#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:31:57 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1282 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000065.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000065
loop_
_publ_author_name
'Zhou, Yongkai'
'Adams, Stefan'
'Rao, R. Prasada'
'Edwards, Doreen D.'
'Neiman, Arkady'
'Pestereva, N.'
_publ_section_title
;
 Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3
;
_journal_issue                   20
_journal_name_full               'Chemistry of Materials'
_journal_page_first              6335
_journal_page_last               6345
_journal_paper_doi               10.1021/cm800466y
_journal_volume                  20
_journal_year                    2008
_chemical_formula_moiety         ' Sc2(WO4)3 '
_chemical_formula_sum            'O12 Sc2 W3'
_chemical_formula_weight         833.45
_chemical_melting_point          ' 1913K '
_chemical_name_common            ' Scandium Tungstate '
_chemical_name_systematic        ' Scandium Tungstate '
_space_group_IT_number           60
_space_group_name_Hall           '-P 2a 2n'
_space_group_name_H-M_alt        'P n c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n c a'
_audit_creation_date             2008-01-25T12:03
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2008-01-25T12:03  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.63194(5)
_cell_length_b                   13.35293(7)
_cell_length_c                   9.55447(5)
_cell_measurement_temperature    900
_cell_volume                     1228.845(11)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.68
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id
2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.017
_pd_meas_2theta_range_max        119.9874
_pd_meas_2theta_range_min        10.0144
_pd_meas_number_of_points        6470
_pd_proc_2theta_range_inc        0.017
_pd_proc_2theta_range_max        119.9874
_pd_proc_2theta_range_min        10.0144
_pd_proc_info_datetime           2008-01-25T12:30:04
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    374.923     2:   -30.2971     3:    3.70565     4:    49.4791    
      5:   -5.20035     6:    9.98100     7:   -10.8934     8:    5.26891    
      9:    9.74324    10:   -24.1019    11:    21.9492    12:   -6.34808    
;
_pd_proc_ls_peak_cutoff          0.00250
_pd_proc_ls_pref_orient_corr
;   March-Dollase
 AXIS  1 Ratio=   0.95661  h= 0.000  k= 1.000  l= 0.000
 Prefered orientation correction range: Min=   0.93562, Max=   1.14235
;
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =    5.296 #2(GV)   =   -4.085 #3(GW)   =    1.920
 #4(GP)   =    0.000 #5(LX)   =    0.855 #6(LY)   =    5.274
 #7(S/L)  =   0.0316 #8(H/L)  =   0.0250
 #9(trns) =     0.00 #10(shft)= -11.6315
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0025 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0500
_pd_proc_ls_prof_wR_expected     0.0362
_pd_proc_ls_prof_wR_factor       0.0654
_pd_proc_number_of_points        6470
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.85
_refine_ls_matrix_type           full
_refine_ls_number_parameters     51
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.06851
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        0.890
_reflns_d_resolution_low         6.676
_reflns_limit_h_max              10
_reflns_limit_h_min              0
