#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:30:51 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1274 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000055.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000055
loop_
_publ_author_name
'Zhou, Yongkai'
'Adams, Stefan'
'Rao, R. Prasada'
'Edwards, Doreen D.'
'Neiman, Arkady'
'Pestereva, N.'
_publ_section_title
;
 Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3
;
_journal_issue                   20
_journal_name_full               'Chemistry of Materials'
_journal_page_first              6335
_journal_page_last               6345
_journal_paper_doi               10.1021/cm800466y
_journal_volume                  20
_journal_year                    2008
_chemical_formula_moiety         ' Sc2(WO4)3 '
_chemical_formula_sum            'O12 Sc2 W3'
_chemical_formula_weight         833.45
_chemical_melting_point          ' 1913K '
_chemical_name_common            ' Scandium Tungstate '
_chemical_name_systematic        ' Scandium Tungstate '
_space_group_IT_number           60
_space_group_name_Hall           '-P 2a 2n'
_space_group_name_H-M_alt        'P n c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n c a'
_audit_creation_date             2008-01-25T12:03
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2008-01-25T12:03  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.63965(5)
_cell_length_b                   13.35026(7)
_cell_length_c                   9.55959(5)
_cell_measurement_temperature    750
_cell_volume                     1230.241(11)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.68
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id
2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.017
_pd_meas_2theta_range_max        119.9874
_pd_meas_2theta_range_min        10.0144
_pd_meas_number_of_points        6470
_pd_proc_2theta_range_inc        0.017
_pd_proc_2theta_range_max        119.9874
_pd_proc_2theta_range_min        10.0144
_pd_proc_info_datetime           2008-01-25T12:28:53
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    363.226     2:   -36.3754     3:    15.4874     4:    43.0560    
      5:   -4.30084     6:    9.93283     7:   -10.1615     8:    5.23537    
      9:    9.93394    10:   -24.2373    11:    23.5464    12:   -7.83530    
;
_pd_proc_ls_peak_cutoff          0.00250
_pd_proc_ls_pref_orient_corr
;   March-Dollase
 AXIS  1 Ratio=   0.95235  h= 0.000  k= 1.000  l= 0.000
 Prefered orientation correction range: Min=   0.92938, Max=   1.15774
;
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =    6.052 #2(GV)   =   -3.642 #3(GW)   =    1.823
 #4(GP)   =    0.000 #5(LX)   =    0.910 #6(LY)   =    5.255
 #7(S/L)  =   0.0319 #8(H/L)  =   0.0250
 #9(trns) =     0.00 #10(shft)=  -8.2368
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0025 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0488
_pd_proc_ls_prof_wR_expected     0.0359
_pd_proc_ls_prof_wR_factor       0.0646
_pd_proc_number_of_points        6470
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.85
_refine_ls_matrix_type           full
_refine_ls_number_parameters     51
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.06199
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        0.890
_reflns_d_resolution_low         6.675
_reflns_limit_h_max              10
_reflns_limit_h_min              0
