#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:31:32 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1279 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000061.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000061
loop_
_publ_author_name
'Zhou, Yongkai'
'Adams, Stefan'
'Rao, R. Prasada'
'Edwards, Doreen D.'
'Neiman, Arkady'
'Pestereva, N.'
_publ_section_title
;
 Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3
;
_journal_issue                   20
_journal_name_full               'Chemistry of Materials'
_journal_page_first              6335
_journal_page_last               6345
_journal_paper_doi               10.1021/cm800466y
_journal_volume                  20
_journal_year                    2008
_chemical_formula_moiety         ' Sc2(WO4)3 '
_chemical_formula_sum            'O12 Sc2 W3'
_chemical_formula_weight         833.45
_chemical_melting_point          ' 1913K '
_chemical_name_common            ' Scandium Tungstate '
_chemical_name_systematic        ' Scandium Tungstate '
_space_group_IT_number           60
_space_group_name_Hall           '-P 2a 2n'
_space_group_name_H-M_alt        'P n c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n c a'
_audit_creation_date             2008-01-25T12:03
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2008-01-25T12:03  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.66276(6)
_cell_length_b                   13.33496(8)
_cell_length_c                   9.57504(6)
_cell_measurement_temperature    400
_cell_volume                     1233.768(13)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.68
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id
2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.017
_pd_meas_2theta_range_max        119.9874
_pd_meas_2theta_range_min        10.0144
_pd_meas_number_of_points        6470
_pd_proc_2theta_range_inc        0.017
_pd_proc_2theta_range_max        119.9874
_pd_proc_2theta_range_min        10.0144
_pd_proc_info_datetime           2008-01-25T12:07:56
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    314.299     2:   -52.8852     3:    37.6447     4:    31.1906    
      5:   -9.46692     6:    13.7145     7:   -9.99606     8:    4.82981    
      9:    7.01768    10:   -18.4546    11:    18.6642    12:   -6.35775    
;
_pd_proc_ls_peak_cutoff          0.00250
_pd_proc_ls_pref_orient_corr
;   March-Dollase
 AXIS  1 Ratio=   0.95224  h= 0.000  k= 1.000  l= 0.000
 Prefered orientation correction range: Min=   0.92921, Max=   1.15818
;
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =   18.320 #2(GV)   =   -6.899 #3(GW)   =    2.348
 #4(GP)   =    0.000 #5(LX)   =    0.654 #6(LY)   =    7.181
 #7(S/L)  =   0.0322 #8(H/L)  =   0.0250
 #9(trns) =     0.00 #10(shft)=  -1.2949
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0025 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0484
_pd_proc_ls_prof_wR_expected     0.0356
_pd_proc_ls_prof_wR_factor       0.0643
_pd_proc_number_of_points        6470
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.85
_refine_ls_matrix_type           full
_refine_ls_number_parameters     51
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.04520
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        0.890
_reflns_d_resolution_low         6.667
_reflns_limit_h_max              10
_reflns_limit_h_min              0
_reflns_limit_k_max              15
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_total             1837
_cod_data_source_file            cm800466y_si_009.cif
_cod_data_source_block           T400K
_cod_original_cell_volume        1233.769(15)
_cod_database_code               4000061
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,+z+1/2
3 +x,-y+1/2,+z+1/2
4 -x+1/2,-y,+z
-1 -x,-y,-z
-2 +x+1/2,-y+1/2,-z+1/2
-3 -x,+y+1/2,-z+1/2
