#------------------------------------------------------------------------------ #$Date: 2025-07-01 16:05:22 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1354 $ #$URL: svn://localhost/testcod/cif/4/10/00/4100035.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4100035 loop_ _publ_author_name 'Lozinska, Magdalena M.' 'Mangano, Enzo' 'Mowat, John P. S.' 'Shepherd, Ashley M.' 'Howe, Russell F.' 'Thompson, Stephen P.' 'Parker, Julia E.' 'Brandani, Stefano' 'Wright, Paul A.' _publ_section_title ; Understanding Carbon Dioxide Adsorption on Univalent Cation Forms of the Flexible Zeolite Rho at Conditions Relevant to Carbon Capture from Flue Gases ; _journal_issue 42 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 17628 _journal_page_last 17642 _journal_paper_doi 10.1021/ja3070864 _journal_volume 134 _journal_year 2012 _chemical_formula_sum 'C0.11 Al0.1 Na0.1 O1.21 Si0.4' _chemical_formula_weight 36.77 _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _symmetry_cell_setting cubic _symmetry_space_group_name_H-M 'I -4 3 m' _audit_creation_date 2012-07-11T15:51 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2012-07-11T15:51 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_formula_units_Z 96 _cell_length_a 14.62823(6) _cell_length_b 14.62823 _cell_length_c 14.62823 _cell_measurement_temperature 298 _cell_volume 3130.223(13) _computing_structure_refinement GSAS _diffrn_ambient_temperature 298 _diffrn_measurement_device_type synchrotron _diffrn_radiation_polarisn_ratio 0.93 _diffrn_radiation_probe x-ray _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.827159 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _pd_block_id 2012-07-11T15:51|Na-Rho-CO2|jpsm|i11 _pd_calc_method 'Rietveld Refinement' _pd_char_colour white _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.005 _pd_meas_2theta_range_max 49.9975 _pd_meas_2theta_range_min 2.0025 _pd_meas_number_of_points 9600 _pd_phase_name 'from C:/Users/john/Dropbox/Magda/MML269b_Diamond/MML269b/HRho.EXP' _pd_proc_2theta_range_inc 0.005 _pd_proc_2theta_range_max 49.99751 _pd_proc_2theta_range_min 2.00251 _pd_proc_info_datetime 2012-07-11T15:51:05 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 7 with 20 terms. Linear interpolation 1: 896.332 2: 448.465 3: 387.081 4: 511.711 5: 745.954 6: 477.094 7: 339.866 8: 305.147 9: 256.885 10: 259.714 11: 254.890 12: 258.733 13: 245.839 14: 268.459 15: 266.766 16: 234.996 17: 201.100 18: 169.492 19: 156.853 20: 152.622 ; _pd_proc_ls_peak_cutoff 0.00085 _pd_proc_ls_profile_function ; CW Profile function number 3 with 19 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. #1(GU) = 47.263 #2(GV) = -1.014 #3(GW) = 1.032 #4(GP) = 0.000 #5(LX) = 0.532 #6(LY) = 2.000 #7(S/L) = 0.0070 #8(H/L) = 0.0008 #9(trns) = 0.00 #10(shft)= 0.0000 #11(stec)= 0.00 #12(ptec)= 0.00 #13(sfec)= 0.00 #14(L11) = 0.102 #15(L22) = 0.122 #16(L33) = 0.127 #17(L12) = 0.034 #18(L13) = -0.014 #19(L23) = 0.010 Peak tails are ignored where the intensity is below 0.0009 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0559 _pd_proc_ls_prof_wR_expected 0.0296 _pd_proc_ls_prof_wR_factor 0.0712 _pd_proc_number_of_points 9600 _pd_spec_mounting ' ?' _refine_ls_goodness_of_fit_all 2.43 _refine_ls_matrix_type full _refine_ls_number_parameters 23 _refine_ls_number_restraints 7 _refine_ls_R_Fsqd_factor 0.07395 _refine_ls_shift/su_max 0.03 _refine_ls_shift/su_mean 0.01 _reflns_d_resolution_high 0.982 _reflns_d_resolution_low 10.344 _reflns_limit_h_max 15 _reflns_limit_h_min 1 _reflns_limit_k_max 10 _reflns_limit_k_min 0 _reflns_limit_l_max 8 _reflns_limit_l_min 0 _reflns_number_total 204 _cod_data_source_file ja3070864_si_002.cif _cod_data_source_block Na-Rho-CO2_publ _cod_original_cell_volume 3130.23(4) _cod_original_formula_sum 'C0.11 Al0.10 Na0.10 O1.21 Si0.40' _cod_database_code 4100035 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 +z,+x,+y 3 +y,+z,+x 4 +y,-x,-z 5 -z,+y,-x 6 -x,-z,+y 7 -x,-y,+z 8 -z,+x,-y 9 -y,-z,+x 10 +x,-y,-z 11 +z,-x,-y 12 -y,+z,-x 13 -y,+x,-z 14 -z,-y,+x 15 +x,-z,-y 16 +x,+z,+y 17 +y,+x,+z 18 +z,+y,+x 19 +y,-z,-x 20 -y,-x,+z 21 +z,-y,-x 22 -x,+z,-y 23 -x,+y,-z 24 -z,-x,+y 101 +x+1/2,+y+1/2,+z+1/2 102 +z+1/2,+x+1/2,+y+1/2 103 +y+1/2,+z+1/2,+x+1/2 104 +y+1/2,-x+1/2,-z+1/2 105 -z+1/2,+y+1/2,-x+1/2 106 -x+1/2,-z+1/2,+y+1/2 107 -x+1/2,-y+1/2,+z+1/2 108 -z+1/2,+x+1/2,-y+1/2 109 -y+1/2,-z+1/2,+x+1/2 110 +x+1/2,-y+1/2,-z+1/2 111 +z+1/2,-x+1/2,-y+1/2 112 -y+1/2,+z+1/2,-x+1/2 113 -y+1/2,+x+1/2,-z+1/2 114 -z+1/2,-y+1/2,+x+1/2 115 +x+1/2,-z+1/2,-y+1/2 116 +x+1/2,+z+1/2,+y+1/2 117 +y+1/2,+x+1/2,+z+1/2 118 +z+1/2,+y+1/2,+x+1/2 119 +y+1/2,-z+1/2,-x+1/2 120 -y+1/2,-x+1/2,+z+1/2 121 +z+1/2,-y+1/2,-x+1/2 122 -x+1/2,+z+1/2,-y+1/2 123 -x+1/2,+y+1/2,-z+1/2 124 -z+1/2,-x+1/2,+y+1/2 loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Si Si1 0.26879(10) 0.11856(12) 0.41920(11) 0.8 Uiso 0.00642(24) 48 Al Al1 0.26806(10) 0.11889(12) 0.41992(11) 0.2 Uiso 0.00642(24) 48 O O1 0.03021(21) 0.20921(18) 0.38306(24) 1.0 Uiso 0.0085(5) 48 O O2 0.20918(22) 0.20918(22) 0.39165(35) 1.0 Uiso 0.0085(5) 24 O O3 0.12759(21) 0.12759(21) 0.62741(33) 1.0 Uiso 0.0085(5) 24 Na Na1 0.3084(6) 0.3084(6) 0.3084(6) 0.4 Uiso 0.0530(25) 8 Na Na3 0.4408(5) 0.0 0.0 0.5 Uiso 0.0530(25) 12 O OC1 0.3828(7) 0.0 0.0 0.5 Uiso 0.0530(25) 12 O OC2 0.2306(7) 0.0 0.0 0.5 Uiso 0.0530(25) 12 C CO1 0.3074(7) 0.0 0.0 0.5 Uiso 0.0530(25) 12 O OC3 0.3683(7) 0.4863(15) 0.3683(7) 0.17101 Uiso 0.0530(25) 24 C CO2 0.3489(7) 0.5597(15) 0.3711(18) 0.08551 Uiso 0.0530(25) 48 O OC4 0.3206(7) 0.6306(15) 0.3849(18) 0.08551 Uiso 0.0530(25) 48 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Si 38.4 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100 81.6937 1.14070 International_Tables_Vol_C Al 9.6 0.000 0.000 6.42020 3.03870 1.90020 0.74260 1.59360 31.5472 1.96460 85.0886 1.11510 International_Tables_Vol_C O 116.209 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C Na 9.2 0.000 0.000 4.76260 3.28500 3.17360 8.84220 1.26740 0.31360 1.11280 129.424 0.67600 International_Tables_Vol_C C 10.104 0.000 0.000 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500 51.6512 0.21560 International_Tables_Vol_C loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Al1 Si1 O1 95.59(13) 1_555 . 17_555 N Al1 Si1 O1 58.98(11) 1_555 . 109_555 N Al1 Si1 O2 63.28(19) 1_555 . 1_555 N Al1 Si1 O3 150.01(19) 1_555 . 112_545 N O1 Si1 O1 114.00(26) 17_555 . 109_555 N O1 Si1 O2 105.94(19) 17_555 . 1_555 N O1 Si1 O3 114.22(27) 17_555 . 112_545 N O1 Si1 O2 110.89(26) 109_555 . 1_555 N O1 Si1 O3 103.11(20) 109_555 . 112_545 N O2 Si1 O3 108.67(26) 1_555 . 112_545 N Si1 Al1 O1 83.87(13) 1_555 . 17_555 N Si1 Al1 O1 120.56(11) 1_555 . 109_555 N Si1 Al1 O2 116.23(19) 1_555 . 1_555 N Si1 Al1 O3 29.72(19) 1_555 . 112_545 N Si1 Al1 Na1 78.98(6) 1_555 . 1_555 N O1 Al1 O1 114.35(27) 17_555 . 109_555 N O1 Al1 O2 106.19(19) 17_555 . 1_555 N O1 Al1 O3 113.42(27) 17_555 . 112_545 N O1 Al1 Na1 126.75(28) 17_555 . 1_555 N O1 Al1 O2 111.66(26) 109_555 . 1_555 N O1 Al1 O3 102.87(20) 109_555 . 112_545 N O1 Al1 Na1 117.84(31) 109_555 . 1_555 N O2 Al1 O3 108.34(26) 1_555 . 112_545 N O2 Al1 Na1 44.10(18) 1_555 . 1_555 N O3 Al1 Na1 64.36(17) 112_545 . 1_555 N Si1 O1 Si1 132.20(20) 17_555 . 111_455 N Si1 O1 Al1 0.0 17_555 . 17_555 N Si1 O1 Al1 131.88(20) 17_555 . 111_455 N Si1 O1 Al1 132.48(20) 111_455 . 17_555 N Si1 O1 Al1 0.0 111_455 . 111_455 N Al1 O1 Al1 132.16(20) 17_555 . 111_455 N Si1 O2 Si1 143.3(4) 1_555 . 17_555 N Si1 O2 Al1 0.0 1_555 . 1_555 N Si1 O2 Al1 142.8(4) 1_555 . 17_555 N Si1 O2 Na1 107.11(18) 1_555 . 1_555 N Si1 O2 Al1 142.8(4) 17_555 . 1_555 N Si1 O2 Al1 0.0 17_555 . 17_555 N Si1 O2 Na1 107.11(18) 17_555 . 1_555 N Al1 O2 Al1 142.4(4) 1_555 . 17_555 N Al1 O2 Na1 107.51(18) 1_555 . 1_555 N Al1 O2 Na1 107.51(18) 17_555 . 1_555 N Si1 O3 Si1 137.70(34) 106_555 . 124_555 N Si1 O3 Al1 0.0 106_555 . 106_555 N Si1 O3 Al1 137.91(33) 106_555 . 124_555 N Si1 O3 Al1 137.91(33) 124_555 . 106_555 N Si1 O3 Al1 0.0 124_555 . 124_555 N Al1 O3 Al1 138.12(33) 106_555 . 124_555 N Al1 Na1 Al1 111.11(24) 1_555 . 2_555 N Al1 Na1 Al1 111.11(24) 1_555 . 3_555 N Al1 Na1 Al1 144.4(5) 1_555 . 16_555 N Al1 Na1 Al1 56.31(11) 1_555 . 17_555 N Al1 Na1 Al1 57.42(10) 1_555 . 18_555 N Al1 Na1 O2 28.39(5) 1_555 . 1_555 N Al1 Na1 O2 83.11(20) 1_555 . 2_555 N Al1 Na1 O2 128.8(5) 1_555 . 3_555 N Al1 Na1 Al1 111.11(24) 2_555 . 3_555 N Al1 Na1 Al1 57.42(10) 2_555 . 16_555 N Al1 Na1 Al1 144.4(5) 2_555 . 17_555 N Al1 Na1 Al1 56.31(11) 2_555 . 18_555 N Al1 Na1 O2 128.8(5) 2_555 . 1_555 N Al1 Na1 O2 28.39(5) 2_555 . 2_555 N Al1 Na1 O2 83.11(20) 2_555 . 3_555 N Al1 Na1 Al1 56.31(11) 3_555 . 16_555 N Al1 Na1 Al1 57.42(10) 3_555 . 17_555 N Al1 Na1 Al1 144.4(5) 3_555 . 18_555 N Al1 Na1 O2 83.11(20) 3_555 . 1_555 N Al1 Na1 O2 128.8(5) 3_555 . 2_555 N Al1 Na1 O2 28.39(5) 3_555 . 3_555 N Al1 Na1 Al1 111.11(24) 16_555 . 17_555 N Al1 Na1 Al1 111.11(24) 16_555 . 