_reflns_limit_k_max              15
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_total             1829
_cod_data_source_file            cm800466y_si_016.cif
_cod_data_source_block           T750K
_cod_original_cell_volume        1230.241(13)
_cod_database_code               4000055
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,+z+1/2
3 +x,-y+1/2,+z+1/2
4 -x+1/2,-y,+z
-1 -x,-y,-z
-2 +x+1/2,-y+1/2,-z+1/2
-3 -x,+y+1/2,-z+1/2
-4 +x+1/2,+y,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Sc Sc1 0.4698(4) 0.38118(24) 0.2478(4) 1.0 Uiso 0.0249(11) 8
W W1 0.25 0.0 0.47167(14) 1.0 Uiso 0.02599(29) 4
W W2 0.11342(11) 0.35649(7) 0.39182(11) 1.0 Uiso 0.02599(29) 8
O O1 0.0904(12) 0.1300(8) 0.0703(12) 1.0 Uiso 0.0530(17) 8
O O2 0.1481(12) 0.0733(8) 0.3697(13) 1.0 Uiso 0.0530(17) 8
O O3 0.0066(12) 0.2646(9) 0.3164(11) 1.0 Uiso 0.0530(17) 8
O O4 0.3356(12) 0.4061(8) 0.0763(12) 1.0 Uiso 0.0530(17) 8
O O5 0.0618(11) 0.4759(9) 0.3240(12) 1.0 Uiso 0.0530(17) 8
O O6 0.2928(13) 0.3462(8) 0.3459(12) 1.0 Uiso 0.0530(17) 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800
51.3531 1.33290 International_Tables_Vol_C
W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982
57.0560 9.88750 International_Tables_Vol_C
O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540500 1.000 K\a~1~ 1
1.544300 0.000 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sc1 O2 90.6(5) -2_666 . -2_666 N
O1 Sc1 O3 94.8(4) -2_666 . -2_666 N
O1 Sc1 O4 173.3(5) -2_666 . 1_555 N
O1 Sc1 O5 81.6(4) -2_666 . 4_565 N
O1 Sc1 O6 93.9(5) -2_666 . 1_555 N
O2 Sc1 O3 88.5(5) -2_666 . -2_666 N
O2 Sc1 O4 92.3(5) -2_666 . 1_555 N
O2 Sc1 O5 92.3(5) -2_666 . 4_565 N
O2 Sc1 O6 174.8(5) -2_666 . 1_555 N
O3 Sc1 O4 91.3(5) -2_666 . 1_555 N
O3 Sc1 O5 176.4(5) -2_666 . 4_565 N
O3 Sc1 O6 93.8(4) -2_666 . 1_555 N
O4 Sc1 O5 92.2(4) 1_555 . 4_565 N
O4 Sc1 O6 83.0(4) 1_555 . 1_555 N
O5 Sc1 O6 85.7(5) 4_565 . 1_555 N
O2 W1 O2 109.8(8) 1_555 . 4_555 N
O2 W1 O4 117.1(5) 1_555 . 2_545 N
O2 W1 O4 100.6(5) 1_555 . 3_555 N
O2 W1 O4 100.6(5) 4_555 . 2_545 N
O2 W1 O4 117.1(5) 4_555 . 3_555 N
O4 W1 O4 112.6(7) 2_545 . 3_555 N
O1 W2 O3 113.7(5) 3_555 . 1_555 N
O1 W2 O5 103.2(5) 3_555 . 1_555 N
O1 W2 O6 112.0(5) 3_555 . 1_555 N
O3 W2 O5 108.1(6) 1_555 . 1_555 N
O3 W2 O6 114.3(6) 1_555 . 1_555 N
O5 W2 O6 104.4(5) 1_555 . 1_555 N
Sc1 O1 W2 153.7(7) -2_466 . 3_554 N
Sc1 O2 W1 158.6(7) -2_555 . 1_555 N
Sc1 O3 W2 151.4(7) -2_466 . 1_555 N
Sc1 O4 W1 145.0(6) 1_555 . 2_554 N
Sc1 O5 W2 172.3(7) 4_565 . 1_555 N
Sc1 O6 W2 157.0(7) 1_555 . 1_555 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sc1 O1 2.097(12) . -2_555 N
Sc1 O2 2.141(12) . -2_555 N
Sc1 O3 2.071(12) . -2_555 N
Sc1 O4 2.114(11) . 1_555 N
Sc1 O5 2.064(11) . 4_565 N
Sc1 O6 2.002(12) . 1_555 N
W1 O2 1.695(12) . 1_555 N
W1 O2 1.695(12) . 4_555 N
W1 O4 1.803(10) . 2_545 N
W1 O4 1.803(10) . 3_555 N
W2 O1 1.730(11) . 3_555 N
W2 O3 1.756(11) . 1_555 N
W2 O5 1.792(11) . 1_555 N
W2 O6 1.790(12) . 1_555 N
O1 Sc1 2.097(12) . -2_455 N
O1 W2 1.730(11) . 3_554 N
O2 Sc1 2.141(12) . -2_455 N
O2 W1 1.695(12) . 1_555 N
O3 Sc1 2.071(12) . -2_455 N
O3 W2 1.756(11) . 1_555 N
O4 Sc1 2.114(11) . 1_555 N
O4 W1 1.803(10) . 2_554 N
O5 Sc1 2.064(11) . 4_565 N
O5 W2 1.792(11) . 1_555 N
O6 Sc1 2.002(12) . 1_555 N
O6 W2 1.790(12) . 1_555 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
353.0 0.0 726.08868 .