_reflns_limit_k_max              15
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_total             1828
_cod_data_source_file            cm800466y_si_019.cif
_cod_data_source_block           T900K
_cod_original_cell_volume        1228.844(13)
_cod_database_code               4000065
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,+z+1/2
3 +x,-y+1/2,+z+1/2
4 -x+1/2,-y,+z
-1 -x,-y,-z
-2 +x+1/2,-y+1/2,-z+1/2
-3 -x,+y+1/2,-z+1/2
-4 +x+1/2,+y,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Sc Sc1 0.4703(4) 0.38180(25) 0.2469(5) 1.0 Uiso 0.0262(12) 8
W W1 0.25 0.0 0.47133(15) 1.0 Uiso 0.02815(31) 4
W W2 0.11298(11) 0.35645(8) 0.39118(12) 1.0 Uiso 0.02815(31) 8
O O1 0.0918(13) 0.1270(9) 0.0682(13) 1.0 Uiso 0.0622(19) 8
O O2 0.1520(13) 0.0756(9) 0.3722(14) 1.0 Uiso 0.0622(19) 8
O O3 0.0047(13) 0.2646(10) 0.3155(12) 1.0 Uiso 0.0622(19) 8
O O4 0.3351(13) 0.4052(8) 0.0732(13) 1.0 Uiso 0.0622(19) 8
O O5 0.0592(12) 0.4749(10) 0.3215(13) 1.0 Uiso 0.0622(19) 8
O O6 0.2919(14) 0.3479(9) 0.3419(13) 1.0 Uiso 0.0622(19) 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800
51.3531 1.33290 International_Tables_Vol_C
W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982
57.0560 9.88750 International_Tables_Vol_C
O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540500 1.000 K\a~1~ 1
1.544300 0.000 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sc1 O2 90.4(5) -2_666 . -2_666 N
O1 Sc1 O3 95.7(5) -2_666 . -2_666 N
O1 Sc1 O4 173.0(5) -2_666 . 1_555 N
O1 Sc1 O5 80.8(5) -2_666 . 4_565 N
O1 Sc1 O6 94.8(5) -2_666 . 1_555 N
O2 Sc1 O3 88.2(5) -2_666 . -2_666 N
O2 Sc1 O4 92.6(5) -2_666 . 1_555 N
O2 Sc1 O5 92.8(5) -2_666 . 4_565 N
O2 Sc1 O6 174.5(6) -2_666 . 1_555 N
O3 Sc1 O4 90.7(5) -2_666 . 1_555 N
O3 Sc1 O5 176.3(5) -2_666 . 4_565 N
O3 Sc1 O6 93.1(5) -2_666 . 1_555 N
O4 Sc1 O5 92.8(5) 1_555 . 4_565 N
O4 Sc1 O6 82.0(5) 1_555 . 1_555 N
O5 Sc1 O6 86.2(5) 4_565 . 1_555 N
O2 W1 O2 111.2(9) 1_555 . 4_555 N
O2 W1 O4 118.3(6) 1_555 . 2_545 N
O2 W1 O4 98.0(6) 1_555 . 3_555 N
O2 W1 O4 98.0(6) 4_555 . 2_545 N
O2 W1 O4 118.3(6) 4_555 . 3_555 N
O4 W1 O4 114.3(8) 2_545 . 3_555 N
O1 W2 O3 115.0(6) 3_555 . 1_555 N
O1 W2 O5 102.6(5) 3_555 . 1_555 N
O1 W2 O6 112.4(6) 3_555 . 1_555 N
O3 W2 O5 106.9(6) 1_555 . 1_555 N
O3 W2 O6 114.6(6) 1_555 . 1_555 N
O5 W2 O6 103.7(5) 1_555 . 1_555 N
Sc1 O1 W2 153.1(7) -2_466 . 3_554 N
Sc1 O2 W1 155.7(7) -2_555 . 1_555 N
Sc1 O3 W2 150.3(7) -2_466 . 1_555 N
Sc1 O4 W1 143.6(7) 1_555 . 2_554 N
Sc1 O5 W2 170.8(7) 4_565 . 1_555 N
Sc1 O6 W2 159.1(8) 1_555 . 1_555 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sc1 O1 2.123(13) . -2_555 N
Sc1 O2 2.163(13) . -2_555 N
Sc1 O3 2.070(13) . -2_555 N
Sc1 O4 2.132(12) . 1_555 N
Sc1 O5 2.062(12) . 4_565 N
Sc1 O6 1.996(13) . 1_555 N
W1 O2 1.675(13) . 1_555 N
W1 O2 1.675(13) . 4_555 N
W1 O4 1.795(11) . 2_545 N
W1 O4 1.795(11) . 3_555 N
W2 O1 1.718(12) . 3_555 N
W2 O3 1.765(12) . 1_555 N
W2 O5 1.792(12) . 1_555 N
W2 O6 1.790(13) . 1_555 N
O1 Sc1 2.123(13) . -2_455 N
O1 W2 1.718(12) . 3_554 N
O2 Sc1 2.163(13) . -2_455 N
O2 W1 1.675(13) . 1_555 N
O3 Sc1 2.070(13) . -2_455 N
O3 W2 1.765(12) . 1_555 N
O4 Sc1 2.132(12) . 1_555 N
O4 W1 1.795(11) . 2_554 N
O5 Sc1 2.062(12) . 4_565 N
O5 W2 1.792(12) . 1_555 N
O6 Sc1 1.996(13) . 1_555 N
O6 W2 1.790(13) . 1_555 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
335.0 0.0 677.38654 .