18_555 N Al1 Na1 O2 128.8(5) 16_555 . 1_555 N Al1 Na1 O2 83.11(20) 16_555 . 2_555 N Al1 Na1 O2 28.39(5) 16_555 . 3_555 N Al1 Na1 Al1 111.11(24) 17_555 . 18_555 N Al1 Na1 O2 28.39(5) 17_555 . 1_555 N Al1 Na1 O2 128.8(5) 17_555 . 2_555 N Al1 Na1 O2 83.11(20) 17_555 . 3_555 N Al1 Na1 O2 83.11(20) 18_555 . 1_555 N Al1 Na1 O2 28.39(5) 18_555 . 2_555 N Al1 Na1 O2 128.8(5) 18_555 . 3_555 N O2 Na1 O2 104.5(4) 1_555 . 2_555 N O2 Na1 O2 104.5(4) 1_555 . 3_555 N O2 Na1 O2 104.5(4) 2_555 . 3_555 N Na3 Na3 OC1 180.0 6_655 . 1_555 N Na3 Na3 OC1 0.0 6_655 . 6_655 N Na3 Na3 CO1 180.0 6_655 . 1_555 N OC1 Na3 OC1 180.0 1_555 . 6_655 N OC1 Na3 CO1 0.0 1_555 . 1_555 N OC1 Na3 CO1 180.0 6_655 . 1_555 N Na3 OC1 Na3 0.0 1_555 . 6_655 N Na3 OC1 CO1 180.0 1_555 . 1_555 N Na3 OC1 CO1 180.0 6_655 . 1_555 N Na3 CO1 OC1 0.0 1_555 . 1_555 N Na3 CO1 OC2 180.0 1_555 . 1_555 N OC1 CO1 OC2 180.0 1_555 . 1_555 N CO2 OC3 CO2 23.9(23) 1_555 . 18_555 N OC3 CO2 CO2 111.4(13) 1_555 . 9_665 N OC3 CO2 CO2 136.9(14) 1_555 . 11_566 N OC3 CO2 CO2 135.2(16) 1_555 . 15_566 N OC3 CO2 CO2 78.1(12) 1_555 . 18_555 N OC3 CO2 OC4 169.4(12) 1_555 . 1_555 N OC3 CO2 OC4 126.7(33) 1_555 . 9_665 N OC3 CO2 OC4 167.2(22) 1_555 . 15_566 N OC3 CO2 OC4 127.6(26) 1_555 . 18_555 N OC3 CO2 OC4 155.2(7) 1_555 . 20_665 N CO2 CO2 CO2 60.00000(20) 9_665 . 11_566 N CO2 CO2 CO2 73.5(15) 9_665 . 15_566 N CO2 CO2 CO2 46.5(15) 9_665 . 18_555 N CO2 CO2 OC4 77.2(11) 9_665 . 1_555 N CO2 CO2 OC4 41.2(12) 9_665 . 9_665 N CO2 CO2 OC4 79.8(14) 9_665 . 15_566 N CO2 CO2 OC4 32.1(7) 9_665 . 18_555 N CO2 CO2 OC4 46.4(15) 9_665 . 20_665 N CO2 CO2 CO2 13.5(15) 11_566 . 15_566 N CO2 CO2 CO2 106.5(15) 11_566 . 18_555 N CO2 CO2 OC4 41.3(4) 11_566 . 1_555 N CO2 CO2 OC4 77.1(13) 11_566 . 9_665 N CO2 CO2 OC4 53.6(29) 11_566 . 15_566 N CO2 CO2 OC4 69.87(29) 11_566 . 18_555 N CO2 CO2 OC4 30.1(9) 11_566 . 20_665 N CO2 CO2 CO2 120.00000(20) 15_566 . 18_555 N CO2 CO2 OC4 39.49220(10) 15_566 . 1_555 N CO2 CO2 OC4 87.5(24) 15_566 . 9_665 N CO2 CO2 OC4 52.4(28) 15_566 . 15_566 N CO2 CO2 OC4 81.2(11) 15_566 . 18_555 N CO2 CO2 OC4 39.46(23) 15_566 . 20_665 N CO2 CO2 OC4 112.5421 18_555 . 1_555 N CO2 CO2 OC4 49.7(16) 18_555 . 9_665 N CO2 CO2 OC4 107.6(12) 18_555 . 15_566 N CO2 CO2 OC4 49.5(14) 18_555 . 18_555 N CO2 CO2 OC4 87.8(5) 18_555 . 20_665 N OC4 CO2 OC4 63.9(19) 1_555 . 9_665 N OC4 CO2 OC4 12.9(28) 1_555 . 15_566 N OC4 CO2 OC4 63.0(14) 1_555 . 18_555 N OC4 CO2 OC4 31.4(7) 1_555 . 20_665 N OC4 CO2 OC4 57.8(11) 9_665 . 15_566 N OC4 CO2 OC4 9.7(19) 9_665 . 18_555 N OC4 CO2 OC4 48.0(24) 9_665 . 20_665 N OC4 CO2 OC4 59.3(10) 15_566 . 18_555 N OC4 CO2 OC4 37.6(14) 15_566 . 20_665 N OC4 CO2 OC4 42.2(13) 18_555 . 20_665 N CO2 OC4 CO2 97.5(15) 1_555 . 11_566 N CO2 OC4 CO2 88.1(28) 1_555 . 15_566 N CO2 OC4 CO2 18.0(14) 1_555 . 18_555 N CO2 OC4 CO2 77.1(7) 1_555 . 20_665 N CO2 OC4 OC4 58.2(15) 1_555 . 9_665 N CO2 OC4 OC4 102.9(17) 1_555 . 11_566 N CO2 OC4 OC4 39.49220(10) 1_555 . 15_566 N CO2 OC4 OC4 67.4579 1_555 . 18_555 N CO2 OC4 OC4 112.8518 1_555 . 20_665 N CO2 OC4 CO2 22.7(25) 11_566 . 15_566 N CO2 OC4 CO2 97.0(20) 11_566 . 18_555 N CO2 OC4 CO2 53.1(23) 11_566 . 20_665 N CO2 OC4 OC4 102.8(11) 11_566 . 9_665 N CO2 OC4 OC4 57.9(13) 11_566 . 11_566 N CO2 OC4 OC4 133.7(19) 11_566 . 15_566 N CO2 OC4 OC4 92.5(24) 11_566 . 18_555 N CO2 OC4 OC4 49.7(16) 11_566 . 20_665 N CO2 OC4 CO2 94.3(23) 15_566 . 18_555 N CO2 OC4 CO2 70.1(6) 15_566 . 20_665 N CO2 OC4 OC4 114.9(6) 15_566 . 9_665 N CO2 OC4 OC4 80.1(20) 15_566 . 11_566 N CO2 OC4 OC4 127.6(28) 15_566 . 15_566 N CO2 OC4 OC4 107.9(12) 15_566 . 18_555 N CO2 OC4 OC4 72.4(12) 15_566 . 20_665 N CO2 OC4 CO2 63.8(12) 18_555 . 20_665 N CO2 OC4 OC4 40.6(24) 18_555 . 9_665 N CO2 OC4 OC4 87.4(28) 18_555 . 11_566 N CO2 OC4 OC4 36.65(7) 18_555 . 15_566 N CO2 OC4 OC4 49.5(14) 18_555 . 18_555 N CO2 OC4 OC4 98.8(11) 18_555 . 20_665 N CO2 OC4 OC4 50.4(16) 20_665 . 9_665 N CO2 OC4 OC4 27.5(8) 20_665 . 11_566 N CO2 OC4 OC4 92.2(5) 20_665 . 15_566 N CO2 OC4 OC4 39.46(23) 20_665 . 18_555 N CO2 OC4 OC4 35.8(7) 20_665 . 20_665 N OC4 OC4 OC4 60.0 9_665 . 11_566 N OC4 OC4 OC4 46.7(22) 9_665 . 15_566 N OC4 OC4 OC4 13.3(22) 9_665 . 18_555 N OC4 OC4 OC4 73.3(22) 9_665 . 20_665 N OC4 OC4 OC4 106.7(22) 11_566 . 15_566 N OC4 OC4 OC4 46.7(22) 11_566 . 18_555 N OC4 OC4 OC4 13.3(22) 11_566 . 20_665 N OC4 OC4 OC4 60.00000(20) 15_566 . 18_555 N OC4 OC4 OC4 119.99990(10) 15_566 . 20_665 N OC4 OC4 OC4 60.00000(10) 18_555 . 20_665 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si1 Si1 3.0186(26) . 106_555 N Si1 Si1 3.0186(26) . 122_545 N Si1 Al1 0.01569 . 1_555 N Si1 Al1 3.0969(28) . 17_555 N Si1 Al1 3.0233(26) . 106_555 N Si1 Al1 3.0075(26) . 122_545 N Si1 O1 1.6460(32) . 17_555 N Si1 O1 1.6556(29) . 109_555 N Si1 O2 1.6371(21) . 1_555 N Si1 O3 1.6682(23) . 112_545 N Si1 Na1 3.267(5) . 1_555 N Al1 Si1 0.01569 . 1_555 N Al1 Si1 3.0969(28) . 17_555 N Al1 Si1 3.0075(26) . 106_555 N Al1 Si1 3.0233(26) . 122_545 N Al1 Al1 3.0859(28) . 17_555 N Al1 Al1 3.1415(33) . 18_555 N Al1 Al1 3.0122(26) . 106_555 N Al1 Al1 3.0122(26) . 122_545 N Al1 O1 1.6477(32) . 17_555 N Al1 O1 1.6476(29) . 109_555 N Al1 O2 1.6301(21) . 1_555 N Al1 O3 1.6818(23) . 112_545 N Al1 Na1 3.270(5) . 1_555 N Al1 Na3 3.6942(23) . 104_555 N O1 Si1 1.6460(32) . 17_555 N O1 Si1 1.6556(29) . 111_455 N O1 Al1 1.6477(32) . 17_555 N O1 Al1 1.6476(29) . 111_455 N O2 Si1 1.6371(21) . 1_555 N O2 Si1 1.6371(21) . 17_555 N O2 Al1 1.6301(21) . 1_555 N O2 Al1 1.6301(21) . 17_555 N O2 Na1 2.386(7) . 1_555 N O3 Si1 1.6682(23) . 106_555 N O3 Si1 1.6682(23) . 124_555 N O3 Al1 1.6818(23) . 106_555 N O3 Al1 1.6818(23) . 124_555 N O3 Na1 2.960(5) . 106_555 N O3 Na3 2.822(4) . 5_556 N Na1 Si1 3.267(5) . 1_555 N Na1 Si1 3.267(5) . 2_555 N Na1 Si1 3.267(5) . 3_555 N Na1 Si1 3.267(5) . 16_555 N Na1 Si1 3.267(5) . 17_555 N Na1 Si1 3.267(5) . 18_555 N Na1 Al1 3.270(5) . 1_555 N Na1 Al1 3.270(5) . 2_555 N Na1 Al1 3.270(5) . 3_555 N Na1 Al1 3.270(5) . 16_555 N Na1 Al1 3.270(5) . 17_555 N Na1 Al1 3.270(5) . 18_555 N Na1 O2 2.386(7) . 1_555 N Na1 O2 2.386(7) . 2_555 N Na1 O2 2.386(7) . 3_555 N Na1 O3 2.960(5) . 107_554 N Na1 O3 2.960(5) . 111_455 N Na1 O3 2.960(5) . 112_545 N Na1 OC3 2.883(22) . 1_555 N Na1 OC3 2.883(22) . 2_555 N Na1 OC3 2.883(22) . 3_555 N Na3 Al1 3.6942(23) . 109_554 N Na3 Al1 3.6942(23) . 112_545 N Na3 Al1 3.6942(23) . 113_545 N Na3 Al1 3.6942(23) . 120_554 N Na3 O3 2.822(4) . 5_655 N Na3 O3 2.822(4) . 14_655 N Na3 Na3 1.731(15) . 6_655 N Na3 OC1 0.850(14) . 1_555 N Na3 OC1 2.580(11) . 6_655 N Na3 OC2 3.075(14) . 1_555 N Na3 CO1 1.952(14) . 1_555 N OC1 Na3 0.850(14) . 1_555 N OC1 Na3 2.580(11) . 6_655 N OC1 CO1 1.103(5) . 1_555 N OC2 Na3 3.075(14) . 1_555 N OC2 CO1 1.123(5) . 1_555 N CO1 Na3 1.952(14) . 1_555 N CO1 OC1 1.103(5) . 1_555 N CO1 OC2 1.123(5) . 1_555 N OC3 Na1 2.883(22) . 1_555 N OC3 CO2 1.1121(12) . 1_555 N OC3 CO2 1.1121(12) . 18_555 N OC3 OC4 2.01(4) . 9_665 N OC3 OC4 2.01(4) . 15_566 N CO2 OC3 1.1121(12) . 1_555 N CO2 CO2 1.71(4) . 9_665 N CO2 CO2 1.71(4) . 11_566 N CO2 CO2 1.43(6) . 15_566 N CO2 CO2 0.46(4) . 18_555 N CO2 CO2 1.89(4) . 20_665 N CO2 OC4 1.13449 . 1_555 N CO2 OC4 1.137(25) . 9_665 N CO2 OC4 1.828(26) . 11_566 N CO2 OC4 0.910(34) . 15_566 N CO2 OC4 1.378(29) . 18_555 N CO2 OC4 1.788(29) . 20_665 N OC4 OC3 2.01(4) . 11_566 N OC4 CO2 1.13449 . 1_555 N OC4 CO2 1.828(26) . 9_665 N OC4 CO2 1.137(25) . 11_566 N OC4 CO2 0.910(34) . 15_566 N OC4 CO2 1.378(29) . 18_555 N OC4 CO2 1.788(29) . 20_665 N OC4 OC4 1.202(33) . 9_665 N OC4 OC4 1.202(33) . 11_566 N OC4 OC4 0.32(6) . 15_566 N OC4 OC4 1.33(4) . 18_555 N OC4 OC4 1.01(4) . 20_665 N loop_ _pd_meas_intensity_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 980(22) 0.002115 896.3 896.3 1007(22) 0.002022 895.4 895.4 999(22) 0.002085 894.6 894.6 974(22) 0.002120 893.7 893.7 992(22) 0.002081 892.8 892.8 1033(22) 0.001986 891.9 891.9 991(22) 0.002089 891.0 891.0 1030(22) 0.001998 890.1 890.1 1037(22) 0.002026 889.2 889.2 968(22) 0.002135 888.4 888.4 1002(22) 0.002016 887.5 887.5 961(21) 0.002194 886.6 886.6 973(22) 0.002144 885.7 885.7 1023(22) 0.002008 884.8 884.8 984(22) 0.002109 883.9 883.9 948(21) 0.002199 883.0 883.0 1063(23) 0.001913 882.1 882.1 997(22) 0.002103 881.3 881.3 1014(22) 0.002035 880.4 880.4 936(21) 0.002172 879.5 879.5 949(21) 0.002187 878.6 878.6 948(21) 0.002197 877.7 877.7 906(21) 0.002272 876.8 876.8 932(21) 0.002249 875.9 875.9 975(22) 0.002159 875.1 875.1 975(22) 0.002049 874.2 874.2 950(21) 0.002186 873.3 873.3 946(21) 0.002214 872.4 872.4 890(21) 0.002257 871.5 871.5 969(22) 0.002100 870.6 870.6 969(22) 0.002160 869.7 869.7 953(22) 0.002152 868.8 868.8 952(21) 0.002211 868.0 868.0 939(21) 0.002232 867.1 867.1 967(22) 0.002099 866.2 866.2 923(21) 0.002228 865.3 865.3 965(22) 0.002141 864.4 864.4 930(21) 0.002194 863.5 863.5 933(21) 0.002174 862.6 862.6 908(21) 0.002331 861.8 861.8 924(21) 0.002225 860.9 860.9 960(22) 0.002119 860.0 860.0 890(21) 0.002358 859.1 859.1 