-4 +x+1/2,+y,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Sc Sc1 0.46764(32) 0.38098(22) 0.2488(4) 1.0 Uiso 0.0185(10) 8
W W1 0.25 0.0 0.47255(13) 1.0 Uiso 0.01708(24) 4
W W2 0.11562(9) 0.35615(7) 0.39366(10) 1.0 Uiso 0.01708(24) 8
O O1 0.0906(10) 0.1350(7) 0.0751(10) 1.0 Uiso 0.0290(14) 8
O O2 0.1379(11) 0.0677(7) 0.3676(11) 1.0 Uiso 0.0290(14) 8
O O3 0.0076(11) 0.2641(8) 0.3189(10) 1.0 Uiso 0.0290(14) 8
O O4 0.3336(10) 0.4069(7) 0.0789(10) 1.0 Uiso 0.0290(14) 8
O O5 0.0662(9) 0.4764(8) 0.3243(10) 1.0 Uiso 0.0290(14) 8
O O6 0.2940(11) 0.3404(7) 0.3523(10) 1.0 Uiso 0.0290(14) 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800
51.3531 1.33290 International_Tables_Vol_C
W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982
57.0560 9.88750 International_Tables_Vol_C
O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540500 1.000 K\a~1~ 1
1.544300 0.500 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sc1 O2 90.9(4) -2_666 . -2_666 N
O1 Sc1 O3 93.0(4) -2_666 . -2_666 N
O1 Sc1 O4 175.1(4) -2_666 . 1_555 N
O1 Sc1 O5 84.3(4) -2_666 . 4_565 N
O1 Sc1 O6 92.8(4) -2_666 . 1_555 N
O2 Sc1 O3 89.6(4) -2_666 . -2_666 N
O2 Sc1 O4 91.1(4) -2_666 . 1_555 N
O2 Sc1 O5 90.6(4) -2_666 . 4_565 N
O2 Sc1 O6 175.2(5) -2_666 . 1_555 N
O3 Sc1 O4 91.5(4) -2_666 . 1_555 N
O3 Sc1 O5 177.3(4) -2_666 . 4_565 N
O3 Sc1 O6 93.3(4) -2_666 . 1_555 N
O4 Sc1 O5 91.3(4) 1_555 . 4_565 N
O4 Sc1 O6 85.0(4) 1_555 . 1_555 N
O5 Sc1 O6 86.8(4) 4_565 . 1_555 N
O2 W1 O2 109.1(7) 1_555 . 4_555 N
O2 W1 O4 114.1(5) 1_555 . 2_545 N
O2 W1 O4 104.4(4) 1_555 . 3_555 N
O2 W1 O4 104.4(4) 4_555 . 2_545 N
O2 W1 O4 114.1(5) 4_555 . 3_555 N
O4 W1 O4 111.0(6) 2_545 . 3_555 N
O1 W2 O3 111.5(4) 3_555 . 1_555 N
O1 W2 O5 105.6(4) 3_555 . 1_555 N
O1 W2 O6 111.1(4) 3_555 . 1_555 N
O3 W2 O5 108.3(5) 1_555 . 1_555 N
O3 W2 O6 113.6(5) 1_555 . 1_555 N
O5 W2 O6 106.3(4) 1_555 . 1_555 N
Sc1 O1 W2 152.8(6) -2_466 . 3_554 N
Sc1 O2 W1 165.3(6) -2_555 . 1_555 N
Sc1 O3 W2 152.3(6) -2_466 . 1_555 N
Sc1 O4 W1 145.7(5) 1_555 . 2_554 N
Sc1 O5 W2 173.5(6) 4_565 . 1_555 N
Sc1 O6 W2 151.6(6) 1_555 . 1_555 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sc1 O1 2.074(10) . -2_555 N
Sc1 O2 2.102(11) . -2_555 N
Sc1 O3 2.077(10) . -2_555 N
Sc1 O4 2.108(10) . 1_555 N
Sc1 O5 2.060(10) . 4_565 N
Sc1 O6 2.023(10) . 1_555 N
W1 O2 1.731(10) . 1_555 N
W1 O2 1.731(10) . 4_555 N
W1 O4 1.798(9) . 2_545 N
W1 O4 1.798(9) . 3_555 N
W2 O1 1.758(10) . 3_555 N
W2 O3 1.763(10) . 1_555 N
W2 O5 1.801(10) . 1_555 N
W2 O6 1.781(10) . 1_555 N
O1 Sc1 2.074(10) . -2_455 N
O1 W2 1.758(10) . 3_554 N
O2 Sc1 2.102(11) . -2_455 N
O2 W1 1.731(10) . 1_555 N
O3 Sc1 2.077(10) . -2_455 N
O3 W2 1.763(10) . 1_555 N
O4 Sc1 2.108(10) . 1_555 N
O4 W1 1.798(9) . 2_554 N
O5 Sc1 2.060(10) . 4_565 N
O5 W2 1.801(10) . 1_555 N
O6 Sc1 2.023(10) . 1_555 N
O6 W2 1.781(10) . 1_555 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
322.0 0.0 623.85565 .
296.0 0.0 620.64709 .
290.0 0.0 617.46326 .
319.0 0.0 614.30402 .
300.0 0.0 611.16876 .
311.0 0.0 608.05829 .
315.0 0.0 604.97162 .
309.0 0.0 601.90887 .
311.0 0.0 598.87042 .
300.0 0.0 595.85516 .
319.0 0.0 592.86401 .
300.0 0.0 589.89606 .
318.0 0.0 586.95154 .
327.0 0.0 584.03046 .
313.0 0.0 581.13239 .
308.0 0.0 578.25732 .
328.0 0.0 575.40515 .
338.0 0.0 572.57556 .
309.0 0.0 569.76910 .
318.0 0.0 566.98505 .
299.0 0.0 564.22339 .
297.0 0.0 561.48395 .
327.0 0.0 558.76660 .
322.0 0.0 556.07159 .
317.0 0.0 553.39856 .
332.0 0.0 550.74725 .
327.0 0.0 548.11774 .
317.0 0.0 545.50970 .
326.0 0.0 542.92322 .
315.0 0.0 540.35846 .
327.0 0.0 537.81445 .
336.0 0.0 535.29181 .
314.0 0.0 532.79022 .
303.0 0.0 530.30975 .
306.0 0.0 527.85010 .
322.0 0.0 525.41101 .
323.0 0.0 522.99255 .
301.0 0.0 520.59442 .
307.0 0.0 518.21680 .
284.0 0.0 515.85974 .
301.0 0.0 513.52258 .
312.0 0.0 511.20551 .
290.0 0.0 508.90814 .
309.0 0.0 506.63098 .
326.0 0.0 504.37366 .
295.0 0.0 502.13565 .
327.0 0.0 499.91724 .