336.0 0.0 673.53168 .
331.0 0.0 669.70624 .
316.0 0.0 665.90979 .
325.0 0.0 662.14185 .
326.0 0.0 658.40332 .
343.0 0.0 654.69305 .
338.0 0.0 651.01111 .
376.0 0.0 647.35797 .
336.0 0.0 643.73236 .
340.0 0.0 640.13525 .
362.0 0.0 636.56592 .
345.0 0.0 633.02417 .
349.0 0.0 629.51025 .
342.0 0.0 626.02380 .
335.0 0.0 622.56470 .
331.0 0.0 619.13263 .
325.0 0.0 615.72736 .
333.0 0.0 612.34961 .
330.0 0.0 608.99854 .
323.0 0.0 605.67395 .
340.0 0.0 602.37585 .
345.0 0.0 599.10388 .
346.0 0.0 595.85858 .
336.0 0.0 592.63947 .
348.0 0.0 589.44598 .
351.0 0.0 586.27844 .
344.0 0.0 583.13654 .
336.0 0.0 580.02014 .
337.0 0.0 576.92963 .
353.0 0.0 573.86389 .
355.0 0.0 570.82349 .
336.0 0.0 567.80792 .
325.0 0.0 564.81775 .
330.0 0.0 561.85229 .
341.0 0.0 558.91132 .
328.0 0.0 555.99481 .
331.0 0.0 553.10248 .
356.0 0.0 550.23486 .
360.0 0.0 547.39136 .
345.0 0.0 544.57166 .
355.0 0.0 541.77594 .
337.0 0.0 539.00372 .
338.0 0.0 536.25549 .
325.0 0.0 533.53082 .
311.0 0.0 530.82928 .
332.0 0.0 528.15106 .
344.0 0.0 525.49579 .
338.0 0.0 522.86383 .
307.0 0.0 520.25476 .
336.0 0.0 517.66852 .
324.0 0.0 515.10455 .
335.0 0.0 512.56323 .
378.0 0.0 510.04440 .
314.0 0.0 507.54791 .
317.0 0.0 505.07367 .
346.0 0.0 502.62125 .
332.0 0.0 500.19067 .
330.0 0.0 497.78220 .
304.0 0.0 495.39536 .
358.0 0.0 493.03009 .
339.0 0.0 490.68604 .
358.0 0.0 488.36331 .
335.0 0.0 486.06201 .
343.0 0.0 483.78192 .
331.0 0.0 481.52277 .
350.0 0.0 479.28424 .
353.0 0.0 477.06653 .
357.0 0.0 474.86954 .
360.0 0.0 472.69321 .
356.0 0.0 470.53726 .
348.0 0.0 468.40143 .
343.0 0.0 466.28589 .
344.0 0.0 464.19031 .
339.0 0.0 462.11505 .
328.0 0.0 460.05945 .
328.0 0.0 458.02338 .
324.0 0.0 456.00720 .
361.0 0.0 454.01038 .
340.0 0.0 452.03317 .
343.0 0.0 450.07532 .
385.0 0.0 448.13644 .
374.0 0.0 446.21664 .
355.0 0.0 444.31583 .
348.0 0.0 442.43411 .
365.0 0.0 440.57108 .
362.0 0.0 438.72662 .
348.0 0.0 436.90079 .
347.0 0.0 435.09335 .
345.0 0.0 433.30435 .
349.0 0.0 431.53366 .
337.0 0.0 429.78085 .
327.0 0.0 428.04614 .
318.0 0.0 426.32944 .
342.0 0.0 424.63062 .