870(21) 0.002378 858.2 858.2 938(21) 0.002179 857.3 857.3 860(20) 0.002452 856.4 856.4 906(21) 0.002296 855.5 855.5 888(21) 0.002290 854.7 854.7 909(21) 0.002278 853.8 853.8 890(21) 0.002338 852.9 852.9 929(21) 0.002171 852.0 852.0 879(21) 0.002342 851.1 851.1 897(21) 0.002279 850.2 850.2 890(21) 0.002319 849.3 849.3 923(21) 0.002210 848.5 848.5 855(20) 0.002400 847.6 847.6 841(20) 0.002421 846.7 846.7 878(20) 0.002387 845.8 845.8 895(21) 0.002338 844.9 844.9 852(20) 0.002427 844.0 844.0 891(21) 0.002338 843.1 843.1 882(20) 0.002385 842.3 842.3 857(20) 0.002407 841.4 841.4 891(21) 0.002330 840.5 840.5 881(21) 0.002356 839.6 839.6 828(20) 0.002499 838.7 838.7 879(21) 0.002353 837.8 837.8 892(21) 0.002311 836.9 836.9 835(20) 0.002432 836.0 836.0 840(20) 0.002517 835.2 835.2 868(20) 0.002436 834.3 834.3 884(21) 0.002284 833.4 833.4 860(20) 0.002425 832.5 832.5 877(21) 0.002378 831.6 831.6 880(21) 0.002312 830.7 830.7 844(20) 0.002484 829.8 829.8 802(20) 0.002625 829.0 829.0 818(20) 0.002530 828.1 828.1 864(21) 0.002360 827.2 827.2 839(20) 0.002494 826.3 826.3 833(20) 0.002463 825.4 825.4 854(20) 0.002392 824.5 824.5 813(20) 0.002596 823.6 823.6 805(20) 0.002514 822.7 822.7 846(20) 0.002424 821.9 821.9 876(20) 0.002428 821.0 821.0 809(20) 0.002545 820.1 820.1 811(20) 0.002544 819.2 819.2 815(20) 0.002576 818.3 818.3 836(20) 0.002470 817.4 817.4 858(20) 0.002398 816.5 816.5 828(20) 0.002516 815.7 815.7 808(20) 0.002540 814.8 814.8 784(19) 0.002641 813.9 813.9 805(20) 0.002603 813.0 813.0 823(20) 0.002500 812.1 812.1 790(20) 0.002614 811.2 811.2 802(20) 0.002580 810.3 810.3 809(20) 0.002566 809.4 809.4 815(20) 0.002499 808.6 808.6 799(20) 0.002556 807.7 807.7 842(20) 0.002436 806.8 806.8 780(19) 0.002639 805.9 805.9 820(20) 0.002507 805.0 805.0 852(21) 0.002379 804.1 804.1 802(20) 0.002538 803.2 803.2 752(19) 0.002738 802.4 802.4 758(19) 0.002746 801.5 801.5 761(19) 0.002711 800.6 800.6 736(19) 0.002858 799.7 799.7 781(19) 0.002634 798.8 798.8 749(19) 0.002735 797.9 797.9 771(19) 0.002651 797.0 797.0 825(20) 0.002503 796.1 796.1 837(20) 0.002397 795.3 795.3 794(20) 0.002623 794.4 794.4 772(19) 0.002698 793.5 793.5 780(19) 0.002643 792.6 792.6 773(19) 0.002740 791.7 791.7 825(20) 0.002488 790.8 790.8 762(19) 0.002672 789.9 789.9 799(20) 0.002626 789.1 789.1 788(20) 0.002624 788.2 788.2 770(19) 0.002634 787.3 787.3 712(18) 0.002936 786.4 786.4 790(20) 0.002601 785.5 785.5 756(19) 0.002691 784.6 784.6 765(19) 0.002710 783.7 783.7 796(20) 0.002593 782.8 782.8 800(20) 0.002507 782.0 782.0 785(19) 0.002657 781.1 781.1 766(19) 0.002785 780.2 780.2 775(19) 0.002638 779.3 779.3 779(19) 0.002647 778.4 778.4 765(19) 0.002733 777.5 777.5 802(20) 0.002530 776.6 776.6 758(19) 0.002701 775.8 775.8 742(19) 0.002840 774.9 774.9 749(19) 0.002680 774.0 774.0 721(19) 0.002810 773.1 773.1 769(19) 0.002721 772.2 772.2 760(19) 0.002734 771.3 771.3 746(19) 0.002685 770.4 770.4 750(19) 0.002765 769.5 769.5 758(19) 0.002750 768.7 768.7 760(19) 0.002666 767.8 767.8 727(19) 0.002905 766.9 766.9 744(19) 0.002770 766.0 766.0 776(19) 0.002663 765.1 765.1 704(18) 0.002952 764.2 764.2 708(18) 0.002948 763.3 763.3 741(19) 0.002748 762.5 762.5 737(19) 0.002802 761.6 761.6 723(19) 0.002857 760.7 760.7 756(19) 0.002702 759.8 759.8 750(19) 0.002802 758.9 758.9 706(18) 0.002931 758.0 758.0 732(19) 0.002819 757.1 757.1 761(19) 0.002739 756.3 756.3 703(18) 0.002946 755.4 755.4 754(19) 0.002681 754.5 754.5 711(19) 0.002915 753.6 753.6 702(18) 0.002965 752.7 752.7 762(19) 0.002684 751.8 751.8 763(19) 0.002723 750.9 750.9 715(18) 0.002953 750.0 750.0 707(19) 0.002908 749.2 749.2 727(19) 0.002825 748.3 748.3 720(19) 0.002886 747.4 747.4 698(19) 0.002916 746.5 746.5 715(19) 0.002908 745.6 745.6 722(19) 0.002870 744.7 744.7 714(19) 0.002889 743.8 743.8 738(19) 0.002789 743.0 743.0 695(18) 0.003047 742.1 742.1 740(19) 0.002700 741.2 741.2 697(18) 0.002975 740.3 740.3 694(18) 0.003049 739.4 739.4 679(18) 0.003021 738.5 738.5 742(19) 0.002781 737.6 737.6 726(19) 0.002917 736.7 736.7 735(19) 0.002757 735.9 735.9 701(18) 0.002926 735.0 735.0 674(18) 0.003178 734.1 734.1 727(19) 0.002800 733.2 733.2 725(19) 0.002869 732.3 732.3 747(19) 0.002766 731.4 731.4 692(18) 0.002944 730.5 730.5 712(19) 0.002910 729.7 729.7 717(18) 0.002923 728.8 728.8 744(19) 0.002797 727.9 727.9 711(19) 0.002808 727.0 727.0 685(18) 0.003072 726.1 726.1 655(18) 0.003118 725.2 725.2 694(18) 0.002946 724.3 724.3 716(18) 0.002950 723.4 723.4 686(18) 0.003023 722.6 722.6 676(18) 0.002986 721.7 721.7 704(18) 0.002960 720.8 720.8 640(18) 0.003239 719.9 719.9 665(18) 0.003029 719.0 719.0 667(18) 0.003092 718.1 718.1 635(17) 0.003301 717.2 717.2 666(18) 0.003130 716.4 716.4 673(18) 0.003187 715.5 715.5 685(18) 0.003004 714.6 714.6 685(18) 0.002987 713.7 713.7 670(18) 0.003081 712.8 712.8 635(17) 0.003331 711.9 711.9 688(18) 0.002977 711.0 711.0 645(18) 0.003205 710.1 710.1 695(18) 0.002995 709.3 709.3 688(18) 0.002972 708.4 708.4 677(18) 0.003111 707.5 707.5 729(19) 0.002897 706.6 706.6 691(18) 0.002940 705.7 705.7 647(17) 0.003283 704.8 704.8 675(18) 0.003048 703.9 703.9 656(18) 0.003093 703.1 703.1 651(18) 0.003192 702.2 702.2 666(18) 0.003066 701.3 701.3 659(18) 0.003108 700.4 700.4 690(18) 0.003058 699.5 699.5 663(18) 0.003153 698.6 698.6 667(18) 0.003051 697.7 697.7 665(18) 0.003110 696.8 696.8 677(18) 0.003046 696.0 696.0 658(18) 0.003104 695.1 695.1 656(18) 0.003152 694.2 694.2 698(18) 0.003023 693.3 693.3 650(18) 0.003198 692.4 692.4 651(18) 0.003176 691.5 691.5 675(18) 0.003104 690.6 690.6 636(18) 0.003217 689.8 689.8 666(18) 0.003080 688.9 688.9 677(18) 0.003082 688.0 688.0 669(18) 0.003055 687.1 687.1 685(18) 0.002923 686.2 686.2 665(18) 0.003176 685.3 685.3 659(18) 0.003150 684.4 684.4 653(18) 0.003133 683.6 683.6 641(17) 0.003305 682.7 682.7 663(18) 0.003099 681.8 681.8 676(18) 0.003047 680.9 680.9 629(17) 0.003396 680.0 680.0 645(18) 0.003227 679.1 679.1 640(18) 0.003157 678.2 678.2 646(18) 0.003246 677.3 677.3 676(18) 0.003029 676.5 676.5 577(17) 0.00357 675.6 675.6 612(17) 0.003435 674.7 674.7 616(17) 0.003415 673.8 673.8 683(18) 0.003039 672.9 672.9 646(18) 0.003253 672.0 672.0 664(18) 0.003110 671.1 671.1 630(17) 0.003266 670.3 670.3 638(17) 0.003279 669.4 669.4 616(17) 0.003364 668.5 668.5 635(18) 0.003216 667.6 667.6 644(17) 0.003280 666.7 666.7 715(19) 0.002818 665.8 665.8 648(18) 0.003206 664.9 664.9 695(18) 0.002939 664.0 664.0 623(17) 0.003298 663.2 663.2 632(17) 0.003303 662.3 662.3 625(17) 0.003323 661.4 661.4 658(18) 0.003133 660.5 660.5 626(18) 0.003216 659.6 659.6 629(17) 0.003292 658.7 658.7 638(17) 0.003281 657.8 657.8 642(18) 0.003148 657.0 657.0 647(17) 0.003299 656.1 656.1 637(17) 0.003303 655.2 655.2 610(17) 0.003355 654.3 654.3 627(17) 0.003283 653.4 653.4 610(17) 0.003399 652.5 652.5 597(17) 0.003352 651.6 651.6 620(17) 0.003411 650.7 650.7 648(18) 0.003225 649.9 649.9 635(18) 0.003147 649.0 649.0 605(17) 0.003356 648.1 648.1 569(16) 0.00380 647.2 647.2 603(17) 0.003363 646.3 646.3 638(17) 0.003274 645.4 645.4 625(17) 0.003412 644.5 644.5 637(18) 0.003217 643.7 643.7 615(17) 0.003297 642.8 642.8 630(17) 0.003340 641.9 641.9 588(17) 0.003479 641.0 641.0 590(17) 0.003501 640.1 640.1 631(17) 0.003353 639.2 639.2 612(17) 0.003376 638.3 638.3 604(17) 0.003338 637.4 637.4 589(17) 0.00357 636.6 636.6 599(17) 0.003461 635.7 635.7 571(17) 0.00355 634.8 634.8 601(17) 0.003478 633.9 633.9 606(17) 0.003401 633.0 633.0 589(17) 0.003483 632.1 632.1 591(17) 0.003503 631.2 631.2 606(17) 0.003409 630.4 630.4 567(17) 0.00364 629.5 629.5 650(18) 0.003254 628.6 628.6 590(17) 0.00353 627.7 627.7 614(17) 0.003332 626.8 626.8 550(16) 0.00373 625.9 625.9 564(16) 0.00369 625.0 625.0 588(17) 0.003455 624.1 624.1 598(17) 0.003445 623.3 623.3 612(17) 0.003418 622.4 622.4 616(17) 0.003362 621.5 621.5 639(18) 0.003230 620.6 620.6 595(17) 0.00351 619.7 619.7 548(16) 0.00374 618.8 618.8 636(18) 0.003242 617.9 617.9 595(17) 0.003427 617.1 617.1 576(17) 0.00358 616.2 616.2 594(17) 0.003438 615.3 615.3 596(17) 0.00352 614.4 614.4 599(17) 0.003477 613.5 613.5 619(17) 0.003381 612.6 612.6 584(17) 0.00360 611.7 611.7 565(17) 0.00365 610.9 610.9 562(16) 0.00367 610.0 610.0 598(17) 0.003459 609.1 609.1 587(17) 0.003482 608.2 608.2 616(17) 0.003382 607.3 607.3 570(16) 0.00369 606.4 606.4 593(17) 0.003441 605.5 605.5 551(16) 0.00381 604.6 604.6 578(17) 0.00365 603.8 603.8 574(17) 0.003505 602.9 602.9 587(17) 0.003493 602.0 602.0 564(16) 0.00374 601.1 601.1 564(17) 0.00364 600.2 600.2 559(16) 0.00369 599.3 599.3 606(17) 0.003448 598.4 598.4 591(17) 0.003440 597.6 597.6 590(17) 0.003494 596.7 596.7 564(16) 0.00377 595.8 595.8 576(17) 0.00360 594.9 594.9 588(17) 0.003463 594.0 594.0 600(17) 0.00352 593.1 593.1 598(17) 0.003475 592.2 592.2 585(17) 0.00351 591.3 591.3 621(17) 0.003378 590.5 590.5 558(16) 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440.4 440(15) 0.00461 394.7 439.6 449(15) 0.00472 394.5 438.8 453(15) 0.00457 394.2 438.2 417(14) 0.00494 393.9 437.6 415(14) 0.00496 393.6 437.0 427(14) 0.00483 393.4 436.6 442(15) 0.00443 393.1 436.2 404(14) 0.00522 392.8 435.8 433(15) 0.00472 392.6 435.5 434(14) 0.00478 392.3 435.3 431(14) 0.00477 392.0 435.1 442(15) 0.00465 391.7 435.0 453(15) 0.00456 391.5 434.9 431(15) 0.00471 391.2 434.9 398(14) 0.00529 390.9 435.0 422(14) 0.00483 390.7 435.1 432(14) 0.00496 390.4 435.3 452(15) 0.00462 390.1 435.5 439(15) 0.00463 389.8 435.7 428(14) 0.00477 389.6 436.1 444(15) 0.00465 389.3 436.5 445(15) 0.00456 389.0 436.9 482(15) 0.00425 388.7 437.4 410(14) 0.00512 388.5 438.0 438(15) 0.00461 388.2 438.7 440(15) 0.00460 387.9 439.4 430(14) 0.00481 387.7 440.2 447(15) 0.00465 387.4 441.1 434(14) 0.00484 387.1 442.1 443(15) 0.00475 386.8 443.1 410(14) 0.00511 386.6 444.3 467(15) 0.00453 386.3 445.5 412(14) 0.00519 386.0 446.9 424(14) 0.00480 385.8 448.4 450(15) 0.00450 385.5 449.9 491(15) 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950(22) 0.002163 375.7 934.1 1045(22) 0.002005 375.4 1013.3 1183(24) 0.001796 375.2 1112.2 1360(26) 0.001523 374.9 1236.6 1533(27) 0.001328 374.6 1393.3 1646(28) 0.001275 374.4 1589.5 1981(31) 0.001029 374.1 1832.9 2282(34) 0.000884 373.8 2130.6 2626(36) 0.000793 374. 