327.0 0.0 497.71811 .
310.0 0.0 495.53854 .
328.0 0.0 493.37808 .
300.0 0.0 491.23682 .
276.0 0.0 489.11438 .
329.0 0.0 487.01074 .
330.0 0.0 484.92603 .
311.0 0.0 482.86011 .
320.0 0.0 480.81268 .
296.0 0.0 478.78369 .
327.0 0.0 476.77298 .
320.0 0.0 474.78076 .
318.0 0.0 472.80667 .
327.0 0.0 470.85059 .
312.0 0.0 468.91241 .
298.0 0.0 466.99207 .
317.0 0.0 465.08954 .
297.0 0.0 463.20486 .
303.0 0.0 461.33780 .
317.0 0.0 459.48788 .
299.0 0.0 457.65540 .
291.0 0.0 455.84030 .
313.0 0.0 454.04245 .
333.0 0.0 452.26169 .
317.0 0.0 450.49777 .
349.0 0.0 448.75073 .
332.0 0.0 447.02045 .
349.0 0.0 445.30710 .
351.0 0.0 443.61026 .
326.0 0.0 441.92972 .
362.0 0.0 440.26581 .
367.0 0.0 438.61807 .
351.0 0.0 436.98669 .
347.0 0.0 435.37149 .
355.0 0.0 433.77216 .
321.0 0.0 432.18872 .
314.0 0.0 430.62122 .
320.0 0.0 429.06961 .
320.0 0.0 427.53357 .
331.0 0.0 426.01315 .
343.0 0.0 424.50812 .
336.0 0.0 423.01852 .
309.0 0.0 421.54440 .
311.0 0.0 420.08527 .
325.0 0.0 418.64136 .
338.0 0.0 417.21237 .
338.0 0.0 415.79843 .
337.0 0.0 414.39944 .
318.0 0.0 413.01523 .
309.0 0.0 411.64551 .
316.0 0.0 410.29050 .
301.0 0.0 408.94995 .
312.0 0.0 407.62393 .
335.0 0.0 406.31226 .
313.0 0.0 405.01474 .
321.0 0.0 403.73141 .
333.0 0.0 402.46228 .
329.0 0.0 401.20700 .
341.0 0.0 399.96582 .
359.0 0.0 398.73825 .
356.0 0.0 397.52454 .
332.0 0.0 396.32449 .
355.0 0.0 395.13794 .
336.0 0.0 393.96503 .
356.0 0.0 392.80542 .
321.0 0.0 391.65915 .
333.0 0.0 390.52625 .
362.0 0.0 389.40640 .
353.0 0.0 388.29971 .
353.0 0.0 387.20602 .
336.0 0.002976 386.12515 386.14163
343.0 0.002915 385.05737 385.07373
330.0 0.003030 384.00217 384.01855
349.0 0.002865 382.95972 382.97595
346.0 0.002890 381.92987 381.94604
327.0 0.003058 380.91245 380.92862
319.0 0.003135 379.90765 379.92368
340.0 0.002941 378.91522 378.93112
329.0 0.003040 377.93503 377.95090
374.0 0.002674 376.96707 376.98279
346.0 0.002890 376.01117 376.02682
330.0 0.003030 375.06744 375.08304
328.0 0.003049 374.13568 374.15118
337.0 0.002967 373.21579 373.23132
321.0 0.003115 372.30780 372.32321
332.0 0.003012 371.41159 371.42688
347.0 0.002882 370.52707 370.54224
350.0 0.002857 369.65408 369.66919
354.0 0.002825 368.79279 368.80777
352.0 0.002841 367.94284 367.95776
355.0 0.002817 367.10422 367.11899
349.0 0.002865 366.27704 366.29184
348.0 0.002874 365.46109 365.47577
336.0 0.002976 364.65634 364.67090
341.0 0.002933 363.86258 363.87711
348.0 0.002874 363.07986 363.09430
341.0 0.002933 362.30814 362.32251
352.0 0.002841 361.54736 361.56165
351.0 0.002849 360.79736 360.81155
325.0 0.003077 360.05807 360.07220
322.0 0.003106 359.32947 359.34338
333.0 0.003003 358.61148 358.62534
357.0 0.002801 357.90408 357.91782
377.0 0.002653 357.20706 357.22073
381.0 0.002625 356.52048 356.53409
358.0 0.002793 355.84406 355.85757
341.0 0.002933 355.17810 355.19150
359.0 0.002786 354.52225 354.53558
370.0 0.002703 353.87653 353.88983
344.0 0.002907 353.24084 353.25400
365.0 0.002740 352.61505 352.62817
358.0 0.002793 351.99930 352.01236
352.0 0.002841 351.39337 351.40631
392.0 0.002551 350.79718 355.41525
385.0 0.002597 350.21072 355.25757
362.0 0.002762 349.63394 357.48590
375.0 0.002667 349.06671 357.73267
375.0 0.002667 348.50903 358.15714
402.0 0.002488 347.96078 358.82828
409.0 0.002445 347.42191 359.89536
385.0 0.002597 346.89230 361.91003
372.0 0.002688 346.37204 366.72992
435.0 0.002299 345.86093 377.23709
422.0 0.002370 345.35889 394.45187
475.0 0.002105 344.86600 417.55887
493.0 0.002028 344.38208 445.39499
453.0 0.002208 343.90714 476.72742
477.0 0.002096 343.44107 511.10104
513.0 0.001949 342.98370 548.67438
513.0 0.001949 342.53522 589.83038
568.0 0.001761 342.09531 635.06207
653.0 0.001531 341.66409 684.99817
