.3495(3) 1_555 ?
C40 O40 2.4315(3) 1_555 ?
O1 C1 1.23133(15 1_555 ?
O1 C2 2.3629(4) 1_555 ?
O1 C16 3.0888(4) 1_555 ?
O1 O2 2.1799(3) 1_555 ?
O1 Pb01 2.4762(3) 1_555 ?
O2 C1 1.25729(19 1_555 ?
O2 C2 2.3778(3) 1_555 ?
O2 O1 2.1799(3) 1_555 ?
O2 O4 3.0238(3) 1_555 ?
O2 Pb01 2.4721(4) 1_555 ?
O2 Pb02 2.7880(3) 1_555 ?
O3 C3 1.25312(15 1_555 ?
O3 C4 2.3712(3) 1_555 ?
O3 O4 2.1804(3) 1_555 ?
O3 O12 2.9401(4) 2_547 ?
O3 Pb01 2.8002(4) 1_555 ?
O3 Pb03 2.5904(4) 2_547 ?
O4 C3 1.17236(13 1_555 ?
O4 C4 2.3295(3) 1_555 ?
O4 O2 3.0238(3) 1_555 ?
O4 O3 2.1804(3) 1_555 ?
O4 Pb01 2.6772(3) 1_555 ?
O4 Pb03 2.5955(4) 2_557 ?
O5 C5 1.22514(14 1_555 ?
O5 C6 2.3019(4) 1_555 ?
O5 O6 2.1854(3) 1_555 ?
O5 Pb02 2.4648(3) 1_555 ?
O6 C5 1.26424(19 1_555 ?
O6 C6 2.4006(3) 1_555 ?
O6 O5 2.1854(3) 1_555 ?
O6 Pb02 2.4633(4) 1_555 ?
O6 Pb03 2.6933(4) 1_555 ?
O7 C7 1.28812(15 1_555 ?
O7 C8 2.4417(3) 1_555 ?
O7 O8 2.1300(3) 1_555 ?
O7 O27 2.9094(4) 1_555 ?
O7 Pb04 2.4796(4) 1_555 ?
O7 PbO7 2.6662(3) 1_555 ?
O8 C7 1.19085(15 1_555 ?
O8 C8 2.3085(3) 1_555 ?
O8 O7 2.1300(3) 1_555 ?
O8 O28 2.9772(4) 1_545 ?
O8 Pb04 2.5572(4) 1_545 ?
O8 PbO7 2.8315(4) 1_555 ?
O9 C9 1.28371(12 1_555 ?
O9 C10 2.3272(3) 1_555 ?
O9 O10 2.1995(2) 1_555 ?
O9 Pb03 2.2522(3) 1_555 ?
O10 C9 1.19737(17 1_555 ?
O10 C10 2.3477(3) 1_555 ?
O10 O9 2.1995(2) 1_555 ?
O10 Pb03 3.0920(4) 1_555 ?
O10 Pb06 2.8863(3) 2_547 ?
O11 C11 1.27983(16 1_555 ?
O11 C12 2.4261(3) 1_555 ?
O11 O12 2.1275(3) 1_555 ?
O11 Pb01 2.5294(4) 2_547 ?
O11 Pb03 2.7522(4) 1_555 ?
O12 C11 1.16123(13 1_555 ?
O12 C12 2.3568(3) 1_555 ?
O12 O3 2.9401(4) 2_557 ?
O12 O11 2.1275(3) 1_555 ?
O12 Pb01 2.6226(4) 2_557 ?
O12 Pb03 2.4941(3) 1_555 ?
O13 C13 1.13866(13 1_555 ?
O13 C14 2.2912(3) 1_555 ?
O13 O14 2.0439(3) 1_555 ?
O13 O14 2.9529(4) 2_547 ?
O13 Pb02 2.5232(4) 1_545 ?
O13 Pb02 2.7071(4) 2_547 ?
O14 C13 1.25505(16 1_555 ?
O14 C14 2.4020(3) 1_555 ?
O14 O13 2.0439(3) 1_555 ?
O14 O13 2.9529(4) 2_557 ?
O14 Pb02 2.5537(4) 1_555 ?
O14 Pb02 2.7904(4) 2_547 ?