2488. 3030(38) 0.000676 373. 2906. 3452(41) 0.000586 373. 3383. 4079(44) 0.000509 373. 3903. 4663(48) 0.000436 372. 4441. 5156(51) 0.000392 372. 4946. 5555(52) 0.000368 372. 5352. 5818(54) 0.0003478 372. 5584. 5830(54) 0.0003452 371. 5589. 5513(52) 0.000375 371. 5367. 5056(50) 0.000405 371. 4968. 4475(47) 0.000449 371. 4465. 3913(43) 0.000531 370. 3927. 3418(41) 0.000597 370. 3404. 2922(38) 0.000697 370. 2925. 2490(35) 0.000826 369.5 2502.5 2183(33) 0.000940 369.2 2141.6 1931(31) 0.001056 368.9 1840.4 1686(29) 0.001225 368.6 1593.8 1451(26) 0.001425 368.4 1394.8 1291(25) 0.001595 368.1 1235.8 1198(24) 0.001733 367.8 1109.3 1097(23) 0.001856 367.6 1008.6 970(22) 0.002127 367.3 927.9 886(21) 0.002324 367.0 862.7 810(20) 0.002566 366.7 809.1 749(19) 0.002763 366.5 764.4 741(19) 0.002805 366.2 726.7 683(18) 0.002984 365.9 694.3 657(18) 0.003092 365.7 666.2 687(18) 0.003030 365.4 643.9 582(17) 0.00359 365.1 622.2 581(17) 0.00357 364.8 602.9 538(16) 0.00390 364.6 585.6 544(16) 0.00382 364.3 570.1 515(16) 0.00389 364.0 556.2 540(16) 0.00381 363.8 543.5 519(16) 0.00401 363.5 532.1 513(16) 0.00389 363.2 521.6 500(16) 0.00411 362.9 512.1 496(15) 0.00428 362.7 503.4 472(15) 0.00432 362.4 495.3 475(15) 0.00430 362.1 487.9 478(15) 0.00434 361.9 481.1 478(15) 0.00425 361.6 474.8 465(15) 0.00441 361.3 469.0 452(15) 0.00472 361.0 463.5 422(14) 0.00490 360.8 458.5 428(15) 0.00476 360.5 453.8 429(14) 0.00491 360.2 449.4 446(15) 0.00454 360.0 445.2 419(14) 0.00489 359.7 441.4 422(14) 0.00501 359.4 437.7 435(15) 0.00473 359.1 434.3 428(15) 0.00465 358.9 431.1 404(14) 0.00521 358.6 428.0 431(15) 0.00475 358.3 425.2 424(15) 0.00474 358.1 422.4 407(14) 0.00516 357.8 419.9 385(14) 0.00543 357.5 417.4 427(14) 0.00482 357.2 415.1 414(14) 0.00510 357.0 412.9 401(14) 0.00516 356.7 410.8 430(14) 0.00483 356.4 408.8 394(14) 0.00526 356.2 406.9 414(14) 0.00500 355.9 405.0 416(14) 0.00490 355.6 403.3 377(14) 0.00538 355.3 401.6 390(14) 0.00527 355.1 400.0 397(14) 0.00505 354.8 398.4 354(13) 0.00587 354.5 397.0 342(13) 0.00602 354.2 395.5 372(13) 0.00567 354.0 394.2 362(13) 0.00578 353.7 392.9 378(14) 0.00541 353.4 391.6 363(13) 0.00566 353.2 390.4 396(14) 0.00527 352.9 389.2 384(14) 0.00538 352.6 388.1 369(13) 0.00555 352.3 386.9 360(13) 0.00574 352.1 385.9 396(14) 0.00524 351.8 384.9 370(13) 0.00564 351.5 383.9 388(14) 0.00534 351.3 382.9 387(14) 0.00547 351.0 382.0 368(14) 0.00544 350.7 381.0 360(13) 0.00596 350.4 380.2 373(13) 0.00561 350.2 379.3 379(14) 0.00545 349.9 378.5 359(13) 0.00581 349.6 377.7 338(13) 0.00618 349.4 376.9 378(13) 0.00554 349.1 376.1 384(13) 0.00551 348.8 375.3 353(13) 0.00612 348.5 374.6 330(13) 0.00613 348.3 373.9 353(13) 0.00581 348.0 373.2 388(13) 0.00549 347.7 372.5 376(14) 0.00545 347.5 371.9 370(13) 0.00550 347.2 371.3 353(13) 0.00591 346.9 370.7 372(14) 0.00541 346.6 370.0 361(13) 0.00572 346.4 369.4 349(13) 0.00614 346.1 368.9 350(13) 0.00579 345.8 367.4 376(14) 0.00535 345.6 366.8 354(13) 0.00587 345.3 366.3 361(13) 0.00578 345.0 365.7 374(14) 0.00548 344.7 365.2 342(13) 0.00609 344.5 364.7 352(13) 0.00577 344.2 364.2 372(14) 0.00542 343.9 363.7 351(13) 0.00595 343.7 363.2 384(13) 0.00564 343.4 362.8 370(13) 0.00555 343.1 362.3 384(14) 0.00538 342.8 361.9 371(13) 0.00557 342.6 361.4 372(13) 0.00551 342.3 361.0 364(13) 0.00571 342.0 360.6 356(13) 0.00570 341.8 360.1 378(14) 0.00538 341.5 359.7 373(13) 0.00560 341.2 359.3 375(13) 0.00555 340.9 358.9 379(14) 0.00534 340.7 358.6 393(14) 0.00532 340.4 358.2 381(14) 0.00543 340.1 357.8 353(13) 0.00583 339.9 357.5 357(13) 0.00596 339.8 357.3 368(13) 0.00565 339.7 357.2 352(13) 0.00579 339.7 357.0 350(13) 0.00603 339.6 356.9 369(13) 0.00569 339.5 356.8 371(14) 0.00548 339.5 356.6 346(13) 0.00616 339.4 356.5 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257.5 495.9 496(16) 0.00415 257.4 512.7 521(16) 0.00387 257.3 531.2 529(16) 0.00393 257.3 551.6 525(16) 0.00395 257.2 573.8 592(17) 0.003409 257.2 598.0 626(17) 0.003295 257.1 624.1 647(18) 0.003264 257.0 652.3 722(19) 0.002844 257.0 682.3 707(18) 0.002927 256.9 714.1 738(19) 0.002889 256.8 747.4 788(20) 0.002557 256.8 782.0 802(20) 0.002563 256.7 817.4 843(20) 0.002514 256.7 853.1 902(21) 0.002289 256.6 888.2 919(21) 0.002231 256.5 921.8 945(21) 0.002230 256.5 952.9 936(21) 0.002219 256.4 980.4 1035(22) 0.001981 256.3 1002.9 1020(22) 0.002061 256.3 1019.4 1036(22) 0.002021 256.2 1029.1 1038(23) 0.001953 256.2 1031.3 1011(22) 0.002066 256.1 1025.9 975(22) 0.002128 256.0 1013.2 953(22) 0.002128 256.0 993.9 908(21) 0.002284 255.9 969.0 865(20) 0.002382 255.8 939.7 854(20) 0.002394 255.8 907.2 848(20) 0.002470 255.7 872.4 808(20) 0.002524 255.6 836.6 801(20) 0.002552 255.6 800.4 746(19) 0.002764 255.5 764.8 692(18) 0.002943 255.5 730.1 657(18) 0.003073 255.4 696.7 634(18) 0.003231 255.3 665.0 614(17) 0.003326 255.3 635.2 561(16) 0.00367 255.2 607.2 544(16) 0.00377 255.1 581.1 524(16) 0.00390 255.1 557.1 533(16) 0.00380 255.0 534.9 505(16) 0.00405 255.0 514.5 495(15) 0.00417 254.9 495.9 501(16) 0.00411 254.8 479.0 454(15) 0.00465 254.8 463.7 471(15) 0.00442 254.7 449.8 464(15) 0.00446 254.6 437.3 442(14) 0.00478 254.6 426.1 433(14) 0.00480 254.5 416.0 437(14) 0.00478 254.5 407.0 433(15) 0.00474 254.4 399.0 404(14) 0.00524 254.3 391.8 389(14) 0.00528 254.3 385.5 365(13) 0.00576 254.2 380.0 376(13) 0.00559 254.1 375.1 352(13) 0.00574 254.1 370.9 355(13) 0.00572 254.0 367.3 325(12) 0.00653 253.9 364.2 333(13) 0.00618 253.9 361.7 380(14) 0.00536 253.8 359.6 367(13) 0.00559 253.8 358.0 342(13) 0.00600 253.7 356.8 370(13) 0.00553 253.6 356.1 372(13) 0.00566 253.6 355.8 394(14) 0.00522 253.5 355.9 417(14) 0.00488 253.4 356.3 388(14) 0.00538 253.4 357.2 388(14) 0.00523 253.3 358.4 374(14) 0.00532 253.3 359.9 404(14) 0.00526 253.2 361.8 403(14) 0.00506 253.1 363.9 431(15) 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327(13) 0.00620 250.8 304.7 312(12) 0.00665 250.7 304.0 306(12) 0.00697 250.7 303.5 321(12) 0.00645 250.6 303.2 339(13) 0.00622 250.6 303.0 321(12) 0.00651 250.5 303.1 302(12) 0.00670 250.4 303.4 295(12) 0.00694 250.4 303.9 331(13) 0.00622 250.3 304.4 318(12) 0.00649 250.2 305.3 305(12) 0.00685 250.2 306.5 306(12) 0.00687 250.1 307.8 319(13) 0.00639 250.1 309.5 333(13) 0.00607 250.0 311.3 299(12) 0.00719 249.9 313.5 336(13) 0.00616 249.9 315.9 308(12) 0.00661 249.8 318.6 341(13) 0.00600 249.7 321.6 319(12) 0.00646 249.7 324.8 319(13) 0.00627 249.6 328.4 321(13) 0.00633 249.5 332.2 356(13) 0.00581 249.5 336.2 328(13) 0.00619 249.4 340.5 323(12) 0.00642 249.4 344.9 300(12) 0.00716 249.3 349.4 337(13) 0.00610 249.2 354.0 350(13) 0.00591 249.2 358.5 363(13) 0.00585 249.1 362.8 395(14) 0.00503 249.0 366.7 360(13) 0.00585 249.0 370.1 361(13) 0.00578 248.9 372.9 375(13) 0.00549 248.9 374.8 379(14) 0.00539 248.8 375.9 356(13) 0.00593 248.7 376.1 350(13) 0.00590 248.7 375.3 353(13) 0.00597 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388(14) 0.00516 244.1 377.4 357(13) 0.00562 244.0 368.6 366(13) 0.00557 243.9 360.6 354(13) 0.00584 243.9 353.1 329(13) 0.00610 243.8 346.2 322(13) 0.00635 243.8 340.0 352(13) 0.00574 243.7 334.2 324(12) 0.00648 243.6 329.0 364(13) 0.00589 243.6 324.3 343(13) 0.00602 243.5 320.0 318(12) 0.00642 243.4 316.1 341(13) 0.00594 243.4 312.7 309(12) 0.00677 243.3 309.6 327(13) 0.00624 243.3 306.8 294(12) 0.00721 243.2 304.3 299(12) 0.00694 243.1 302.2 303(12) 0.00673 243.1 300.3 319(12) 0.00655 243.0 298.6 347(13) 0.00617 242.9 297.1 305(12) 0.00662 242.9 295.9 296(12) 0.00710 242.8 294.9 313(12) 0.00676 242.8 294.0 328(13) 0.00625 242.7 293.3 330(12) 0.00641 242.6 292.7 343(13) 0.00608 242.6 292.4 280(12) 0.00712 242.5 292.2 320(12) 0.00649 242.4 292.1 322(12) 0.00646 