685.0 0.001460 341.24146 740.47845
686.0 0.001458 340.82733 802.61664
829.0 0.001206 340.42154 872.83496
827.0 0.001209 340.02417 952.92737
958.0 0.001044 339.63516 1045.41333
1090.0 0.000917 339.25446 1153.89758
1277.0 0.000783 338.88190 1283.48560
1515.0 0.000660 338.51749 1442.23828
1817.0 0.000550 338.16110 1643.18298
2204.0 0.000454 337.81281 1910.61841
2737.0 0.000365 337.47247 2299.46753
3418.0 0.0002926 337.14005 2930.00024
4121.0 0.0002427 336.81543 3767.16504
4155.0 0.0002407 336.49863 3919.46704
3238.0 0.0003088 336.18954 2945.45996
2090.0 0.000478 335.88818 1975.68286
1198.0 0.000835 335.59436 1074.08850
676.0 0.001479 335.30811 609.57996
483.0 0.002070 335.02945 472.36877
423.0 0.002364 334.75815 427.15286
416.0 0.002404 334.49426 402.87708
411.0 0.002433 334.23773 387.21152
393.0 0.002545 333.98853 376.37976
396.0 0.002525 333.74643 368.52332
390.0 0.002564 333.51154 362.60919
375.0 0.002667 333.28384 358.02185
360.0 0.002778 333.06314 354.37549
346.0 0.002890 332.84943 351.41653
361.0 0.002770 332.64270 348.97391
389.0 0.002571 332.44290 346.92688
383.0 0.002611 332.24988 345.18918
371.0 0.002695 332.06366 343.69711
350.0 0.002857 331.88419 342.40317
350.0 0.002857 331.71140 341.27127
364.0 0.002747 331.54526 340.27353
390.0 0.002564 331.38571 334.35498
383.0 0.002611 331.23267 333.95343
360.0 0.002778 331.08615 331.09390
332.0 0.003012 330.94595 330.95361
352.0 0.002841 330.81216 330.81979
377.0 0.002653 330.68484 330.69223
394.0 0.002538 330.56357 330.57101
368.0 0.002717 330.44864 330.45593
377.0 0.002653 330.33981 330.34702
347.0 0.002882 330.23721 330.24426
354.0 0.002825 330.14059 330.14764
371.0 0.002695 330.04999 330.05695
349.0 0.002865 329.96539 329.97232
378.0 0.002646 329.88675 329.89352
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2110.0 0.000474 382.48898 2144.34546
2923.0 0.0003421 382.24988 2884.81738
3957.0 0.0002527 382.01108 3860.94775
4390.0 0.0002278 381.77234 4430.97363
3401.0 0.0002940 381.53372 3607.88574
2365.0 0.000423 381.29523 2530.87964
2116.0 0.000473 381.05685 2262.94556
2314.0 0.000432 380.81860 2394.47266
2024.0 0.000494 380.58057 2084.42017
1233.0 0.000811 380.34268 1319.02332
789.0 0.001267 380.10489 826.53882
585.0 0.001709 379.86719 636.32141
555.0 0.001802 379.62976 567.63184
538.0 0.001859 379.39240 536.26660
526.0 0.001901 379.15527 523.00763
524.0 0.001908 378.91827 526.37463
546.0 0.001832 378.68140 548.01465
614.0 0.001629 378.44476 588.03986
643.0 0.001555 378.20822 646.79242
701.0 0.001427 377.97198 729.01227
820.0 0.001220 377.73581 840.20044
947.0 0.001056 377.49969 1000.59454
1263.0 0.000792 377.26392 1240.63684
1510.0 0.000662 377.02832 1574.30835
1886.0 0.000530 376.79288 1860.99548
1811.0 0.000552 376.55765 1737.80664
1405.0 0.000712 376.32245 1386.00366
1310.0 0.000763 376.08771 1315.40991
1422.0 0.000703 375.85300 1499.12903
1638.0 0.000611 375.61847 1657.85535
1645.0 0.000608 375.38422 1673.23914
1791.0 0.000558 375.15005 1813.12720
2320.0 0.000431 374.91623 2223.60791
3108.0 0.0003218 374.68250 2946.76807
4044.0 0.0002473 374.44907 3876.53955
4352.0 0.0002298 374.21579 4315.87061
3441.0 0.0002906 373.98270 3415.58008
2367.0 0.000422 373.74994 2414.64771
2243.0 0.000446 373.51727 2200.17993
2340.0 0.000427 373.28491 2336.27026
2065.0 0.000484 373.05276 2033.53857
1355.0 0.000738 372.82071 1294.31287
795.0 0.001258 372.58905 817.21576
590.0 0.001695 372.35760 634.07147
529.0 0.001890 372.12634 573.16095
538.0 0.001859 371.89536 553.50201
542.0 0.001845 371.66449 555.92889
545.0 0.001835 371.43396 565.98291
530.0 0.001887 371.20364 549.49310
499.0 0.002004 370.97366 503.01056
458.0 0.002183 370.74384 474.28912
442.0 0.002262 370.51419 468.98224
426.0 0.002347 370.28494 465.69150