O15 C15 1.27069(18 1_555 ?
O15 C16 2.3230(3) 1_555 ?
O15 O16 2.2392(2) 1_555 ?
O15 O21 3.0975(4) 1_555 ?
O15 Pb01 2.8443(3) 1_555 ?
O16 C15 1.25623(12 1_555 ?
O16 C16 2.3349(3) 1_555 ?
O16 O15 2.2392(2) 1_555 ?
O16 Pb05 2.2794(3) 1_555 ?
O17 C17 1.17282(14 1_555 ?
O17 C18 2.2845(3) 1_555 ?
O17 O18 2.1543(3) 1_555 ?
O17 O22 2.8931(3) 1_565 ?
O17 Pb05 2.6039(4) 1_565 ?
O17 Pb06 2.6769(3) 1_555 ?
O18 C17 1.30384(14 1_555 ?
O18 C18 2.3592(3) 1_555 ?
O18 O17 2.1543(3) 1_555 ?
O18 O20 2.9103(3) 1_555 ?
O18 O21 2.9885(4) 1_555 ?
O18 Pb05 2.5347(4) 1_555 ?
O18 Pb06 2.5869(3) 1_555 ?
O19 C19 1.20427(15 1_555 ?
O19 C20 2.3564(4) 1_555 ?
O19 O20 2.1302(3) 1_555 ?
O19 Pb06 2.4486(3) 1_555 ?
O20 C19 1.25194(19 1_555 ?
O20 C20 2.3196(3) 1_555 ?
O20 O18 2.9103(3) 1_555 ?
O20 O19 2.1302(3) 1_555 ?
O20 Pb04 2.8542(4) 1_555 ?
O20 Pb06 2.4707(4) 1_555 ?
O21 C21 1.25801(14 1_555 ?
O21 C22 2.3954(3) 1_555 ?
O21 O15 3.0975(4) 1_555 ?
O21 O18 2.9885(4) 1_555 ?
O21 O22 2.1853(3) 1_555 ?
O21 Pb05 2.6837(4) 1_555 ?
O21 Pb06 2.5952(4) 1_555 ?
O22 C21 1.27409(14 1_555 ?
O22 C22 2.3460(3) 1_555 ?
O22 O17 2.8931(3) 1_545 ?
O22 O21 2.1853(3) 1_555 ?
O22 Pb05 2.5616(3) 1_555 ?
O22 Pb06 2.5806(4) 1_545 ?
O23 C23 1.21229(18 1_555 ?
O23 C24 2.3210(3) 1_555 ?
O23 O24 2.1310(3) 1_555 ?
O23 Pb05 2.7372(4) 1_555 ?
O23 PbO7 2.5147(4) 1_555 ?
O24 C23 1.22796(14 1_555 ?
O24 C24 2.3579(4) 1_555 ?
O24 O23 2.1310(3) 1_555 ?
O24 PbO7 2.4681(3) 1_555 ?
O25 C25 1.28781(19 1_555 ?
O25 C26 2.4113(3) 1_555 ?
O25 O26 2.1781(3) 1_555 ?
O25 O32 3.0352(3) 1_555 ?
O25 PbO7 2.7604(3) 1_555 ?
O25 Pb08 2.4228(4) 1_555 ?
O26 C25 1.24449(15 1_555 ?
O26 C26 2.3677(4) 1_555 ?
O26 O25 2.1781(3) 1_555 ?
O26 Pb08 2.4804(3) 1_555 ?
O27 C27 1.21832(15 1_555 ?
O27 C28 2.2567(3) 1_555 ?
O27 O7 2.9094(4) 1_555 ?
O27 O28 2.1207(3) 1_555 ?
O27 Pb04 2.8255(4) 1_555 ?
O27 PbO7 2.5856(4) 1_555 ?
O28 C27 1.21450(14 1_555 ?
O28 C28 2.3943(3) 1_555 ?
O28 O8 2.9772(4) 1_565 ?
O28 O27 2.1207(3) 1_555 ?
O28 O30 3.0617(3) 1_555 ?
O28 Pb04 2.6914(3) 1_555 ?
O28 PbO7 2.5098(4) 1_565 ?
O29 C29 1.21512(15 1_555 ?