242.4 292.2 312(12) 0.00665 242.3 292.4 306(12) 0.00670 242.3 292.7 312(12) 0.00660 242.2 293.1 297(12) 0.00681 242.1 293.6 297(12) 0.00725 242.1 294.2 337(13) 0.00622 242.0 294.9 343(13) 0.00599 241.9 295.6 330(13) 0.00627 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401(14) 0.00528 237.3 422.3 379(14) 0.00546 237.3 414.3 377(13) 0.00555 237.2 406.2 341(13) 0.00619 237.2 398.4 347(13) 0.00576 237.1 391.0 363(13) 0.00585 237.0 383.9 345(13) 0.00593 237.0 377.4 335(13) 0.00628 236.9 371.3 360(13) 0.00587 236.8 365.9 353(13) 0.00586 236.8 361.0 343(13) 0.00603 236.7 356.7 340(13) 0.00606 236.7 353.0 350(13) 0.00589 236.6 349.9 352(13) 0.00573 236.5 347.4 339(13) 0.00617 236.5 345.5 346(13) 0.00590 236.4 344.2 342(13) 0.00582 236.3 343.5 359(13) 0.00577 236.3 343.3 333(13) 0.00614 236.2 343.8 341(13) 0.00598 236.2 344.8 353(13) 0.00593 236.1 346.5 366(13) 0.00561 236.0 348.8 371(13) 0.00568 236.0 351.7 340(13) 0.00625 235.9 355.4 351(13) 0.00590 235.8 359.7 348(13) 0.00593 235.8 364.8 354(13) 0.00596 235.7 370.6 384(13) 0.00552 235.6 377.2 389(14) 0.00529 235.6 384.7 368(13) 0.00568 235.5 393.0 385(14) 0.00545 235.5 402.3 412(14) 0.00481 235.4 412.5 413(14) 0.00495 235.3 423.7 454(15) 0.00458 235.3 435.9 409(14) 0.00503 235.2 449.0 448(15) 0.00457 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365(13) 0.00564 232.7 370.3 370(13) 0.00565 232.7 361.5 329(13) 0.00637 232.6 353.5 339(13) 0.00594 232.5 346.1 337(13) 0.00610 232.5 339.5 330(13) 0.00626 232.4 333.4 313(12) 0.00651 232.3 327.9 316(12) 0.00683 232.3 322.9 323(12) 0.00674 232.2 318.4 303(12) 0.00675 232.1 314.2 325(12) 0.00657 232.1 310.5 321(12) 0.00654 232.0 307.1 318(12) 0.00651 231.9 304.0 287(12) 0.00721 231.9 301.2 307(12) 0.00667 231.8 298.7 315(12) 0.00650 231.7 296.4 286(12) 0.00719 231.7 294.2 296(12) 0.00704 231.6 292.3 297(12) 0.00685 231.5 290.6 305(12) 0.00670 231.5 289.0 298(12) 0.00699 231.4 287.5 303(12) 0.00670 231.3 286.2 267(11) 0.00791 231.3 285.0 314(12) 0.00674 231.2 283.9 292(12) 0.00681 231.1 282.8 291(12) 0.00710 231.1 281.9 288(12) 0.00729 231.0 280.9 278(12) 0.00733 230.9 280.2 300(12) 0.00692 230.9 279.5 342(13) 0.00616 230.8 279.0 307(12) 0.00665 230.7 278.5 259(11) 0.00788 230.7 278.0 288(12) 0.00702 230.6 277.6 289(12) 0.00719 230.5 277.3 283(12) 0.00726 230.5 277.1 271(11) 0.00768 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442.6 393(14) 0.00524 225.6 429.6 425(14) 0.00485 225.5 417.5 410(14) 0.00486 225.4 406.2 410(14) 0.00483 225.4 395.8 363(13) 0.00565 225.3 386.3 365(13) 0.00569 225.2 377.6 346(13) 0.00589 225.2 369.8 340(13) 0.00619 225.1 362.8 364(13) 0.00569 225.0 356.7 335(13) 0.00619 225.0 351.2 345(13) 0.00617 224.9 346.6 369(13) 0.00575 224.8 342.6 348(13) 0.00586 224.8 339.3 344(13) 0.00594 224.7 336.7 345(13) 0.00597 224.6 334.8 337(13) 0.00596 224.6 333.5 371(14) 0.00542 224.5 332.9 373(13) 0.00566 224.4 332.9 341(13) 0.00611 224.4 333.5 330(13) 0.00636 224.3 334.8 352(13) 0.00608 224.2 336.7 324(12) 0.00647 224.2 339.3 342(13) 0.00609 224.1 342.5 331(12) 0.00646 224.0 346.4 342(13) 0.00613 223.9 350.9 344(13) 0.00590 223.9 356.1 364(13) 0.00576 223.8 362.0 350(13) 0.00596 223.7 368.5 382(14) 0.00544 223.7 375.6 388(14) 0.00545 223.6 383.3 391(14) 0.00506 223.5 391.5 414(14) 0.00493 223.5 400.2 389(14) 0.00544 223.4 409.2 431(14) 0.00479 223.3 418.4 424(14) 0.00487 223.3 427.6 442(14) 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296(12) 0.00683 220.8 299.4 304(12) 0.00676 220.7 299.8 314(12) 0.00662 220.7 300.6 323(13) 0.00637 220.6 301.8 309(12) 0.00685 220.5 303.4 319(12) 0.00647 220.5 305.4 341(13) 0.00594 220.4 307.9 315(12) 0.00648 220.3 310.8 299(12) 0.00698 220.3 314.2 339(13) 0.00605 220.2 318.0 293(12) 0.00709 220.1 322.3 320(12) 0.00641 220.1 326.9 326(13) 0.00619 220.0 332.0 337(13) 0.00618 219.9 337.6 361(13) 0.00570 219.9 343.4 396(14) 0.00512 219.8 349.6 378(14) 0.00545 219.7 356.1 339(13) 0.00612 219.7 362.7 342(13) 0.00618 219.6 369.4 399(14) 0.00512 219.5 376.0 392(14) 0.00523 219.5 382.4 427(14) 0.00482 219.4 388.3 426(14) 0.00490 219.3 393.5 415(14) 0.00507 219.3 397.8 416(14) 0.00494 219.2 401.1 438(15) 0.00458 219.1 403.0 395(14) 0.00524 219.1 403.6 410(14) 0.00495 219.0 402.8 389(14) 0.00544 218.9 400.6 393(14) 0.00535 218.8 397.0 395(14) 0.00505 218.8 392.3 397(14) 0.00525 218.7 386.6 328(12) 0.00643 218.6 380.2 377(14) 0.00540 218.6 373.2 365(13) 0.00573 218.5 365.9 388(14) 0.00530 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220(10) 0.00943 194.9 215.7 238(11) 0.00853 194.9 215.4 230(11) 0.00876 194.8 215.2 243(11) 0.00861 194.8 214.9 236(11) 0.00887 194.7 214.7 230(11) 0.00874 194.6 214.6 224(10) 0.00926 194.6 214.4 235(11) 0.00865 194.5 214.3 218(10) 0.00946 194.4 214.3 246(11) 0.00834 194.4 214.2 216(10) 0.00972 194.3 214.2 223(10) 0.00911 194.3 214.2 220(10) 0.00918 194.2 214.2 244(11) 0.00865 194.1 214.2 207(10) 0.00997 194.1 214.2 234(11) 0.00871 194.0 214.2 219(10) 0.00962 193.9 214.2 218(10) 0.00937 193.9 214.2 212(10) 0.00990 193.8 214.2 222(10) 0.00953 193.7 214.2 232(11) 0.00887 193.7 214.2 235(11) 0.00877 193.6 214.3 200(10) 0.01066 193.6 214.3 190(9) 0.01113 193.5 214.3 230(11) 0.00871 193.4 214.3 199(10) 0.01061 193.4 214.4 217(10) 0.00932 193.3 214.5 224(11) 0.00902 193.2 214.6 237(11) 0.00873 193.2 214.7 220(10) 0.00960 193.1 214.9 230(11) 0.00900 193.1 215.1 226(11) 0.00885 193.0 215.4 219(10) 0.00922 192.9 215.7 217(10) 0.00944 192.9 216.1 225(10) 0.00910 192.8 216.5 246(11) 0.00848 192.7 216.9 217(10) 0.00983 192.7 217.5 194(10) 0.01088 192.6 218.1 222(10) 0.00926 192.6 218.8 238(11) 0.00840 192.5 219.6 231(11) 0.00887 192.4 220.5 212(10) 0.01004 192.4 221.5 235(11) 0.00851 192.3 222.6 229(10) 0.00930 192.2 223.9 250(11) 0.00807 192.2 225.3 250(11) 0.00790 192.1 226.8 237(11) 0.00904 192.1 228.5 201(10) 0.01051 192.0 230.3 229(11) 0.00877 191.9 232.1 242(11) 0.00853 191.9 234.3 244(11) 0.00863 191.8 236.8 236(11) 0.00884 191.7 239.4 225(10) 0.00947 191.7 242.3 251(11) 0.00847 191.6 245.3 249(11) 0.00827 191.6 248.6 250(11) 0.00831 191.5 252.2 240(11) 0.00864 191.4 255.9 289(12) 0.00703 191.4 259.9 249(11) 0.00836 191.3 264.1 274(11) 0.00763 191.2 268.4 273(12) 0.00746 191.2 272.9 279(12) 0.00753 191.1 277.5 254(11) 0.00865 191.1 282.1 286(12) 0.00717 191.0 286.7 289(12) 0.00707 190.9 291.1 289(12) 0.00709 190.9 295.3 290(12) 0.00701 190.8 299.2 272(11) 0.00764 190.7 302.6 314(12) 0.00660 190.7 305.4 314(12) 0.00657 190.6 307.5 311(12) 0.00657 190.6 308.8 308(12) 0.00660 190.5 309.2 294(12) 0.00706 190.4 308.8 310(12) 0.00663 190.4 307.6 298(12) 0.00698 190.3 305.6 271(11) 0.00759 190.2 303.0 294(12) 0.00702 190.2 299.8 276(12) 0.00755 190.1 296.2 311(12) 0.00678 190.1 292.3 298(12) 0.00688 190.0 288.2 266(11) 0.00787 189.9 284.0 286(12) 0.00710 189.9 279.9 283(12) 0.00713 189.8 275.8 261(11) 0.00789 189.7 271.9 287(12) 0.00723 189.7 268.1 240(11) 0.00853 189.6 264.6 279(12) 0.00719 189.6 261.4 245(11) 0.00886 189.5 258.3 261(11) 0.00768 189.4 255.6 247(11) 0.00840 189.4 253.2 278(12) 0.00735 189.3 251.0 265(11) 0.00798 189.2 249.2 251(11) 0.00819 189.2 247.6 261(11) 0.00811 189.1 246.3 241(11) 0.00834 189.1 245.4 241(11) 0.00861 189.0 244.7 248(11) 0.00842 188.9 244.4 232(10) 0.00913 188.9 244.3 224(10) 0.00935 188.8 244.5 249(11) 0.00832 188.7 245.0 236(11) 0.00889 188.7 245.8 244(11) 0.00845 188.6 246.9 242(11) 0.00849 188.6 248.2 265(12) 0.00754 188.5 249.9 263(11) 0.00791 188.4 251.9 273(11) 0.00767 188.4 254.2 267(11) 0.00761 188.3 256.7 252(11) 0.00799 188.2 259.6 245(11) 0.00855 188.2 262.7 269(12) 0.00729 188.1 266.1 267(11) 0.00780 188.1 269.8 303(12) 0.00685 188.0 273.7 300(12) 0.00689 187.9 277.8 306(12) 0.00662 187.9 282.1 273(11) 0.00782 187.8 286.5 286(12) 0.00721 187.7 291.0 299(12) 0.00688 187.7 295.5 308(12) 0.00682 187.6 299.8 310(12) 0.00679 187.6 304.0 295(12) 0.00707 187.5 307.9 321(12) 0.00653 187.4 311.3 301(12) 0.00694 187.4 314.1 291(12) 0.00720 187.3 316.3 328(13) 0.00634 187.2 317.7 341(13) 0.00617 187.2 318.2 307(12) 0.00671 187.1 317.9 324(12) 0.00650 187.1 316.8 292(12) 0.00722 187.0 314.9 288(12) 0.00717 186.9 312.3 309(12) 0.00675 186.9 309.1 319(13) 0.00633 186.8 305.4 281(12) 0.00740 186.7 301.4 254(11) 0.00848 186.7 297.1 299(12) 0.00673 186.6 292.7 268(11) 0.00768 186.6 288.2 299(12) 0.00681 186.5 283.9 290(12) 0.00717 186.4 279.6 255(11) 0.00798 186.4 275.5 256(11) 0.00790 186.3 271.6 254(11) 0.00802 186.2 268.0 275(12) 0.00740 186.2 264.7 255(11) 0.00814 186.1 261.6 257(11) 0.00813 186.1 258.8 246(11) 0.00838 186.0 256.3 273(11) 0.00757 185.9 254.2 281(12) 0.00732 185.9 252.4 246(11) 0.00813 185.8 250.9 251(11) 0.00830 185.7 249.7 228(10) 0.00923 185.7 248.9 247(11) 0.00816 185.6 248.3 263(11) 0.00789 185.6 248.1 238(11) 0.00899 185.5 248.3 285(12) 0.00700 185.4 248.8 254(11) 0.00791 185.4 249.6 260(11) 0.00788 185.3 250.8 260(11) 0.00784 185.2 252.3 270(11) 0.00761 185.2 254.1 276(11) 0.00761 185.1 