397.0 0.002519 370.05582 443.80521
378.0 0.002646 369.82706 418.65170
346.0 0.002890 369.59851 404.66647
359.0 0.002786 369.37018 396.22766
349.0 0.002865 369.14218 392.34204
354.0 0.002825 368.91443 389.44675
378.0 0.002646 368.68695 387.09961
348.0 0.002874 368.45975 384.21439
338.0 0.002959 368.23276 382.56689
344.0 0.002907 368.00604 381.12567
380.0 0.002632 367.77966 379.84674
378.0 0.002646 367.55350 378.69983
340.0 0.002941 367.32764 377.66119
333.0 0.003003 367.10205 371.47159
345.0 0.002899 366.87680 370.91354
372.0 0.002688 366.65179 370.39401
365.0 0.002740 366.42709 369.90723
362.0 0.002762 366.20273 369.44839
359.0 0.002786 365.97855 366.48703
358.0 0.002793 365.75467 366.22122
353.0 0.002833 365.53110 365.96078
314.0 0.003185 365.30795 365.70514
344.0 0.002907 365.08499 365.45325
317.0 0.003155 364.86230 365.20490
357.0 0.002801 364.64001 364.95959
325.0 0.003077 364.41797 364.71680
335.0 0.002985 364.19623 364.31454
348.0 0.002874 363.97488 364.08582
348.0 0.002874 363.75369 363.85806
339.0 0.002950 363.53293 363.63123
356.0 0.002809 363.31247 363.32214
338.0 0.002959 363.09232 363.10205
310.0 0.003226 362.87256 362.88226
328.0 0.003049 362.65298 362.66269
346.0 0.002890 362.43378 362.44357
336.0 0.002976 362.21503 362.22470
350.0 0.002857 361.99643 362.00620
353.0 0.002833 361.77826 361.78806
353.0 0.002833 361.56036 361.57016
305.0 0.003279 361.34280 361.35266
297.0 0.003367 361.12564 361.13544
306.0 0.003268 360.90881 360.91861
332.0 0.003012 360.69226 360.70209
327.0 0.003058 360.47601 360.48590
342.0 0.002924 360.26025 360.27011
357.0 0.002801 360.04468 360.05463
319.0 0.003135 359.82962 359.83951
315.0 0.003175 359.61481 359.62473
330.0 0.003030 359.40024 359.41028
323.0 0.003096 359.18619 359.19617
316.0 0.003165 358.97244 358.98242
306.0 0.003268 358.75909 358.76910
301.0 0.003322 358.54602 358.55606
312.0 0.003205 358.33334 358.34344
335.0 0.002985 358.12106 358.13107
339.0 0.002950 357.90912 357.91919
325.0 0.003077 357.69751 357.70764
317.0 0.003155 357.48630 357.49640
330.0 0.003030 357.27536 357.28552
361.0 0.002770 357.06494 357.07510
339.0 0.002950 356.85480 356.86493
333.0 0.003003 356.64511 356.65524
364.0 0.002747 356.43576 356.44583
346.0 0.002890 356.22672 356.23685
353.0 0.002833 356.01816 356.02826
363.0 0.002755 355.80984 355.82001
327.0 0.003058 355.60208 355.61221
346.0 0.002890 355.39459 355.40475
355.0 0.002817 355.18738 355.19763
333.0 0.003003 354.98074 354.99103
351.0 0.002849 354.77438 354.78467
351.0 0.002849 354.56842 354.57880
378.0 0.002646 354.36292 354.37320
359.0 0.002786 354.15775 354.16806
351.0 0.002849 353.95303 353.96329
348.0 0.002874 353.74866 353.75894
350.0 0.002857 353.54471 353.55508
380.0 0.002632 353.34113 353.35150
381.0 0.002625 353.13791 353.14828
313.0 0.003195 352.93521 352.94559
344.0 0.002907 352.73282 352.74319
364.0 0.002747 352.53088 355.73898
348.0 0.002874 352.32932 355.76050
335.0 0.002985 352.12814 355.80679
346.0 0.002890 351.92737 355.88147
369.0 0.002710 351.72705 355.98898
342.0 0.002924 351.52713 357.74872
366.0 0.002732 351.32764 358.05237
326.0 0.003067 351.12842 358.42111
336.0 0.002976 350.92978 358.86652
345.0 0.002899 350.73151 359.40338
337.0 0.002967 350.53363 360.04968
362.0 0.002762 350.33630 360.82901
375.0 0.002667 350.13919 373.40872
359.0 0.002786 349.94260 375.37018
367.0 0.002725 349.74646 377.67636
350.0 0.002857 349.55081 380.41071
353.0 0.002833 349.35541 389.17767
350.0 0.002857 349.16049 393.53940
383.0 0.002611 348.96603 398.88284
384.0 0.002604 348.77200 405.58173
416.0 0.002404 348.57843 414.27042
442.0 0.002262 348.38519 426.40366
458.0 0.002183 348.19244 450.49161
500.0 0.002000 348.00021 485.51410