368.0 0.0 422.94955 .
354.0 0.0 421.28583 .
337.0 0.0 419.63980 .
327.0 0.0 418.01117 .
337.0 0.0 416.39993 .
334.0 0.0 414.80603 .
321.0 0.0 413.22894 .
316.0 0.0 411.66901 .
347.0 0.0 410.12610 .
343.0 0.0 408.59982 .
333.0 0.0 407.09042 .
356.0 0.0 405.59744 .
323.0 0.0 404.12115 .
335.0 0.0 402.66132 .
317.0 0.0 401.21768 .
330.0 0.0 399.79044 .
326.0 0.0 398.37915 .
341.0 0.0 396.98389 .
378.0 0.0 395.60483 .
357.0 0.0 394.24139 .
330.0 0.0 392.89380 .
328.0 0.0 391.56180 .
325.0 0.003077 390.24527 390.24118
318.0 0.003145 388.94446 388.94037
352.0 0.002841 387.65891 387.65485
388.0 0.002577 386.38864 386.38464
322.0 0.003106 385.13367 385.12967
350.0 0.002857 383.89362 383.88962
351.0 0.002849 382.66870 382.66479
350.0 0.002857 381.45871 381.45468
321.0 0.003115 380.26355 380.25964
333.0 0.003003 379.08304 379.07916
355.0 0.002817 377.91711 377.91324
353.0 0.002833 376.76590 376.76208
347.0 0.002882 375.62909 375.62531
362.0 0.002762 374.50671 374.50296
327.0 0.003058 373.39856 373.39484
322.0 0.003106 372.30460 372.30084
335.0 0.002985 371.22485 371.22110
358.0 0.002793 370.15906 370.15540
358.0 0.002793 369.10724 369.10358
346.0 0.002890 368.06918 368.06558
343.0 0.002915 367.04495 367.04123
344.0 0.002907 366.03439 366.03082
349.0 0.002865 365.03748 365.03391
339.0 0.002950 364.05408 364.05054
333.0 0.003003 363.08398 363.08047
345.0 0.002899 362.12720 362.12366
353.0 0.002833 361.18384 361.18036
339.0 0.002950 360.25360 360.25009
360.0 0.002778 359.33640 359.33298
361.0 0.002770 358.43219 358.42874
327.0 0.003058 357.54089 357.53745
324.0 0.003086 356.66248 356.65915
325.0 0.003077 355.79681 355.79349
323.0 0.003096 354.94382 354.94049
328.0 0.003049 354.10342 354.10010
330.0 0.003030 353.27542 353.27213
331.0 0.003021 352.45996 352.45667
334.0 0.002994 351.65689 351.65359
335.0 0.002985 350.86603 350.86273
327.0 0.003058 350.08734 350.08414
345.0 0.002899 349.32071 349.31747
349.0 0.002865 348.56622 348.56299
360.0 0.002778 347.82367 347.82037
366.0 0.002732 347.09290 347.08972
360.0 0.002778 346.37402 346.37079
337.0 0.002967 345.66675 345.66357
330.0 0.003030 344.97119 344.96805
400.0 0.002500 344.28723 348.29465
352.0 0.002841 343.61465 347.96698
364.0 0.002747 342.95355 349.70819
353.0 0.002833 342.30374 349.69485
389.0 0.002571 341.66519 349.80444
346.0 0.002890 341.03784 350.07187
385.0 0.002597 340.42163 350.55157
365.0 0.002740 339.81631 351.33929
392.0 0.002551 339.22205 352.68954
390.0 0.002564 338.63867 355.66962
437.0 0.002288 338.06613 363.13901
416.0 0.002404 337.50427 377.49783
418.0 0.002392 336.95303 398.42560
424.0 0.002358 336.41232 424.85471
480.0 0.002083 335.88229 455.41724
504.0 0.001984 335.36264 489.19360
468.0 0.002137 334.85339 526.15955
498.0 0.002008 334.35431 566.68463
537.0 0.001862 333.86560 611.30188
630.0 0.001587 333.38696 660.65857
656.0 0.001524 332.91840 715.52112
754.0 0.001326 332.45990 776.89423
822.0 0.001217 332.01132 846.23499
896.0 0.001116 331.57260 925.42963
963.0 0.001038 331.14368 1016.85315
1058.0 0.000945 330.72452 1124.11755
1203.0 0.000831 330.31503 1252.29895
1440.0 0.000694 329.91513 1409.24683
1698.0 0.000589 329.52478 1607.85181
2169.0 0.000461 329.14377 1871.47668
2791.0 0.000358 328.77228 2251.99902
3525.0 0.0002837 328.41010 2876.51660
4265.0 0.0002345 328.05716 3767.37842
4186.0 0.0002389 327.71335 3944.00269
3151.0 0.0003174 327.37869 2886.03906
2001.0 0.000500 327.05316 1941.84277
1117.0 0.000895 326.73660 1020.05176
659.0 0.001517 326.42889 576.73358
486.0 0.002058 326.13013 457.17322
441.0 0.002268 325.84015 415.19937
413.0 0.002421 325.55884 391.66779
382.0 0.002618 325.28622 376.45514
364.0 0.002747 325.02228 365.94431
376.0 0.002660 324.76678 358.32260