349.0 0.0 721.84222 .
353.0 0.0 717.62811 .
336.0 0.0 713.44543 .
345.0 0.0 709.29401 .
332.0 0.0 705.17462 .
316.0 0.0 701.08612 .
353.0 0.0 697.02844 .
348.0 0.0 693.00238 .
351.0 0.0 689.00616 .
340.0 0.0 685.04114 .
344.0 0.0 681.10645 .
359.0 0.0 677.20190 .
342.0 0.0 673.32776 .
335.0 0.0 669.48340 .
319.0 0.0 665.66888 .
336.0 0.0 661.88403 .
324.0 0.0 658.12836 .
328.0 0.0 654.40271 .
342.0 0.0 650.70612 .
333.0 0.0 647.03851 .
339.0 0.0 643.39984 .
352.0 0.0 639.78949 .
360.0 0.0 636.20837 .
369.0 0.0 632.65564 .
368.0 0.0 629.13116 .
338.0 0.0 625.63483 .
333.0 0.0 622.16638 .
343.0 0.0 618.72583 .
349.0 0.0 615.31348 .
351.0 0.0 611.92816 .
348.0 0.0 608.57056 .
331.0 0.0 605.24005 .
331.0 0.0 601.93701 .
339.0 0.0 598.66113 .
332.0 0.0 595.41187 .
329.0 0.0 592.18921 .
349.0 0.0 588.99310 .
343.0 0.0 585.82379 .
330.0 0.0 582.68085 .
347.0 0.0 579.56384 .
327.0 0.0 576.47290 .
346.0 0.0 573.40759 .
383.0 0.0 570.36847 .
359.0 0.0 567.35510 .
325.0 0.0 564.36694 .
319.0 0.0 561.40411 .
324.0 0.0 558.46631 .
362.0 0.0 555.55408 .
348.0 0.0 552.66663 .
357.0 0.0 549.80408 .
370.0 0.0 546.96594 .
366.0 0.0 544.15222 .
344.0 0.0 541.36322 .
367.0 0.0 538.59851 .
364.0 0.0 535.85791 .
342.0 0.0 533.14124 .
338.0 0.0 530.44836 .
357.0 0.0 527.77948 .
329.0 0.0 525.13440 .
332.0 0.0 522.51263 .
348.0 0.0 519.91394 .
335.0 0.0 517.33862 .
339.0 0.0 514.78650 .
345.0 0.0 512.25757 .
347.0 0.0 509.75146 .
356.0 0.0 507.26779 .
333.0 0.0 504.80679 .
333.0 0.0 502.36838 .
337.0 0.0 499.95242 .
338.0 0.0 497.55875 .
363.0 0.0 495.18695 .
331.0 0.0 492.83725 .
353.0 0.0 490.50931 .
357.0 0.0 488.20337 .
354.0 0.0 485.91898 .
357.0 0.0 483.65579 .
347.0 0.0 481.41431 .
368.0 0.0 479.19385 .
392.0 0.0 476.99475 .
356.0 0.0 474.81674 .
347.0 0.0 472.65942 .
348.0 0.0 470.52286 .
360.0 0.0 468.40692 .
375.0 0.0 466.31189 .
370.0 0.0 464.23703 .
349.0 0.0 462.18256 .
348.0 0.0 460.14825 .
361.0 0.0 458.13391 .
361.0 0.0 456.13977 .
354.0 0.0 454.16544 .
345.0 0.0 452.21072 .
347.0 0.0 450.27563 .
365.0 0.0 448.36008 .
378.0 0.0 446.46408 .
368.0 0.0 444.58740 .
367.0 0.0 442.72952 .
326.0 0.0 440.89096 .