558.0 0.001792 347.80832 544.10028
623.0 0.001605 347.61688 630.04504
698.0 0.001433 347.42593 749.09973
879.0 0.001138 347.23529 910.54810
1111.0 0.000900 347.04520 1131.26270
1452.0 0.000689 346.85550 1459.26392
1956.0 0.000511 346.66632 1925.19238
2390.0 0.000418 346.47748 2385.38379
2389.0 0.000419 346.28915 2356.04272
1889.0 0.000529 346.10129 1807.57886
1648.0 0.000607 345.91379 1511.96057
1756.0 0.000569 345.72681 1634.57141
2005.0 0.000499 345.54028 1934.07068
1937.0 0.000516 345.35413 2074.61743
1962.0 0.000510 345.16855 2132.18555
2201.0 0.000454 344.98331 2482.28174
2918.0 0.0003427 344.79858 3203.70947
4068.0 0.0002458 344.61432 4397.91553
5558.0 0.0001799 344.43045 6077.62256
6861.0 0.0001458 344.24716 7457.97510
6199.0 0.0001613 344.06424 6734.29395
4365.0 0.0002291 343.88177 4643.48633
3303.0 0.0003028 343.69980 3689.10181
3508.0 0.0002851 343.51819 3931.35791
3898.0 0.0002565 343.33713 4312.06348
3315.0 0.0003017 343.15656 3672.66553
2468.0 0.000405 342.97647 2648.42114
2249.0 0.000445 342.79681 2287.15820
2572.0 0.000389 342.61752 2568.36670
3235.0 0.0003091 342.43881 3200.77051
3526.0 0.0002836 342.26053 3619.65869
2914.0 0.0003432 342.08276 3097.17114
2112.0 0.000473 341.90543 2313.65259
1979.0 0.000505 341.72855 2113.14941
2201.0 0.000454 341.55222 2380.52124
2500.0 0.000400 341.37628 2615.99316
2224.0 0.000450 341.20081 2266.12549
1419.0 0.000705 341.02585 1560.88440
945.0 0.001058 340.85138 1071.99500
830.0 0.001205 340.67743 903.41510
765.0 0.001307 340.50378 895.48761
820.0 0.001220 340.33078 863.20544
664.0 0.001506 340.15823 706.86804
495.0 0.002020 339.98611 556.54852
466.0 0.002146 339.81445 477.89548
418.0 0.002392 339.64334 443.96942
392.0 0.002551 339.47278 425.75705
399.0 0.002506 339.30255 413.48611
391.0 0.002558 339.13281 404.44125
403.0 0.002481 338.96368 397.56738
403.0 0.002481 338.79498 392.31729
364.0 0.002747 338.62671 381.97852
365.0 0.002740 338.45905 380.49350
362.0 0.002762 338.29178 381.28543
357.0 0.002801 338.12506 385.51431
379.0 0.002639 337.95868 388.50375
391.0 0.002558 337.79303 403.62689
409.0 0.002445 337.62772 422.34155
437.0 0.002288 337.46286 449.30557
475.0 0.002105 337.29858 490.37122
519.0 0.001927 337.13477 548.93152
572.0 0.001748 336.97150 601.19562
577.0 0.001733 336.80862 593.06464
537.0 0.001862 336.64624 517.67249
486.0 0.002058 336.48447 471.03995
468.0 0.002137 336.32309 470.86975
470.0 0.002128 336.16229 483.80499
447.0 0.002237 336.00198 468.57736
423.0 0.002364 335.84216 423.87448
444.0 0.002252 335.68283 393.35110
422.0 0.002370 335.52399 383.10660
398.0 0.002513 335.36563 383.26794
436.0 0.002294 335.20782 387.98590
455.0 0.002198 335.05045 398.85281
474.0 0.002110 334.89365 420.28336
550.0 0.001818 334.73727 462.19626
563.0 0.001776 334.58148 532.28088
658.0 0.001520 334.42618 636.21942
746.0 0.001340 334.27124 784.58636
941.0 0.001063 334.11700 984.98712
1362.0 0.000734 333.96317 1274.78748
1885.0 0.000531 333.80984 1709.16650
2381.0 0.000420 333.65717 2223.68604
2594.0 0.000386 333.50479 2425.91504
1980.0 0.000505 333.35300 1928.67419
1352.0 0.000740 333.20166 1389.24280
1308.0 0.000765 333.05103 1249.32556
1442.0 0.000693 332.90073 1356.56042
1484.0 0.000674 332.75098 1374.44519
1123.0 0.000890 332.60181 1056.34924
684.0 0.001462 332.45306 705.03906
505.0 0.001980 332.30484 525.22845
465.0 0.002151 332.15714 458.86951
421.0 0.002375 332.00992 429.99271
406.0 0.002463 331.86322 414.95688
423.0 0.002364 331.71707 406.35361
427.0 0.002342 331.57141 401.90588
401.0 0.002494 331.42621 401.87079
423.0 0.002364 331.28156 403.41544
467.0 0.002141 331.13751 410.93079
483.0 0.002070 330.99393 421.09720
473.0 0.002114 330.85083 440.80212
505.0 0.001980 330.70828 477.75754
548.0 0.001825 330.56619 537.10156