O29 C30 2.3723(4) 1_555 ?
O29 O30 2.1121(3) 1_555 ?
O29 Pb04 2.4276(3) 1_555 ?
O30 C29 1.29038(19 1_555 ?
O30 C30 2.3936(3) 1_555 ?
O30 O28 3.0617(3) 1_555 ?
O30 O29 2.1121(3) 1_555 ?
O30 Pb04 2.4181(4) 1_555 ?
O30 Pb09 2.7109(3) 1_555 ?
O31 C31 1.22562(14 1_555 ?
O31 C32 2.3651(3) 1_555 ?
O31 O32 2.0284(3) 1_555 ?
O31 O36 2.8643(3) 1_555 ?
O31 Pb08 2.6956(4) 1_555 ?
O31 Pb09 2.6329(4) 1_555 ?
O32 C31 1.25807(13 1_555 ?
O32 C32 2.3340(3) 1_555 ?
O32 O25 3.0352(3) 1_555 ?
O32 O31 2.0284(3) 1_555 ?
O32 Pb08 2.6815(3) 1_555 ?
O32 Pb09 2.5333(4) 1_545 ?
O33 C33 1.22107(18 1_555 ?
O33 C34 2.3448(3) 1_555 ?
O33 O34 2.1263(3) 1_555 ?
O33 O35 3.0950(4) 1_555 ?
O33 Pb09 2.7604(4) 1_555 ?
O33 Pb10 2.8510(4) 1_555 ?
O34 C33 1.19164(12 1_555 ?
O34 C34 2.3250(3) 1_555 ?
O34 O33 2.1263(3) 1_555 ?
O34 Pb09 2.3569(3) 1_555 ?
O35 C35 1.20450(14 1_555 ?
O35 C36 2.3975(3) 1_555 ?
O35 O33 3.0950(4) 1_555 ?
O35 O36 2.1080(3) 1_555 ?
O35 Pb08 2.5533(4) 1_565 ?
O35 Pb09 2.7489(4) 1_555 ?
O36 C35 1.29403(14 1_555 ?
O36 C36 2.3618(3) 1_555 ?
O36 O31 2.8643(3) 1_555 ?
O36 O35 2.1080(3) 1_555 ?
O36 Pb08 2.5497(4) 1_555 ?
O36 Pb09 2.6284(3) 1_555 ?
O37 C37 1.29301(13 1_555 ?
O37 C38 2.3348(3) 1_555 ?
O37 O38 2.2567(3) 1_555 ?
O37 Pb10 2.2847(3) 1_555 ?
O38 C37 1.22197(17 1_555 ?
O38 C38 2.3981(3) 1_555 ?
O38 O37 2.2567(3) 1_555 ?
O38 Pb08 2.8051(3) 2_756 ?
O38 Pb10 3.0759(4) 1_555 ?
O39 C39 1.20780(13 1_555 ?
O39 C40 2.3495(3) 1_555 ?
O39 O40 2.1653(3) 1_555 ?
O39 O40 3.0501(4) 2_756 ?
O39 Pb10 2.5239(3) 1_555 ?
O39 Pb10 2.6356(4) 2_756 ?
O40 C39 1.30816(15 1_555 ?
O40 C40 2.4315(3) 1_555 ?
O40 O39 2.1653(3) 1_555 ?
O40 O39 3.0501(4) 2_746 ?
O40 Pb10 2.7220(4) 1_555 ?
O40 Pb10 2.6194(4) 2_746 ?
Pb01 C1 2.8185(4) 1_555 ?
Pb01 C3 3.0367(5) 1_555 ?
Pb01 O1 2.4762(3) 1_555 ?
Pb01 O2 2.4721(4) 1_555 ?
Pb01 O3 2.8002(4) 1_555 ?
Pb01 O4 2.6772(3) 1_555 ?
Pb01 O11 2.5294(4) 2_557 ?
Pb01 O12 2.6226(4) 2_547 ?
Pb01 O15 2.8443(3) 1_555 ?
Pb02 C5 2.8030(4) 1_555 ?
Pb02 O2 2.7880(3) 1_555 ?
Pb02 O5 2.4648(3) 1_555 ?