331.0 0.0 439.07135 .
351.0 0.0 437.27057 .
346.0 0.0 435.48868 .
362.0 0.0 433.72510 .
340.0 0.0 431.98019 .
350.0 0.0 430.25375 .
352.0 0.0 428.54547 .
330.0 0.0 426.85553 .
363.0 0.0 425.18344 .
347.0 0.0 423.52954 .
337.0 0.0 421.89346 .
330.0 0.0 420.27509 .
324.0 0.0 418.67450 .
347.0 0.0 417.09128 .
336.0 0.0 415.52554 .
371.0 0.0 413.97736 .
307.0 0.0 412.44620 .
350.0 0.0 410.93216 .
357.0 0.0 409.43524 .
353.0 0.002833 407.95505 407.95245
333.0 0.003003 406.49203 406.48941
402.0 0.002488 405.04553 405.04300
373.0 0.002681 403.61563 403.61337
386.0 0.002591 402.20245 402.20004
386.0 0.002591 400.80536 400.80316
335.0 0.002985 399.42484 399.42273
335.0 0.002985 398.06046 398.05847
361.0 0.002770 396.71222 396.71030
348.0 0.002874 395.37997 395.37817
305.0 0.003279 394.06360 394.06180
356.0 0.002809 392.76312 392.76147
336.0 0.002976 391.47839 391.47684
338.0 0.002959 390.20923 390.20779
338.0 0.002959 388.95563 388.95419
367.0 0.002725 387.71744 387.71613
365.0 0.002740 386.49457 386.49341
314.0 0.003185 385.28705 385.28586
342.0 0.002924 384.09464 384.09357
386.0 0.002591 382.91724 382.91635
385.0 0.002597 381.75467 381.75381
375.0 0.002667 380.60724 380.60638
380.0 0.002632 379.47449 379.47375
349.0 0.002865 378.35635 378.35568
360.0 0.002778 377.25284 377.25223
366.0 0.002732 376.16364 376.16318
365.0 0.002740 375.08905 375.08865
343.0 0.002915 374.02881 374.02841
343.0 0.002915 372.98267 372.98242
359.0 0.002786 371.95065 371.95044
348.0 0.002874 370.93259 370.93243
344.0 0.002907 369.92868 369.92853
355.0 0.002817 368.93851 368.93851
351.0 0.002849 367.96210 367.96219
358.0 0.002793 366.99945 366.99951
349.0 0.002865 366.05014 366.05026
371.0 0.002695 365.11453 365.11478
360.0 0.002778 364.19235 364.19266
344.0 0.002907 363.28345 363.28375
366.0 0.002732 362.38779 362.38818
371.0 0.002695 361.50519 361.50574
371.0 0.002695 360.63580 360.63632
352.0 0.002841 359.77927 359.77991
365.0 0.002740 358.93567 358.93631
365.0 0.002740 358.10492 358.10556
340.0 0.002941 357.28677 357.28754
363.0 0.002755 356.48135 361.12711
349.0 0.002865 355.68848 362.89658
376.0 0.002660 354.90808 362.79572
364.0 0.002747 354.14005 362.82730
397.0 0.002519 353.38419 363.02951
386.0 0.002591 352.64078 363.46228
376.0 0.002660 351.90939 364.23309
422.0 0.002370 351.18997 365.64386
401.0 0.002494 350.48267 368.93588
414.0 0.002415 349.78711 377.13290
456.0 0.002193 349.10342 392.36658
462.0 0.002165 348.43161 414.11819
501.0 0.001996 347.77127 441.29037
476.0 0.002101 347.12253 472.48682
487.0 0.002053 346.48529 506.87634
521.0 0.001919 345.85947 544.48541
557.0 0.001795 345.24500 585.69281
605.0 0.001653 344.64175 631.03040
691.0 0.001447 344.04959 681.14728
698.0 0.001433 343.46863 736.79907
762.0 0.001312 342.89865 798.96570
848.0 0.001179 342.33963 869.07330
918.0 0.001089 341.79147 949.01404
1031.0 0.000970 341.25409 1041.12708
1085.0 0.000922 340.72736 1148.84644
1300.0 0.000769 340.21133 1277.15649
1516.0 0.000660 339.70587 1433.41248
1759.0 0.000569 339.21097 1629.85815
2144.0 0.000466 338.72632 1887.82751
2697.0 0.000371 338.25211 2252.71118
3537.0 0.0002827 337.78809 2837.70532
4215.0 0.0002372 337.33426 3731.72070
4260.0 0.0002347 336.89063 4152.38965
3376.0 0.0002962 336.45694 3164.03979
2177.0 0.000459 336.03333 2173.24023
1300.0 0.000769 335.61948 1191.25098
721.0 0.001387 335.21558 643.81329
509.0 0.001965 334.82135 486.59430
443.0 0.002257 334.43680 435.51727
402.0 0.002488 334.06189 408.13083
405.0 0.002469 333.69653 390.65894
408.0 0.002451 333.34064 378.68033
395.0 0.002532 332.99408 370.03665
407.0 0.002457 332.65683 363.54767
396.0 0.002525 332.32898 358.52045
371.0 0.002695 332.01022 354.52386