655.0 0.001527 330.42465 627.81036
770.0 0.001299 330.28366 753.30737
950.0 0.001053 330.14319 940.56042
1257.0 0.000796 330.00314 1219.21387
1600.0 0.000625 329.86365 1623.43555
1951.0 0.000513 329.72470 2058.38037
2107.0 0.000475 329.58624 2194.80103
2010.0 0.000498 329.44836 1997.60242
2061.0 0.000485 329.31097 2029.29126
2289.0 0.000437 329.17404 2368.58960
2461.0 0.000406 329.03775 2565.75220
2182.0 0.000458 328.90186 2168.85889
1624.0 0.000616 328.76654 1595.83191
1331.0 0.000751 328.63174 1360.83325
1353.0 0.000739 328.49744 1434.19348
1465.0 0.000683 328.36374 1530.46655
1465.0 0.000683 328.23044 1469.41260
1583.0 0.000632 328.09772 1477.83594
1864.0 0.000536 327.96552 1706.86780
2025.0 0.000494 327.83383 1954.99866
1749.0 0.000572 327.70264 1817.11938
1384.0 0.000723 327.57205 1467.83862
1368.0 0.000731 327.44193 1370.41248
1608.0 0.000622 327.31229 1564.53467
1959.0 0.000510 327.18314 1894.41797
2190.0 0.000457 327.05463 2130.49780
2206.0 0.000453 326.92654 2130.49902
1804.0 0.000554 326.79910 1774.83838
1239.0 0.000807 326.67212 1267.74915
1016.0 0.000984 326.54559 1027.32300
1059.0 0.000944 326.41968 1035.03467
1111.0 0.000900 326.29425 1103.73181
1031.0 0.000970 326.16937 995.83630
696.0 0.001437 326.04501 725.95355
510.0 0.001961 325.92111 536.67719
392.0 0.002551 325.79782 452.14468
372.0 0.002688 325.67496 417.49805
404.0 0.002475 325.55267 397.36459
359.0 0.002786 325.43088 386.00253
376.0 0.002660 325.30969 378.21356
388.0 0.002577 325.18900 372.78036
366.0 0.002732 325.06879 366.60678
349.0 0.002865 324.94907 362.50229
346.0 0.002890 324.82993 360.06140
374.0 0.002674 324.71127 358.58075
336.0 0.002976 324.59317 358.11139
375.0 0.002667 324.47565 357.34900
346.0 0.002890 324.35855 358.45566
405.0 0.002469 324.24200 360.29926
395.0 0.002532 324.12598 363.46609
429.0 0.002331 324.01053 368.66245
413.0 0.002421 323.89557 375.27927
457.0 0.002188 323.78107 391.67792
501.0 0.001996 323.66721 423.18454
498.0 0.002008 323.55380 476.92484
565.0 0.001770 323.44089 557.90503
671.0 0.001490 323.32852 671.46222
867.0 0.001153 323.21671 833.35498
1110.0 0.000901 323.10541 1068.06860
1428.0 0.000700 322.99460 1406.57361
1761.0 0.000568 322.88437 1734.58655
1711.0 0.000584 322.77463 1710.17505
1308.0 0.000765 322.66541 1283.27356
972.0 0.001029 322.55664 983.50885
957.0 0.001045 322.44852 950.85480
1029.0 0.000972 322.34088 1043.17737
1026.0 0.000975 322.23370 1034.16345
833.0 0.001200 322.12717 796.28729
570.0 0.001754 322.02097 561.45673
439.0 0.002278 321.91547 442.85513
372.0 0.002688 321.81042 395.97211
355.0 0.002817 321.70581 374.98523
390.0 0.002564 321.60184 362.71429
416.0 0.002404 321.49838 356.24451
410.0 0.002439 321.39536 356.32745
393.0 0.002545 321.29297 352.36792
369.0 0.002710 321.19098 349.46695
351.0 0.002849 321.08957 347.32886
361.0 0.002770 320.98877 345.76175
354.0 0.002825 320.88834 347.51318
344.0 0.002907 320.78851 346.90387
361.0 0.002770 320.68918 346.61420
350.0 0.002857 320.59033 346.60950
344.0 0.002907 320.49207 346.86987
324.0 0.003086 320.39426 347.38766
322.0 0.003106 320.29700 348.16537
330.0 0.003030 320.20026 349.21634
364.0 0.002747 320.10406 350.56427
326.0 0.003067 320.00833 352.24689
360.0 0.002778 319.91309 354.31805
351.0 0.002849 319.81845 356.85196
360.0 0.002778 319.72430 359.95743
368.0 0.002717 319.63058 361.77844
377.0 0.002653 319.53760 366.71448
387.0 0.002584 319.44485 373.43881
399.0 0.002506 319.35278 381.77673
393.0 0.002545 319.26120 393.98639
452.0 0.002212 319.17010 413.01862
479.0 0.002088 319.07953 447.83994
536.0 0.001866 318.98944 501.29779
561.0 0.001783 318.89993 580.18274
708.0 0.001412 318.81091 688.00385
870.0 0.001149 318.72241 843.70386