393.0 0.002545 324.51981 352.58472
383.0 0.002611 324.28122 348.13336
365.0 0.002740 324.05099 344.59378
362.0 0.002762 323.82910 341.72095
371.0 0.002695 323.61526 339.34851
379.0 0.002639 323.40976 337.36011
357.0 0.002801 323.21234 335.67188
342.0 0.002924 323.02295 334.22250
380.0 0.002632 322.84146 332.96594
371.0 0.002695 322.66794 331.86731
345.0 0.002899 322.50232 330.89966
342.0 0.002924 322.34442 325.19321
386.0 0.002591 322.19427 322.19116
382.0 0.002618 322.05176 322.04874
358.0 0.002793 321.91693 321.91382
388.0 0.002577 321.78967 321.78653
341.0 0.002933 321.66980 321.66669
335.0 0.002985 321.55750 321.55432
361.0 0.002770 321.45245 321.44934
334.0 0.002994 321.35477 321.35165
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431.0 0.002320 409.24872 449.61371
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624.0 0.001603 408.06479 597.19037
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2158.0 0.000463 407.06873 2033.30591
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1494.0 0.000669 406.57724 1417.37036
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2715.0 0.000368 405.76810 2892.86475
3531.0 0.0002832 405.60785 3849.86011
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628.0 0.001592 402.21039 658.24359
536.0 0.001866 402.06198 549.59039
459.0 0.002179 401.91400 492.72800
450.0 0.002222 401.76669 473.20535
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439.0 0.002278 400.89371 425.42661
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414.0 0.002415 400.60703 415.71490
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438.0 0.002283 400.32254 416.33301
429.0 0.002331 400.18106 421.87979
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431.0 0.002320 399.89981 433.96747
432.0 0.002315 399.75998 448.68274
432.0 0.002315 399.62076 468.92899
457.0 0.002188 399.48206 500.31964
484.0 0.002066 399.34378 548.07605
568.0 0.001761 399.20621 613.23615
568.0 0.001761 399.06915 633.93701
491.0 0.002037 398.93268 552.31134
455.0 0.002198 398.79672 496.00797
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477.0 0.002096 398.52646 516.55310
493.0 0.002028 398.39209 517.29834
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392.0 0.002551 397.86041 420.84998
419.0 0.002387 397.72891 420.68427
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410.0 0.002439 397.46756 424.45407
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464.0 0.002155 397.20837 435.95798
489.0 0.002045 397.07965 445.65451
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544.0 0.001838 396.82394 504.09558
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721.0 0.001387 396.57034 671.65033
777.0 0.001287 396.44449 802.82507
936.0 0.001068 396.31918 990.85754
1281.0 0.000781 396.19443 1271.18799
1930.0 0.000518 396.07019 1709.86230
2414.0 0.000414 395.94659 2255.74341
2287.0 0.000437 395.82355 2263.69995
1441.0 0.000694 395.70105 1519.91064
1059.0 0.000944 395.57913 1130.90588
1213.0 0.000824 395.45770 1164.01343
1423.0 0.000703 395.33701 1356.50439
1324.0 0.000755 395.21674 1311.87488
890.0 0.001124 395.09714 883.93085
592.0 0.001689 394.97809 613.71979
483.0 0.002070 394.85956 523.30005
465.0 0.002151 394.74164 492.87952
495.0 0.002020 394.62433 479.65167
492.0 0.002033 394.50757 475.29776
524.0 0.001908 394.39145 479.25269
556.0 0.001799 394.27570 495.46698
578.0 0.001730 394.16064 528.84131
614.0 0.001629 394.04617 583.61267
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830.0 0.001205 393.81900 791.80988
1043.0 0.000959 393.70627 979.37610
1369.0 0.000730 393.59418 1274.78552
1795.0 0.000557 393.48254 1703.26807
2032.0 0.000492 393.37158 2063.08740
1935.0 0.000517 393.26120 1929.00464