377.0 0.002653 331.70053 351.27707
377.0 0.002653 331.39996 348.59070
379.0 0.002639 331.10840 346.33264
350.0 0.002857 330.82571 344.40891
347.0 0.002882 330.55188 342.75040
366.0 0.002732 330.28677 341.30563
389.0 0.002571 330.03049 340.03552
400.0 0.002500 329.78278 338.90982
382.0 0.002618 329.54364 332.64401
357.0 0.002801 329.31302 332.15158
371.0 0.002695 329.09088 329.09357
361.0 0.002770 328.87708 328.87982
342.0 0.002924 328.67169 328.67432
385.0 0.002597 328.47449 328.47711
361.0 0.002770 328.28540 328.28809
345.0 0.002899 328.10449 328.10718
350.0 0.002857 327.93161 327.93442
330.0 0.003030 327.76675 327.76950
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1487.0 0.000672 375.46918 1432.59265
1239.0 0.000807 375.33871 1188.84790
761.0 0.001314 375.20895 762.75366
569.0 0.001757 375.07990 561.25665
469.0 0.002132 374.95123 495.30801
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1942.0 0.000515 372.98050 1960.80835
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1395.0 0.000717 372.51312 1404.95862
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750.0 0.001333 371.94308 729.90649
696.0 0.001437 371.83093 704.00623
773.0 0.001294 371.71948 766.15900
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1853.0 0.000540 371.27991 1789.25671
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1265.0 0.000791 371.06390 1334.67883
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1499.0 0.000667 370.85052 1455.31470
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1358.0 0.000736 370.43130 1410.62451
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1667.0 0.000600 367.85162 1605.67603
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803.0 0.001245 368.06085 812.94165
847.0 0.001181 368.13120 870.10535
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1251.0 0.000799 368.34402 1201.18689
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822.0 0.001217 368.63208 799.08411
662.0 0.001511 368.70483 674.14612
708.0 0.001412 368.77786 678.01331
781.0 0.001280 368.85126 752.50977
915.0 0.001093 368.92480 866.14526
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2666.0 0.000375 369.75354 2267.37769
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1296.0 0.000772 370.45602 1020.18835
812.0 0.001232 370.53546 686.39508
580.0 0.001724 370.61508 539.58893
506.0 0.001976 370.69501 485.63168
452.0 0.002212 370.77505 460.41968
455.0 0.002198 370.85541 445.35458
427.0 0.002342 370.93604 437.41385
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461.0 0.002169 371.17944 455.18564
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538.0 0.001859 371.34290 537.38593
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414.0 0.002415 373.99112 388.43982
379.0 0.002639 374.07986 385.07278
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349.0 0.002865 374.70605 377.74496
387.0 0.002584 374.79626 377.09683
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344.0 0.002907 374.97714 376.81931
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383.0 0.002611 377.76596 393.88834
399.0 0.002506 377.86115 401.79446
402.0 0.002488 377.95633 413.69077
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434.0 0.002304 378.81882 450.94791
477.0 0.002096 378.91522 461.07104
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393.0 0.002545 379.20511 433.42697
399.0 0.002506 379.30179 413.43082
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367.0 0.002725 379.49573 403.73645
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391.0 0.002558 379.78738 409.96060
442.0 0.002262 379.88474 417.10422
413.0 0.002421 379.98221 429.78973
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621.0 0.001610 384.53662 565.71991