1083.0 0.000923 318.63443 1069.30493
1349.0 0.000741 318.54694 1341.85730
1571.0 0.000637 318.45990 1486.52734
1441.0 0.000694 318.37344 1301.72900
1139.0 0.000878 318.28748 1074.78857
1187.0 0.000842 318.20206 1078.35303
1380.0 0.000725 318.11713 1311.66260
1686.0 0.000593 318.03271 1659.08228
1913.0 0.000523 317.94879 2015.31702
2277.0 0.000439 317.86536 2428.91064
3066.0 0.0003262 317.78244 3205.58496
4510.0 0.0002217 317.70004 4422.36768
5884.0 0.0001700 317.61813 5796.39648
6033.0 0.0001658 317.53674 6084.42871
4496.0 0.0002224 317.45584 4557.67480
2887.0 0.0003464 317.37546 3128.85229
2585.0 0.000387 317.29559 2766.89771
2911.0 0.0003435 317.21631 3091.52002
3127.0 0.0003198 317.13742 3318.97534
2596.0 0.000385 317.05902 2655.67334
1572.0 0.000636 316.98117 1606.96313
919.0 0.001088 316.90381 968.57098
652.0 0.001534 316.82693 701.40607
574.0 0.001742 316.75061 595.06409
518.0 0.001931 316.67480 545.58551
476.0 0.002101 316.59946 524.41559
469.0 0.002132 316.52460 525.35675
495.0 0.002020 316.45023 549.82672
575.0 0.001739 316.37640 597.72351
693.0 0.001443 316.30307 680.83667
755.0 0.001325 316.23013 798.07233
869.0 0.001151 316.15778 931.64166
1025.0 0.000976 316.08594 1019.48718
1063.0 0.000941 316.01462 1048.87891
986.0 0.001014 315.94366 998.69269
882.0 0.001134 315.87332 913.06635
859.0 0.001164 315.80341 931.17059
1031.0 0.000970 315.73407 1040.37061
1246.0 0.000803 315.66513 1199.47888
1438.0 0.000695 315.59668 1363.26648
1485.0 0.000673 315.52887 1372.06311
1178.0 0.000849 315.46136 1116.56616
825.0 0.001212 315.39450 831.22760
710.0 0.001408 315.32803 718.20508
721.0 0.001387 315.26208 727.40717
780.0 0.001282 315.19669 776.33337
764.0 0.001309 315.13168 724.45789
591.0 0.001692 315.06711 567.56250
464.0 0.002155 315.00314 447.43781
385.0 0.002597 314.93970 385.95184
333.0 0.003003 314.87662 362.68539
351.0 0.002849 314.81409 351.30237
321.0 0.003115 314.75211 343.95554
333.0 0.003003 314.69046 338.79028
335.0 0.002985 314.62936 334.96982
324.0 0.003086 314.56882 332.04089
319.0 0.003135 314.50864 329.86270
329.0 0.003040 314.44897 328.01028
355.0 0.002817 314.38980 326.49191
304.0 0.003289 314.33118 325.22983
314.0 0.003185 314.27298 324.16754
332.0 0.003012 314.21518 323.26450
345.0 0.002899 314.15799 322.49088
354.0 0.002825 314.10120 321.39395
315.0 0.003175 314.04489 320.84164
318.0 0.003145 313.98911 319.60492
313.0 0.003195 313.93365 319.23468
302.0 0.003311 313.87891 318.91678
304.0 0.003289 313.82446 318.42563
284.0 0.00352 313.77057 318.21069
299.0 0.003344 313.71710 317.64670
321.0 0.003115 313.66406 316.61945
333.0 0.003003 313.61160 316.65417
337.0 0.002967 313.55951 316.72116
298.0 0.003356 313.50797 316.82446
313.0 0.003195 313.45688 316.97006
312.0 0.003205 313.40619 317.16638
300.0 0.003333 313.35608 316.99826
293.0 0.003413 313.30634 317.39008
302.0 0.003311 313.25711 317.88190
320.0 0.003125 313.20834 318.50983
298.0 0.003356 313.15997 319.32971
315.0 0.003175 313.11212 320.43460
336.0 0.002976 313.06476 322.02054
340.0 0.002941 313.01782 325.71289
347.0 0.002882 312.97137 330.43646
358.0 0.002793 312.92532 339.03214
371.0 0.002695 312.87979 352.65674
387.0 0.002584 312.83469 373.57489
415.0 0.002410 312.79001 402.87207
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898.0 0.001114 310.49832 841.57520
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884.0 0.001131 310.46484 813.73212
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914.0 0.001094 310.47516 877.47040
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721.0 0.001387 310.48679 740.33118
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1464.0 0.000683 310.53915 1469.49243
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410.0 . . .