1932.0 0.000518 393.15134 1879.46704
2360.0 0.000424 393.04208 2252.05420
2527.0 0.000396 392.93338 2492.22241
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1533.0 0.000652 392.71777 1437.15662
1247.0 0.000802 392.61084 1178.90063
1307.0 0.000765 392.50452 1232.64600
1311.0 0.000763 392.39877 1254.84644
1043.0 0.000959 392.29364 942.70581
753.0 0.001328 392.18903 685.59192
634.0 0.001577 392.08496 618.54419
655.0 0.001527 391.98157 641.03271
681.0 0.001468 391.87866 704.71417
780.0 0.001282 391.77652 812.08923
943.0 0.001060 391.67480 976.41449
1283.0 0.000779 391.57370 1247.50269
1691.0 0.000591 391.47324 1627.71619
1719.0 0.000582 391.37332 1779.34155
1289.0 0.000776 391.27396 1410.81250
1103.0 0.000907 391.17526 1211.39551
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2290.0 0.000437 390.88257 2109.66016
2118.0 0.000472 390.78610 2087.32007
1396.0 0.000716 390.69037 1483.35864
936.0 0.001068 390.59518 1006.14874
863.0 0.001159 390.50049 907.28638
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912.0 0.001096 390.22015 885.39337
605.0 0.001653 390.12790 622.18658
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436.0 0.002294 389.94513 468.76651
462.0 0.002165 389.85464 451.61404
440.0 0.002273 389.76471 441.01349
426.0 0.002347 389.67538 435.03058
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452.0 0.002212 389.49847 428.74414
441.0 0.002268 389.41086 428.77048
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467.0 0.002141 389.23758 434.63019
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507.0 0.001972 388.98193 494.54196
535.0 0.001869 388.89792 554.79675
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740.0 0.001351 388.73169 773.54388
930.0 0.001075 388.64935 950.19208
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1550.0 0.000645 388.32626 1576.42871
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862.0 0.001160 388.16827 924.67493
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412.0 0.002427 386.98895 398.04837
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402.0 0.002488 386.71768 395.65466
418.0 0.002392 386.65131 395.24356
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399.0 0.002506 386.45578 394.56940
403.0 0.002481 386.39175 401.38519
391.0 0.002558 386.32834 401.88516
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380.0 0.002632 386.20325 401.41605
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421.0 0.002375 386.08047 407.14120
388.0 0.002577 386.02002 408.90021
415.0 0.002410 385.96008 410.98114
396.0 0.002525 385.90076 412.49905
405.0 0.002469 385.84201 415.55603
432.0 0.002315 385.78387 419.28662
420.0 0.002381 385.72626 423.94354
450.0 0.002222 385.66925 429.93875
468.0 0.002137 385.61282 438.06241
470.0 0.002128 385.55701 450.88538
487.0 0.002053 385.50183 473.62332
548.0 0.001825 385.44711 514.75769
625.0 0.001600 385.39297 576.39886
702.0 0.001425 385.33954 667.58405
785.0 0.001274 385.28656 792.43860
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1358.0 0.000736 385.18246 1261.90820
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1362.0 0.000734 385.03061 1148.93372
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1750.0 0.000571 384.88397 1746.80249
2174.0 0.000460 384.83621 2201.37451
2598.0 0.000385 384.78912 2620.19849
3626.0 0.0002758 384.74252 3412.41968
4979.0 0.0002008 384.69641 4778.36865
5526.0 0.0001810 384.65109 5726.15723
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2470.0 0.000405 384.56192 2563.95337
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2957.0 0.0003382 384.43253 3038.47754
2649.0 0.000378 384.39056 2660.48120
1610.0 0.000621 384.34912 1509.24280
909.0 0.001100 384.30835 899.34637