256.3 277(12) 0.00733 185.1 258.9 263(11) 0.00776 185.0 261.8 272(11) 0.00768 184.9 264.8 282(12) 0.00724 184.9 268.4 280(12) 0.00739 184.8 272.3 287(12) 0.00737 184.7 276.5 285(12) 0.00732 184.7 281.0 308(12) 0.00657 184.6 285.8 318(12) 0.00648 184.6 290.7 325(13) 0.00620 184.5 295.9 315(12) 0.00656 184.4 301.1 332(13) 0.00634 184.4 306.4 319(12) 0.00650 184.3 311.5 329(13) 0.00626 184.2 316.3 354(13) 0.00592 184.2 320.7 357(13) 0.00577 184.1 324.7 348(13) 0.00595 184.1 327.9 366(13) 0.00560 184.0 330.3 354(13) 0.00588 183.9 331.8 369(13) 0.00564 183.9 332.3 351(13) 0.00581 183.8 331.7 317(12) 0.00665 183.7 330.1 366(14) 0.00547 183.7 327.5 367(13) 0.00559 183.6 324.1 346(13) 0.00590 183.6 319.8 331(13) 0.00633 183.5 315.0 334(13) 0.00607 183.4 309.8 320(13) 0.00635 183.4 304.2 304(12) 0.00671 183.3 298.4 299(12) 0.00705 183.2 292.5 273(11) 0.00795 183.2 286.7 287(12) 0.00723 183.1 281.0 279(12) 0.00751 183.1 275.4 283(12) 0.00745 183.0 270.1 260(11) 0.00804 182.9 264.9 269(11) 0.00769 182.9 260.1 251(11) 0.00846 182.8 255.5 263(11) 0.00783 182.7 251.3 246(11) 0.00878 182.7 247.3 256(11) 0.00795 182.6 243.5 240(11) 0.00823 182.5 240.1 235(11) 0.00886 182.5 237.0 249(11) 0.00852 182.4 234.1 237(11) 0.00838 182.4 231.5 217(10) 0.00971 182.3 229.1 254(11) 0.00813 182.2 226.9 242(11) 0.00828 182.2 225.0 218(10) 0.00955 182.1 223.3 219(10) 0.01026 182.0 221.8 233(11) 0.00888 182.0 220.5 217(10) 0.00930 181.9 219.4 216(10) 0.00986 181.9 218.5 236(11) 0.00839 181.8 217.7 200(10) 0.01038 181.7 217.1 210(10) 0.00969 181.7 216.6 239(11) 0.00851 181.6 216.3 227(10) 0.00924 181.5 216.1 244(11) 0.00812 181.5 216.0 204(10) 0.01019 181.4 216.0 198(10) 0.01052 181.4 216.2 226(10) 0.00924 181.3 216.4 214(10) 0.00986 181.2 216.8 223(11) 0.00885 181.2 217.2 222(10) 0.00912 181.1 217.6 210(10) 0.00959 181.0 218.1 199(10) 0.01043 181.0 218.6 212(10) 0.00974 180.9 219.1 227(11) 0.00905 180.9 219.5 206(10) 0.00993 180.8 219.8 205(10) 0.01051 180.7 220.1 228(10) 0.00912 180.7 220.2 210(10) 0.01002 180.6 220.2 210(10) 0.01020 180.5 219.9 215(10) 0.00951 180.5 219.6 207(10) 0.00964 180.4 219.0 196(10) 0.01069 180.4 218.3 195(10) 0.01077 180.3 217.5 231(11) 0.00881 180.2 216.5 197(10) 0.01046 180.2 215.5 225(11) 0.00886 180.1 214.4 199(10) 0.01035 180.0 213.3 214(10) 0.00987 180.0 212.2 234(11) 0.00877 179.9 211.0 221(10) 0.00908 179.9 210.0 224(10) 0.00931 179.8 208.9 213(10) 0.00984 179.7 207.9 213(10) 0.00969 179.7 207.0 215(10) 0.00992 179.6 206.2 220(10) 0.00933 179.5 205.4 207(10) 0.00984 179.5 204.7 199(10) 0.01032 179.4 204.1 205(10) 0.00988 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0.00968 157.3 213.3 220(10) 0.00963 157.3 213.5 219(10) 0.00954 157.2 213.5 212(10) 0.00974 157.2 213.2 203(10) 0.01045 157.2 212.7 226(10) 0.00917 157.2 211.9 209(10) 0.00990 157.1 210.9 195(10) 0.01098 157.1 209.8 188(9) 0.01126 157.1 208.5 196(9) 0.01127 157.1 207.1 229(10) 0.00942 157.0 205.6 214(10) 0.00954 157.0 204.1 213(10) 0.00975 157.0 202.5 201(10) 0.01031 157.0 201.0 186(10) 0.01106 156.9 199.5 209(10) 0.00965 156.9 198.0 197(10) 0.01065 156.9 196.5 190(10) 0.01034 156.9 195.2 181(9) 0.01143 156.9 193.9 182(9) 0.01178 156.8 192.7 208(10) 0.01006 156.8 191.6 208(10) 0.00948 156.8 190.6 183(9) 0.01134 156.8 189.6 208(10) 0.00975 156.8 188.8 213(10) 0.00946 156.8 188.0 201(10) 0.01066 156.8 187.4 187(10) 0.01093 156.8 186.8 187(10) 0.01096 156.8 186.4 201(10) 0.01033 156.8 186.0 191(10) 0.01088 156.8 185.7 188(9) 0.01110 156.8 185.5 193(9) 0.01110 156.7 185.4 207(10) 0.00986 156.7 185.3 200(10) 0.01007 156.7 185.4 195(10) 0.01070 156.7 185.5 214(10) 0.00964 156.7 185.7 198(10) 0.01025 156.7 186.0 198(10) 0.01103 156.7 186.3 216(10) 0.00980 156.7 186.8 198(10) 0.01038 156.7 187.2 200(10) 0.01007 156.7 187.7 190(10) 0.01082 156.7 188.3 204(10) 0.00991 156.7 188.9 217(10) 0.00984 156.6 189.5 213(10) 0.00998 156.6 190.1 212(10) 0.00990 156.6 190.7 220(10) 0.00918 156.6 191.3 172(9) 0.01197 156.6 191.8 202(10) 0.00984 156.6 192.3 200(10) 0.01047 156.6 192.7 191(9) 0.01123 156.6 193.1 215(10) 0.00970 156.6 193.4 204(10) 0.01039 156.6 193.5 208(10) 0.01016 156.6 193.6 211(10) 0.00978 156.6 193.7 199(10) 0.01069 156.5 193.6 193(10) 0.01095 156.5 193.6 209(10) 0.00995 156.5 193.4 192(10) 0.01095 156.5 193.3 212(10) 0.00975 156.5 193.2 213(10) 0.00943 156.5 193.1 210(10) 0.01023 156.5 193.1 201(10) 0.01049 156.5 193.1 206(10) 0.00953 156.5 193.2 208(10) 0.01000 156.5 193.3 216(10) 0.00984 156.5 193.6 210(10) 0.00956 156.4 194.0 213(10) 0.00956 156.4 194.5 194(10) 0.01092 156.4 195.1 225(11) 0.00882 156.4 195.8 188(10) 0.01096 156.4 196.7 190(9) 0.01109 156.4 197.8 199(10) 0.01044 156.4 199.0 223(11) 0.00895 156.4 200.4 217(10) 0.00983 156.4 201.9 183(9) 0.01128 156.4 203.7 208(10) 0.00976 156.4 205.6 216(10) 0.01010 156.4 207.8 211(10) 0.01009 156.3 210.1 229(11) 0.00900 156.3 212.7 212(10) 0.01007 156.3 215.5 241(11) 0.00872 156.3 218.5 211(10) 0.00987 156.3 221.7 219(10) 0.00958 156.3 225.1 236(11) 0.00898 156.3 228.8 239(11) 0.00884 156.3 232.6 224(10) 0.00938 156.3 236.7 247(11) 0.00815 156.3 240.9 271(11) 0.00763 156.3 245.2 248(11) 0.00822 156.3 249.7 257(11) 0.00786 156.2 254.2 262(11) 0.00770 156.2 258.7 273(11) 0.00782 156.2 263.2 279(12) 0.00715 156.2 267.5 258(11) 0.00819 156.2 271.6 266(11) 0.00772 156.2 275.4 299(12) 0.00679 156.2 278.8 296(12) 0.00709 156.2 281.7 284(12) 0.00748 156.2 283.9 296(12) 0.00690 156.2 285.5 339(13) 0.00599 156.2 286.3 288(11) 0.00756 156.2 286.4 335(13) 0.00616 156.1 285.6 314(13) 0.00634 156.1 284.2 300(12) 0.00675 156.1 282.0 275(12) 0.00741 156.1 279.2 301(12) 0.00673 156.1 275.8 257(11) 0.00798 156.1 272.0 249(11) 0.00855 156.1 267.9 278(12) 0.00742 156.1 263.5 274(12) 0.00750 156.1 259.0 221(10) 0.00959 156.1 254.4 261(11) 0.00776 156.1 249.8 256(11) 0.00791 156.1 245.2 264(11) 0.00786 156.0 240.7 247(11) 0.00825 156.0 236.3 240(11) 0.00868 156.0 232.1 219(10) 0.00988 156.0 228.1 229(11) 0.00892 156.0 224.2 236(11) 0.00861 156.0 220.6 226(10) 0.00939 156.0 217.2 225(10) 0.00917 156.0 213.9 203(10) 0.01053 156.0 210.8 208(10) 0.01023 156.0 207.9 223(10) 0.00931 156.0 205.3 230(10) 0.00933 156.0 202.8 220(10) 0.00983 155.9 200.5 208(10) 0.01010 155.9 198.4 206(10) 0.00979 155.9 196.5 195(10) 0.01073 155.9 194.7 206(10) 0.01005 155.9 193.1 201(10) 0.01030 155.9 191.6 168(9) 0.01255 155.9 190.2 177(9) 0.01178 155.9 189.0 188(10) 0.01106 155.9 187.9 184(9) 0.01169 155.9 186.8 174(9) 0.01256 155.9 185.9 189(10) 0.01072 155.9 185.1 180(9) 0.01113 155.8 184.3 196(10) 0.01051 155.8 183.7 174(9) 0.01194 155.8 183.1 177(9) 0.01209 155.8 182.5 184(9) 0.01121 155.8 182.1 161(9) 0.01270 155.8 181.6 191(10) 0.01098 155.8 181.3 183(9) 0.01169 155.8 181.0 182(10) 0.01103 155.8 180.7 152(9) 0.01332 155.8 180.5 183(9) 0.01120 155.8 180.4 186(10) 0.01105 155.8 180.2 203(10) 0.01030 155.7 180.2 194(10) 0.01070 155.7 180.1 184(10) 0.01077 155.7 180.1 187(10) 0.01097 155.7 180.2 182(9) 0.01138 155.7 180.3 192(10) 0.01106 155.7 180.4 225(10) 0.00936 155.7 180.6 192(10) 0.01085 155.7 180.8 194(10) 0.01088 155.7 181.0 195(10) 0.01056 155.7 181.4 192(10) 0.01075 155.7 181.7 206(10) 0.00959 155.7 182.2 171(9) 0.01249 155.6 182.6 206(10) 0.01007 155.6 183.2 202(10) 0.01049 155.6 183.8 214(10) 0.00969 155.6 184.5 198(10) 0.01065 155.6 185.3 185(10) 0.01089 155.6 186.2 211(10) 0.00962 155.6 187.1 178(9) 0.01164 155.6 188.2 201(10) 0.01001 155.6 189.3 226(11) 0.00886 155.6 190.6 196(10) 0.01078 155.6 191.9 208(10) 0.00945 155.6 193.4 197(10) 0.01026 155.5 195.0 171(9) 0.01259 155.5 196.7 195(10) 0.01049 155.5 198.6 217(10) 0.00932 155.5 200.6 219(10) 0.00940 155.5 202.7 203(10) 0.01027 155.5 205.0 248(11) 0.00806 155.5 207.4 244(11) 0.00856 155.5 209.9 212(10) 0.00983 155.5 212.6 209(10) 0.00994 155.5 215.4 207(10) 0.01042 155.5 218.3 201(10) 0.01042 155.5 221.4 215(10) 0.00943 155.4 224.5 229(10) 0.00914 155.4 227.7 239(11) 0.00893 155.4 230.9 244(11) 0.00837 155.4 234.2 258(11) 0.00807 155.4 237.4 247(11) 0.00845 155.4 240.5 268(12) 0.00752 155.4 243.5 251(11) 0.00841 155.4 246.3 249(11) 0.00848 155.4 248.9 274(12) 0.00750 155.4 251.1 281(12) 0.00718 155.4 253.0 282(12) 0.00732 155.4 254.4 252(11) 0.00830 155.3 255.4 285(12) 0.00717 155.3 255.8 232(11) 0.00907 155.3 255.8 279(12) 0.00734 155.3 255.3 294(12) 0.00704 155.3 254.3 249(11) 0.00831 155.3 252.9 263(11) 0.00757 155.3 251.1 276(12) 0.00738 155.3 249.0 249(11) 0.00809 155.3 246.7 260(11) 0.00785 155.3 244.1 269(11) 0.00771 155.3 241.5 245(11) 0.00864 155.3 238.8 238(11) 0.00848 155.2 236.1 237(11) 0.00885 155.2 233.5 227(11) 0.00906 155.2 230.9 228(11) 0.00889 155.2 228.4 213(10) 0.00963 155.2 226.1 222(10) 0.00929 155.2 223.9 235(11) 0.00850 155.2 221.9 216(10) 0.00988 155.2 220.0 213(10) 0.00974 155.2 218.4 213(10) 0.00939 155.2 216.9 215(10) 0.00951 155.2 215.7 227(10) 0.00908 155.2 214.7 213(10) 0.00965 155.1 213.9 210(10) 0.00983 155.1 213.3 205(10) 0.01025 155.1 212.9 227(10) 