Pb02 O6 2.4633(4) 1_555 ?
Pb02 O13 2.5232(4) 1_565 ?
Pb02 O13 2.7071(4) 2_557 ?
Pb02 O14 2.5537(4) 1_555 ?
Pb02 O14 2.7904(4) 2_557 ?
Pb03 C9 3.0143(4) 1_555 ?
Pb03 C11 2.9840(4) 1_555 ?
Pb03 O3 2.5904(4) 2_557 ?
Pb03 O4 2.5955(4) 2_547 ?
Pb03 O6 2.6933(4) 1_555 ?
Pb03 O9 2.2522(3) 1_555 ?
Pb03 O10 3.0920(4) 1_555 ?
Pb03 O11 2.7522(4) 1_555 ?
Pb03 O12 2.4941(3) 1_555 ?
Pb04 C29 2.8542(4) 1_555 ?
Pb04 O7 2.4796(4) 1_555 ?
Pb04 O8 2.5572(4) 1_565 ?
Pb04 O20 2.8542(4) 1_555 ?
Pb04 O27 2.8255(4) 1_555 ?
Pb04 O28 2.6914(3) 1_555 ?
Pb04 O29 2.4276(3) 1_555 ?
Pb04 O30 2.4181(4) 1_555 ?
Pb05 C15 3.0401(4) 1_555 ?
Pb05 C21 3.0239(4) 1_555 ?
Pb05 O16 2.2794(3) 1_555 ?
Pb05 O17 2.6039(4) 1_545 ?
Pb05 O18 2.5347(4) 1_555 ?
Pb05 O21 2.6837(4) 1_555 ?
Pb05 O22 2.5616(3) 1_555 ?
Pb05 O23 2.7372(4) 1_555 ?
Pb06 C17 2.9916(4) 1_555 ?
Pb06 C19 2.8281(4) 1_555 ?
Pb06 O10 2.8863(3) 2_557 ?
Pb06 O17 2.6769(3) 1_555 ?
Pb06 O18 2.5869(3) 1_555 ?
Pb06 O19 2.4486(3) 1_555 ?
Pb06 O20 2.4707(4) 1_555 ?
Pb06 O21 2.5952(4) 1_555 ?
Pb06 O22 2.5806(4) 1_565 ?
PbO7 C23 2.8464(4) 1_555 ?
PbO7 O7 2.6662(3) 1_555 ?
PbO7 O8 2.8315(4) 1_555 ?
PbO7 O23 2.5147(4) 1_555 ?
PbO7 O24 2.4681(3) 1_555 ?
PbO7 O25 2.7604(3) 1_555 ?
PbO7 O27 2.5856(4) 1_555 ?
PbO7 O28 2.5098(4) 1_545 ?
Pb08 C25 2.8426(4) 1_555 ?
Pb08 O25 2.4228(4) 1_555 ?
Pb08 O26 2.4804(3) 1_555 ?
Pb08 O31 2.6956(4) 1_555 ?
Pb08 O32 2.6815(3) 1_555 ?
Pb08 O35 2.5533(4) 1_545 ?
Pb08 O36 2.5497(4) 1_555 ?
Pb08 O38 2.8051(3) 2_746 ?
Pb09 C33 2.8933(4) 1_555 ?
Pb09 O30 2.7109(3) 1_555 ?
Pb09 O31 2.6329(4) 1_555 ?
Pb09 O32 2.5333(4) 1_565 ?
Pb09 O33 2.7604(4) 1_555 ?
Pb09 O34 2.3569(3) 1_555 ?
Pb09 O35 2.7489(4) 1_555 ?
Pb09 O36 2.6284(3) 1_555 ?
Pb10 C37 2.9943(4) 1_555 ?
Pb10 C39 3.0204(4) 1_555 ?
Pb10 O33 2.8510(4) 1_555 ?
Pb10 O37 2.2847(3) 1_555 ?
Pb10 O38 3.0759(4) 1_555 ?
Pb10 O39 2.5239(3) 1_555 ?
Pb10 O39 2.6356(4) 2_746 ?
Pb10 O40 2.7220(4) 1_555 ?
Pb10 O40 2.6194(4) 2_756 ?

_cod_database_fobs_code 4300009