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621.0 0.001610 384.22827 645.74750
632.0 0.001582 384.18921 632.68634
685.0 0.001460 384.15060 652.20752
738.0 0.001355 384.11261 708.95691
780.0 0.001282 384.07516 772.79340
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643.0 0.001555 384.00198 622.72388
590.0 0.001695 383.96622 599.29797
620.0 0.001613 383.93109 643.35388
659.0 0.001517 383.89645 727.62543
747.0 0.001339 383.86243 809.20953
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1009.0 0.000991 383.79605 1012.26031
1103.0 0.000907 383.76373 1188.69543
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910.0 0.001099 383.70068 940.21857
874.0 0.001144 383.66998 969.43134
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1511.0 0.000662 383.61035 1504.67273
1806.0 0.000554 383.58130 1717.13782
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884.0 0.001131 383.52502 893.54767
669.0 0.001495 383.49768 751.35480
765.0 0.001307 383.47101 789.56543
927.0 0.001079 383.44473 889.00500
862.0 0.001160 383.41910 865.47449
629.0 0.001590 383.39392 643.04333
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442.0 0.002262 383.34546 447.62811
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378.0 0.002646 383.19281 396.35193
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402.0 0.002488 383.15411 393.31735
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420.0 0.002381 383.02118 387.04605
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370.0 0.002703 382.99329 386.50583
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400.0 0.002500 382.96762 385.76245
382.0 0.002618 382.95560 384.36761
362.0 0.002762 382.94409 384.33209
388.0 0.002577 382.93307 384.30984
379.0 0.002639 382.92270 384.30127
365.0 0.002740 382.91278 384.30667
371.0 0.002695 382.90332 383.67996
378.0 0.002646 382.89450 383.75757
379.0 0.002639 382.88614 383.85123
384.0 0.002604 382.87836 383.96500
389.0 0.002571 382.87109 384.10464
398.0 0.002513 382.86438 384.27762
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1577.0 0.000634 384.36298 1478.56702
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630.0 0.001587 384.43884 634.20496
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817.0 0.001224 384.71759 737.33325
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654.0 0.001529 385.24234 564.48419
761.0 0.001314 385.28867 614.24756
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2353.0 0.000425 385.87527 2426.96094
3138.0 0.0003187 385.92670 3048.23389
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849.0 0.001178 386.18927 849.62622
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1519.0 0.000658 386.35129 1379.42896
1832.0 0.000546 386.40607 1609.23413
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1193.0 0.000838 386.51660 1193.59729
1233.0 0.000811 386.57242 1209.80078
1527.0 0.000655 386.62866 1432.25940
2111.0 0.000474 386.68518 1787.85510
2181.0 0.000459 386.74222 1860.26025
1559.0 0.000641 386.79941 1351.08276
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987.0 0.001013 387.15057 858.27057
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2316.0 0.000432 387.45276 2285.71338
2751.0 0.000364 387.51431 2779.84668
2796.0 0.000358 387.57605 2861.29004
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1759.0 0.000569 388.01813 1922.73279
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1737.0 0.000576 388.14740 1784.10742
1120.0 0.000893 388.21249 1112.09717
788.0 0.001269 388.27795 753.70892
653.0 0.001531 388.34369 628.56891
635.0 0.001575 388.40985 587.58929
632.0 0.001582 388.47623 590.74310
652.0 0.001534 388.54297 631.40955
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1197.0 0.000835 388.74509 1057.35059