0.00907 155.1 212.7 205(10) 0.00986 155.1 212.7 202(10) 0.01047 155.1 213.0 253(11) 0.00816 155.1 213.4 203(10) 0.01023 155.1 214.0 213(10) 0.00989 155.1 214.9 207(10) 0.01009 155.1 215.9 219(10) 0.00917 155.1 217.0 207(10) 0.00996 155.1 218.4 213(10) 0.00965 155.0 219.8 211(10) 0.00975 155.0 221.4 220(10) 0.00967 155.0 223.2 236(11) 0.00870 155.0 224.9 215(10) 0.00952 155.0 226.8 229(10) 0.00914 155.0 228.6 225(10) 0.00923 155.0 230.4 257(11) 0.00776 155.0 232.2 238(11) 0.00849 155.0 233.8 233(11) 0.00885 155.0 235.3 239(11) 0.00858 155.0 236.5 251(11) 0.00799 155.0 237.5 225(10) 0.00925 154.9 238.1 249(11) 0.00830 154.9 238.5 260(11) 0.00822 154.9 238.4 269(11) 0.00772 154.9 238.0 243(11) 0.00847 154.9 237.3 238(11) 0.00883 154.9 236.2 250(11) 0.00859 154.9 234.8 216(10) 0.01001 154.9 233.2 225(10) 0.00908 154.9 231.3 210(10) 0.00989 154.9 229.2 221(10) 0.00930 154.9 227.0 220(10) 0.00939 154.8 224.8 236(11) 0.00846 154.8 222.4 214(10) 0.00959 154.8 220.1 194(10) 0.01101 154.8 217.8 198(10) 0.01058 154.8 215.5 215(10) 0.00953 154.8 213.4 214(10) 0.00967 154.8 211.3 187(9) 0.01129 154.8 209.3 195(10) 0.01059 154.8 207.4 216(10) 0.00940 154.8 205.6 206(10) 0.01015 154.8 204.0 206(10) 0.00990 154.8 202.5 224(11) 0.00881 154.7 201.2 215(10) 0.00971 154.7 199.9 204(10) 0.00978 154.7 198.9 190(10) 0.01082 154.7 197.9 201(10) 0.01054 154.7 197.1 196(10) 0.01044 154.7 196.5 203(10) 0.01050 154.7 195.9 187(9) 0.01176 154.7 195.5 189(10) 0.01066 154.7 195.2 194(10) 0.01030 154.7 195.1 166(9) 0.01276 154.7 195.1 203(10) 0.01010 154.7 195.1 193(10) 0.01100 154.6 195.3 179(9) 0.01172 154.6 195.6 213(10) 0.00945 154.6 196.0 205(10) 0.00977 154.6 196.5 184(9) 0.01136 154.6 197.0 187(9) 0.01148 154.6 197.7 176(9) 0.01194 154.6 198.3 188(9) 0.01130 154.6 199.0 203(10) 0.01028 154.6 199.7 177(9) 0.01160 154.6 200.4 205(10) 0.01008 154.6 201.1 183(9) 0.01143 154.6 201.8 181(9) 0.01119 154.5 202.3 179(9) 0.01140 154.5 202.8 207(10) 0.00936 154.5 203.1 202(10) 0.01042 154.5 203.4 194(10) 0.01102 154.5 203.5 183(9) 0.01132 154.5 203.4 197(10) 0.01032 154.5 203.3 181(9) 0.01146 154.5 203.0 205(10) 0.00984 154.5 202.6 190(10) 0.01072 154.5 202.1 195(10) 0.01062 154.5 201.6 189(9) 0.01115 154.5 201.1 188(10) 0.01066 154.4 200.5 185(9) 0.01133 154.4 200.0 179(9) 0.01129 154.4 199.5 177(9) 0.01178 154.4 199.0 185(9) 0.01135 154.4 198.7 189(10) 0.01095 154.4 198.3 192(10) 0.01056 154.4 198.1 182(9) 0.01177 154.4 198.0 186(10) 0.01066 154.4 198.0 209(10) 0.00982 154.4 198.1 194(10) 0.01078 154.4 198.3 178(9) 0.01181 154.4 198.6 181(9) 0.01143 154.3 199.1 183(9) 0.01151 154.3 199.8 193(10) 0.01094 154.3 200.5 171(9) 0.01218 154.3 201.4 216(10) 0.00963 154.3 202.5 200(10) 0.01098 154.3 203.7 195(10) 0.01041 154.3 205.0 206(10) 0.00969 154.3 206.6 209(10) 0.00976 154.3 208.2 214(10) 0.00950 154.3 210.0 205(10) 0.00984 154.3 212.0 221(10) 0.00953 154.3 214.1 199(10) 0.01056 154.2 216.4 204(10) 0.01010 154.2 218.8 199(10) 0.01052 154.2 221.3 216(10) 0.00989 154.2 223.9 220(11) 0.00905 154.2 226.6 205(10) 0.01018 154.2 229.3 230(11) 0.00894 154.2 232.1 220(11) 0.00902 154.2 234.9 257(11) 0.00787 154.2 237.7 258(11) 0.00795 154.2 240.4 247(11) 0.00775 154.2 243.0 227(10) 0.00918 154.2 245.3 255(11) 0.00809 154.1 247.5 254(11) 0.00820 154.1 249.4 240(11) 0.00872 154.1 250.9 266(11) 0.00774 154.1 252.2 226(11) 0.00886 154.1 253.0 275(12) 0.00726 154.1 253.5 244(11) 0.00859 154.1 253.6 250(11) 0.00810 154.1 253.3 284(12) 0.00715 154.1 252.8 225(10) 0.00934 154.1 251.9 261(11) 0.00769 154.1 250.9 244(11) 0.00859 154.1 249.6 235(11) 0.00895 154.0 248.3 224(10) 0.00924 154.0 246.9 232(11) 0.00893 154.0 245.6 219(10) 0.00941 154.0 244.2 252(11) 0.00792 154.0 243.0 230(11) 0.00903 154.0 241.9 237(11) 0.00865 154.0 241.0 237(11) 0.00873 154.0 240.3 231(10) 0.00921 154.0 239.8 205(10) 0.01039 154.0 239.5 228(11) 0.00893 154.0 239.6 235(11) 0.00880 154.0 239.9 241(11) 0.00861 153.9 240.4 242(11) 0.00849 153.9 241.3 219(10) 0.00962 153.9 242.6 240(11) 0.00876 153.9 244.1 229(11) 0.00874 153.9 246.0 236(10) 0.00909 153.9 248.2 224(10) 0.00951 153.9 250.8 251(11) 0.00806 153.9 253.7 243(11) 0.00860 153.9 256.9 243(11) 0.00868 153.9 260.5 238(11) 0.00881 153.9 264.4 250(11) 0.00820 153.9 268.7 222(10) 0.00977 153.8 273.3 237(11) 0.00864 153.8 278.1 298(12) 0.00685 153.8 283.2 278(11) 0.00768 153.8 288.6 287(12) 0.00708 153.8 294.1 303(12) 0.00669 153.8 299.8 302(12) 0.00692 153.8 305.5 310(12) 0.00688 153.8 311.2 305(12) 0.00663 153.8 316.8 309(12) 0.00665 153.8 322.3 309(12) 0.00675 153.8 327.3 341(13) 0.00597 153.8 332.0 321(12) 0.00661 153.7 336.1 344(13) 0.00589 153.7 339.5 334(13) 0.00624 153.7 342.1 338(13) 0.00619 153.7 343.9 333(13) 0.00634 153.7 344.7 347(13) 0.00591 153.7 344.5 319(12) 0.00650 153.7 343.4 331(13) 0.00618 153.7 341.2 312(12) 0.00660 153.7 338.2 334(13) 0.00625 153.7 334.4 341(13) 0.00613 153.7 329.8 320(13) 0.00629 153.7 324.6 317(12) 0.00653 153.6 318.8 301(12) 0.00705 153.6 312.8 294(12) 0.00706 153.6 306.5 280(12) 0.00742 153.6 300.0 275(12) 0.00755 153.6 293.4 273(12) 0.00750 153.6 286.9 249(11) 0.00836 153.6 280.5 275(12) 0.00752 153.6 274.1 250(11) 0.00834 153.6 268.0 238(11) 0.00876 153.6 262.0 270(11) 0.00762 153.6 256.3 248(11) 0.00813 153.6 250.8 242(11) 0.00851 153.5 245.5 214(10) 0.00999 153.5 240.5 240(11) 0.00861 153.5 235.8 226(10) 0.00914 153.5 231.3 229(10) 0.00927 153.5 227.1 236(11) 0.00870 153.5 223.1 219(10) 0.00947 153.5 219.4 203(10) 0.01039 153.5 215.9 196(10) 0.01053 153.5 212.6 212(10) 0.00974 153.5 209.6 212(10) 0.00970 153.5 206.7 197(10) 0.01058 153.5 204.1 205(10) 0.00981 153.4 201.6 215(10) 0.00962 153.4 199.3 190(10) 0.01063 153.4 197.2 208(10) 0.00958 153.4 195.2 204(10) 0.01049 153.4 193.4 192(10) 0.01086 153.4 191.7 193(10) 0.01059 153.4 190.1 189(10) 0.01099 153.4 188.6 186(10) 0.01095 153.4 187.3 179(9) 0.01164 153.4 186.0 186(9) 0.01121 153.4 184.8 194(10) 0.01061 153.4 183.8 182(10) 0.01096 153.3 182.8 214(10) 0.00961 153.3 181.8 192(10) 0.01081 153.3 181.0 199(10) 0.01040 153.3 180.2 182(9) 0.01131 153.3 179.4 185(9) 0.01148 153.3 178.7 180(9) 0.01168 153.3 178.1 190(9) 0.01117 153.3 177.5 191(10) 0.01089 153.3 177.0 170(9) 0.01244 153.3 176.5 187(10) 0.01106 153.3 176.0 160(9) 0.01298 153.3 175.6 186(10) 0.01094 153.2 175.3 188(10) 0.01080 153.2 174.9 196(10) 0.01057 153.2 174.6 189(10) 0.01104 153.2 174.4 191(10) 0.01052 153.2 174.1 167(9) 0.01255 153.2 173.9 174(9) 0.01172 153.2 173.8 156(9) 0.01324 153.2 173.6 184(9) 0.01134 153.2 173.6 170(9) 0.01212 153.2 173.5 188(10) 0.01100 153.2 173.5 174(9) 0.01208 153.1 173.5 180(9) 0.01161 153.1 173.6 169(9) 0.01218 153.1 173.7 163(9) 0.01260 153.1 173.8 169(9) 0.01167 153.1 174.0 177(9) 0.01188 153.1 174.3 197(10) 0.01061 153.1 174.5 172(9) 0.01192 153.1 174.9 181(9) 0.01144 153.1 175.2 180(9) 0.01166 153.1 175.7 181(10) 0.01093 153.1 176.1 177(9) 0.01167 153.1 176.6 170(9) 0.01266 153.0 177.2 164(9) 0.01244 153.0 177.8 170(9) 0.01237 153.0 178.4 184(9) 0.01161 153.0 179.1 180(9) 0.01128 153.0 179.8 191(10) 0.01065 153.0 180.5 189(9) 0.01120 153.0 181.3 189(9) 0.01133 153.0 182.1 174(9) 0.01114 153.0 182.9 168(9) 0.01272 153.0 183.7 194(10) 0.01036 153.0 184.4 193(10) 0.01047 153.0 185.2 194(9) 0.01111 152.9 185.8 192(9) 0.01112 152.9 186.5 201(10) 0.01054 152.9 187.0 211(10) 0.00994 152.9 187.4 188(9) 0.01113 152.9 187.7 201(10) 0.00979 152.9 187.9 199(10) 0.01067 152.9 187.9 209(10) 0.01012 152.9 187.9 185(9) 0.01111 152.9 187.6 176(9) 0.01190 152.9 187.3 197(10) 0.01048 152.9 186.9 183(9) 0.01128 152.9 186.3 185(9) 0.01119 152.8 185.7 175(9) 0.01190 152.8 185.0 162(9) 0.01241 152.8 184.3 167(9) 0.01270 152.8 183.6 174(9) 0.01233 152.8 182.8 160(9) 0.01333 152.8 182.1 174(9) 0.01223 152.8 181.3 185(10) 0.01106 152.8 180.6 188(10) 0.01083 152.8 180.0 188(9) 0.01109 152.8 179.4 186(9) 0.01135 152.8 178.8 169(9) 0.01218 152.8 178.3 186(10) 0.01103 152.7 177.9 177(9) 0.01191 152.7 177.6 180(9) 0.01144 152.7 177.3 183(9) 0.01121 152.7 177.0 141(8) 0.01514 152.7 176.9 172(9) 0.01119 152.7 176.8 169(9) 0.01176 152.7 176.8 171(9) 0.01229 152.7 176.9 175(9) 0.01194 152.7 177.0 158(9) 0.01320 152.7 177.2 170(9) 0.01210 152.7 177.5 168(9) 0.01232 152.7 177.8 184(10) 0.01106 152.6 178.2 186(9) 0.01150 152.6 178.7 180(9) 0.01129 152.6 179.2 161(9) 0.01279 152.6 179.8 176(9) . . . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 1 1 0 o 48357.52 49389.50 -180.00 10.34372 100.00 2 0 0 o 4096.529 3319.029 -180.00 7.31412 2.12 2 1 1 o 18708.924 20227.414 27.52 5.97195 25.81 2 2 0 o 12207.166 13737.273 -180.00 5.17186 6.32 3 1 0 o 12566.315 11686.700 0.00 4.62585 10.41 2 2 2 o 43731.79 39883.65 -104.54 4.22281 10.07 3 2 1 o 5138.117 6260.863 -136.61 3.90956 6.08 4 0 0 o 22789.023 22283.125 -180.00 3.65706 2.95 3 3 0 o 1678.678 1543.003 180.00 3.44791 0.39 4 1 1 o 72657.98 66619.68 160.95 3.44791 33.49 4 2 0 o 33010.801 30723.586 0.00 3.27097 13.70 3 3 2 o 22868.527 21971.393 124.55 3.11875 8.63 4 2 2 o 17789.037 15505.699 -0.87 2.98598 6.16 4 3 1 o 6184.393 5874.750 -2.66 2.86883 3.95 5 1 0 o 43703.38 41580.59 0.00 2.86883 13.97 5 2 1 o 21850.453 21415.916 -163.05 2.67074 12.11 4 4 0 o 3871.248 2607.680 -180.00 2.58593 0.50 5 3 0 o 861.461 827.910 0.00 2.50872 0.21 4 3 3 o 17895.576 17153.406 -57.06 2.50872 4.38 4 4 2 o 10189.688 8889.252 149.97 2.43804 2.36 6 0 0 o 53838.19 46241.91 180.00 2.43804 3.11 5 3 2 o 1328.927 1057.500 -30.97 2.37301 0.58 6 1 1 o 3571.429 2801.874 -65.54 2.37301 0.78 6 2 0 o 2212.117 3446.161 0.00 2.31293 0.46 5 4 1 o 1851.351 1449.352 138.57 2.25719 0.73 6 2 2 o 28928.061 26499.611 85.93 2.20529 5.48 6 3 1 o 3002.640 4394.307 159.37 2.15682 1.09 4 4 4 o 6213.478 2866.593 165.22 2.11140 0.36 5 5 0 o 45679.90 40938.67 0.00 2.06874 3.81 5 4 3 o 6208.908 5568.436 84.61 2.06874 2.07 7 1 0 o 16.079 14.442 -180.00 2.06874 0.00 6 4 0 o 2133.675 1977.564 0.00 2.02857 0.34 5 5 2 o 13787.603 14737.057 -34.56 1.99065 2.13 6 3 3 o 307.606 331.412 -54.70 1.99065 0.05 7 2 1 o 265.862 287.144 94.38 1.99065 0.08 6 4 2 o 8116.755 8952.191 -118.80 1.95478 2.42 7 3 0 o 1591.924 658.143 -180.00 1.92078 0.23 6 5 1 o 9749.248 10302.204 156.74 1.85779 2.63 7 3 2 o 4243.853 4515.164 -61.45 1.85779 1.15 8 0 0 o 83399.80 89299.98 0.00 1.82853 2.73 5 5 4 o 4669.768 4637.157 -72.72 1.80061 0.59 7 4 1 o 13338.117 13248.596 -24.64 1.80061 3.39 8 1 1 o 13400.071 13357.593 -104.95 1.80061 1.70 6 4 4 o 7474.725 7019.024 -42.27 1.77393 0.92 8 2 0 o 1624.890 1523.854 0.00 1.77393 0.20 6 5 3 o 228.319 307.350 47.17 1.74841 0.05 8 2 2 o 17008.227 15308.275 141.77 1.72395 1.98 6 6 0 o 26057.313 23609.006 0.00 1.72395 1.52 7 4 3 o 8444.372 8514.211 134.51 1.70050 1.92 7 5 0 o 19804.691 20010.627 -180.00 1.70050 2.25 8 3 1 o 1760.987 1773.478 -152.12 1.70050 0.40 6 6 2 o 588.097 813.830 -156.77 1.67797 0.06 7 5 2 o 7901.451 5791.975 94.92 1.65632 1.70 8 4 0 o 1625.282 1832.205 -180.00 1.63549 0.17 8 3 3 o 3737.859 2627.787 -156.20 1.61542 0.38 9 1 0 o 9024.253 6337.627 -180.00 1.61542 0.93 8 4 2 o 466.831 602.930 150.63 1.59607 0.09 7 6 1 o 4028.959 4267.052 -115.40 1.57740 0.79 6 5 5 o 1612.095 1703.390 51.32 1.57740 0.16 9 2 1 o 9143.073 9605.789 65.81 1.57740 1.79 6 6 4 o 21030.813 24725.389 126.22 1.55937 2.01 7 5 4 o 947.896 1103.150 -122.25 1.54195 0.18 8 5 1 o 11299.734 13150.596 5.90 1.54195 2.12 9 3 0 o 14707.430 17117.016 0.00 1.54195 1.38 7 6 3 o 8848.855 8605.503 -68.70 1.50879 1.59 9 3 2 o 11470.714 11124.633 -52.32 1.50879 2.06 8 4 4 o 27160.787 30041.799 -3.78 1.49299 2.39 9 4 1 o 19935.178 17879.229 147.19 1.47767 3.43 8 5 3 o 1606.742 1441.606 -116.44 1.47767 0.28 7 7 0 o 55480.20 49831.12 0.00 1.47767 2.39 8 6 0 o 6278.461 5730.156 180.00 1.46282 0.53 10 0 0 o 39628.14 36535.34 0.00 1.46282 0.84 7 7 2 o 11569.068 10036.257 84.12 1.44841 0.96 10 1 1 o 15409.071 13493.427 -101.44 1.44841 1.28 8 6 2 o 919.328 685.608 -87.75 1.43442 0.15 10 2 0 o 2148.229 1607.487 -180.00 1.43442 0.17 9 4 3 o 726.996 710.483 144.77 1.42082 0.12 9 5 0 o 1620.075 1573.344 0.00 1.42082 0.13 6 6 6 o 13352.391 14963.422 -131.18 1.40760 0.35 10 2 2 o 9955.605 11390.820 -106.79 1.40760 0.78 9 5 2 o 317.287 249.985 89.84 1.39475 0.05 10 3 1 o 1593.457 1247.452 154.20 1.39475 0.25 7 6 5 o 6452.049 5094.178 -24.48 1.39475 0.99 8 7 1 o 13532.514 13247.032 141.72 1.37006 2.01 7 7 4 o 551.545 539.695 -165.73 1.37006 0.04 8 6 4 o 942.354 906.067 125.70 1.35820 0.14 8 5 5 o 23343.695 22803.414 152.60 1.37006 1.73 9 6 1 o 8202.317 8200.614 -65.60 1.34664 1.18 10 4 0 o 6718.610 6452.093 0.00 1.35820 0.49 10 3 3 o 81885.67 81932.81 88.08 1.34664 5.89 8 7 3 o 2170.933 2397.268 78.80 1.32438 0.30 9 5 4 o 1321.635 1463.029 -39.74 1.32438 0.18 10 4 2 o 6334.060 6621.833 -66.34 1.33537 0.90 11 1 0 o 202.359 225.076 0.00 1.32438 0.01 9 6 3 o 5840.317 5717.578 111.90 1.30319 0.79 10 5 1 o 1271.817 1246.273 -110.78 1.30319 0.17 8 8 0 o 461.921 345.730 0.00 1.29297 0.02 11 2 1 o 9321.975 9178.403 84.48 1.30319 1.26 9 7 0 o 3093.046 3764.237 0.00 1.28298 0.20 8 8 2 o 16060.506 16136.948 -57.42 1.27322 1.04 10 4 4 o 10026.008 10060.351 -172.85 1.27322 0.65 11 3 0 o 1014.404 1251.428 -180.00 1.28298 0.07 9 7 2 o 8756.723 8808.255 -114.90 1.26369 1.11 7 7 6 o 17984.205 18095.086 132.64 1.26369 1.14 10 5 3 o 15509.522 15625.178 -79.80 1.26369 1.97 8 6 6 o 12614.316 9798.974 -49.80 1.25436 0.79 10 6 0 o 714.017 556.074 180.00 1.25436 0.04 11 3 2 o 9276.629 9360.225 -117.87 1.26369 1.18 8 7 5 o 1053.966 1057.210 -18.85 1.24524 0.13 11 4 1 o 4639.844 4678.392 78.66 1.24524 0.57 10 6 2 o 17022.248 16749.930 87.14 1.23631 2.07 8 8 4 o 15556.238 16507.438 -169.47 1.21902 0.92 9 6 5 o 1985.302 1603.694 153.13 1.22757 0.24 9 8 1 o 3139.933 3283.476 -9.77 1.21064 0.37 11 5 0 o 294.363 308.542 0.00 1.21064 0.02 9 7 4 o 15532.995 16260.073 -27.24 1.21064 1.82 11 4 3 o 5062.844 5317.119 -36.04 1.21064 0.59 12 0 0 o 27708.172 29854.979 180.00 1.21902 0.41 10 7 1 o 8838.338 8982.555 110.46 1.19439 1.01 12 2 0 o 0.252 0.215 -180.00 1.20243 0.00 12 1 1 o 3475.131 3660.581 -95.74 1.21064 0.20 11 5 2 o 10033.362 10226.669 99.43 1.19439 1.14 10 5 5 o 10710.605 10923.108 4.07 1.19439 0.61 9 8 3 o 4418.809 4107.012 98.29 1.17878 0.49 10 6 4 o 4614.167 4657.233 126.74 1.18651 0.52 12 2 2 o 17362.980 17652.871 62.16 1.18651 0.98 12 3 1 o 7349.175 6857.680 -88.27 1.17878 0.82 10 7 3 o 9696.979 10517.291 -86.99 1.16376 1.05 11 6 1 o 19923.295 21628.578 -99.33 1.16376 2.16 8 7 7 o 13746.599 13702.749 -58.24 1.14930 0.73 9 9 0 o 11636.197 11589.245 180.00 1.14930 0.31 12 4 0 o 641.839 614.611 0.00 1.15646 0.03 8 8 6 o 7599.172 7347.080 95.99 1.14227 0.40 10 8 0 o 247.029 238.787 0.00 1.14227 0.01 11 5 4 o 1871.957 1866.887 95.38 1.14930 0.20 12 3 3 o 52.656 52.557 -11.94 1.14930 0.00 11 6 3 o 47.508 42.219 -20.04 1.13537 0.00 9 9 2 o 5928.896 5277.979 132.91 1.13537 0.31 9 7 6 o 2961.428 2633.025 118.48 1.13537 0.31 12 4 2 o 724.120 700.685 102.07 1.14227 0.08 10 8 2 o 327.459 260.575 78.21 1.12859 0.03 11 7 0 o 1329.329 1302.459 0.00 1.12193 0.07 9 8 5 o 2656.016 2601.947 -77.06 1.12193 0.27 12 5 1 o 2395.926 2354.905 -169.34 1.12193 0.24 10 6 6 o 18846.545 18563.357 -84.03 1.11539 0.94 13 1 0 o 5382.278 5323.624 0.00 1.12193 0.27 10 7 5 o 7542.749 6825.075 114.80 1.10896 0.75 11 7 2 o 1168.439 1057.641 -21.98 1.10896 0.12 13 2 1 o 3636.415 3275.425 -136.94 1.10896 0.36 9 9 4 o 3677.944 4055.863 54.32 1.09643 0.18 12 5 3 o 927.565 1040.445 -126.33 1.09643 0.09 12 4 4 o 3691.804 3752.438 148.69 1.10264 0.18 10 9 1 o 6.025 5.080 78.96 1.08432 0.00 10 8 4 o 639.130 481.603 95.01 1.09032 0.06 12 6 0 o 485.416 364.328 0.00 1.09032 0.02 13 3 0 o 1072.122 1210.895 0.00 1.09643 0.05 11 6 5 o 479.988 405.327 -57.86 1.08432 0.05 12 6 2 o 1588.219 1393.180 -133.33 1.07841 0.15 13 3 2 o 1455.792 1231.703 146.49 1.08432 0.14 13 4 1 o 36.818 36.901 -122.62 1.07259 0.00 11 7 4 o 4939.592 4920.747 -160.22 1.07259 0.46 11 8 1 o 8143.689 8087.567 -146.28 1.07259 0.76 10 9 3 o 6307.041 4931.694 -79.37 1.06124 0.57 11 8 3 o 3597.404 3700.012 78.29 1.05025 0.32 9 8 7 o 656.710 675.612 178.98 1.05025 0.06 8 8 8 o 6904.471 6357.166 129.89 1.05570 0.10 12 5 5 o 625.834 645.295 110.62 1.05025 0.03 13 4 3 o 665.743 686.863 24.91 1.05025 0.06 12 7 1 o 10599.883 10907.493 55.33 1.05025 0.95 13 5 0 o 3175.250 3271.563 0.00 1.05025 0.14 9 9 6 o 7481.973 7296.688 -50.49 1.03958 0.33 12 6 4 o 6929.487 7164.531 -36.32 1.04487 0.61 10 10 0 o 1263.474 1079.750 0.00 1.03437 0.03 10 8 6 o 282.105 240.252 109.68 1.03437 0.02 13 5 2 o 3202.255 3130.776 -37.38 1.03958 0.28 10 7 7 o 838.006 818.321 -9.09 1.03958 0.04 14 0 0 o 1583.235 1646.001 0.00 1.04487 0.02 12 7 3 o 1915.232 1735.438 113.11 1.02924 0.16 11 9 0 o 7152.586 6461.594 0.00 1.02924 0.31 14 2 0 o 820.848 692.065 0.00 1.03437 0.04 14 1 1 o 11916.653 11690.854 119.62 1.03958 0.52 10 10 2 o 2235.893 1779.097 130.73 1.02418 0.10 10 9 5 o 1184.518 1069.191 123.23 1.01920 0.10 11 7 6 o 1398.121 1263.256 88.51 1.01920 0.12 11 9 2 o 4524.964 4083.608 3.77 1.01920 0.38 14 2 2 o 2295.291 1802.148 -56.79 1.02418 0.10 12 8 0 o 138.227 117.638 0.00 1.01429 0.01 14 3 1 o 5644.072 5109.984 70.36 1.01920 0.48 13 6 1 o 1617.007 1461.390 72.36 1.01920 0.14 11 8 5 o 9703.459 8814.418 -54.08 1.00944 0.80 12 8 2 o 6712.414 6700.705 -140.36 1.00467 0.55 13 5 4 o 1150.161 1044.244 -26.90 1.00944 0.10 13 6 3 o 1731.516 2017.517 140.97 0.99997 0.14 14 4 0 o 1947.603 1943.733 180.00 1.00467 0.08 12 6 6 o 1851.758 1996.125 176.78 0.99533 0.07 10 10 4 o 10605.685 11448.305 -67.32 0.99533 0.43 14 3 3 o 1459.109 1714.137 -83.37 0.99997 0.06 12 7 5 o 1292.311 1358.230 109.89 0.99075 0.10 13 7 0 o 24412.447 25647.225 -180.00 0.99075 0.98 11 9 4 o 7195.651 7555.919 147.47 0.99075 0.58 14 4 2 o 1906.766 2053.957 -83.61 0.99533 0.15 13 7 2 o 367.604 360.852 -8.62 0.98178 0.03 11 10 1 o 193.630 190.251 -84.67 0.98178 0.02 14 5 1 o 2358.450 2313.257 119.46 0.98178 0.19