1565.0 0.000639 388.81308 1365.97937
1739.0 0.000575 388.88138 1600.48828
1428.0 0.000700 388.94992 1324.55249
962.0 0.001040 389.01886 927.11725
781.0 0.001280 389.08807 812.81470
879.0 0.001138 389.15768 887.14807
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1198.0 0.000835 389.50977 1156.94897
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747.0 0.001339 389.65277 702.61621
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723.0 0.001383 389.79688 700.55066
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624.0 0.001603 404.87616 602.50128
665.0 0.001504 404.97635 640.85181
830.0 0.001205 405.07651 717.85889
941.0 0.001063 405.17679 772.09686
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616.0 0.001623 405.87964 594.65802
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3438.0 0.0002909 406.48318 3367.94995
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1194.0 0.000838 406.88596 1324.80481
1426.0 0.000701 406.98679 1577.03162
1862.0 0.000537 407.08740 1946.65100
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1632.0 0.000613 407.28897 1622.58411
992.0 0.001008 407.38977 1010.10760
700.0 0.001429 407.49054 738.58252
586.0 0.001706 407.59134 661.73962
603.0 0.001658 407.69211 639.05176
557.0 0.001795 407.79291 588.78882
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485.0 0.002062 407.99448 505.48282
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526.0 0.001901 408.19611 521.27942
555.0 0.001802 408.29694 552.87683
601.0 0.001664 408.39771 597.60974
622.0 0.001608 408.49847 608.34912
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470.0 0.002128 408.90152 482.78180
486.0 0.002058 409.00223 500.39487
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447.0 0.002237 409.30432 477.54440
423.0 0.002364 409.40497 457.91010
435.0 0.002299 409.50558 455.04053
440.0 0.002273 409.60620 456.55045
462.0 0.002165 409.70688 470.82010
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515.0 0.001942 409.90796 525.46887
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473.0 0.002114 410.20944 487.07666
481.0 0.002079 410.30988 480.56937
518.0 0.001931 410.41028 493.72604
537.0 0.001862 410.51068 519.55115
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663.0 0.001508 410.71124 617.18616
748.0 0.001337 410.81158 707.05896
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1716.0 0.000583 411.11203 1633.56665
2327.0 0.000430 411.21216 2172.12598
2456.0 0.000407 411.31226 2233.48926
1606.0 0.000623 411.41232 1541.57178
991.0 0.001009 411.51224 1018.85034
850.0 0.001176 411.61212 886.03418
913.0 0.001095 411.71204 970.46521
1228.0 0.000814 411.81183 1183.03796
1473.0 0.000679 411.91162 1414.76465
1490.0 0.000671 412.01132 1339.91113
1077.0 0.000929 412.11093 995.21704
838.0 0.001193 412.21060 826.27478
871.0 0.001148 412.31012 847.91772
991.0 0.001009 412.40967 943.73798
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560.0 0.001786 412.80701 560.89124
551.0 0.001815 412.90619 580.96613
615.0 0.001626 413.00531 631.68933
656.0 0.001524 413.10437 684.17267
646.0 0.001548 413.20328 649.46246
570.0 0.001754 413.30225 547.46869
493.0 0.002028 413.40115 489.15030
445.0 0.002247 413.49985 467.72659
462.0 0.002165 413.59851 459.90024
466.0 0.002146 413.69720 456.77585
459.0 0.002179 413.79578 456.37326
439.0 0.002278 413.89429 458.09052
465.0 0.002151 413.99265 462.04019
476.0 0.002101 414.09097 469.01324
495.0 0.002020 414.18918 482.23120
527.0 0.001898 414.28735 504.56274
589.0 0.001698 414.38544 550.87738
697.0 0.001435 414.48343 624.00031
833.0 0.001200 414.58136 753.18372
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417.0 . . .