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564.0 0.001773 384.73663 513.83856
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687.0 0.001456 384.93661 578.05365
742.0 0.001348 385.03677 677.10901
881.0 0.001135 385.13678 868.47260
1202.0 0.000832 385.23685 1177.80762
1628.0 0.000614 385.33691 1681.85071
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719.0 0.001391 386.53799 765.68372
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555.0 0.001802 386.73816 626.99841
574.0 0.001742 386.83817 593.34961
523.0 0.001912 386.93814 537.86853
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643.0 0.001555 387.43805 609.92041
593.0 0.001686 387.53799 584.78491
502.0 0.001992 387.63791 512.16187
450.0 0.002222 387.73770 471.88348
448.0 0.002232 387.83759 466.08206
445.0 0.002247 387.93732 477.50018
467.0 0.002141 388.03717 499.53430
487.0 0.002053 388.13687 512.37329
488.0 0.002049 388.23657 487.17328
470.0 0.002128 388.33624 453.29523
437.0 0.002288 388.43588 439.03671
422.0 0.002370 388.53546 439.15112
441.0 0.002268 388.63507 442.77252
468.0 0.002137 388.73465 460.18839
492.0 0.002033 388.83408 487.68445
532.0 0.001880 388.93347 524.99268
577.0 0.001733 389.03290 549.08649
563.0 0.001776 389.13229 521.72394
524.0 0.001908 389.23169 486.03555
524.0 0.001908 389.33090 476.35773
535.0 0.001869 389.43005 492.06958
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632.0 0.001582 389.62842 585.24725
765.0 0.001307 389.72748 673.52887
861.0 0.001161 389.82642 797.32806
1051.0 0.000951 389.92535 1028.09680
1438.0 0.000695 390.02429 1397.92651
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2344.0 0.000427 390.22186 2199.19604
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1511.0 0.000662 390.41922 1549.78809
1138.0 0.000879 390.51782 1201.73389
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1257.0 0.000796 391.00980 1206.51758
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910.0 0.001099 391.20612 935.37952
965.0 0.001036 391.30411 944.83539
1043.0 0.000959 391.40204 1008.19281
963.0 0.001038 391.49997 907.71631
674.0 0.001484 391.59775 694.60449
520.0 0.001923 391.69547 582.59882
588.0 0.001701 391.79306 564.10815
532.0 0.001880 391.89069 595.59308
654.0 0.001529 391.98813 655.91498
708.0 0.001412 392.08554 694.22632
682.0 0.001466 392.18286 624.02020
551.0 0.001815 392.28006 521.22791
470.0 0.002128 392.37717 468.20987
431.0 0.002320 392.47424 448.28552
448.0 0.002232 392.57120 440.37088
428.0 0.002336 392.66803 436.72995
439.0 0.002278 392.76480 435.61530
467.0 0.002141 392.86139 436.34811
434.0 0.002304 392.95804 438.85278
438.0 0.002283 393.05453 443.43839
479.0 0.002088 393.15088 448.52637
496.0 0.002016 393.24713 462.39151
509.0 0.001965 393.34335 486.72928
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653.0 0.001531 393.53540 605.75714
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428.0 0.002336 397.36600 433.10791
393.0 0.002545 397.45648 428.97433
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401.0 0.002494 397.63708 427.48734
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2493.0 0.000401 403.50391 2559.35010
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548.0 0.001825 404.40744 583.79565
537.0 0.001862 404.48120 562.84979
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677.0 0.001477 404.70108 655.07941
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439.0 0.002278 407.22995 446.87646
411.0 0.002433 407.29333 445.17905
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481.0 0.002079 407.48209 512.21808
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528.0 0.001894 407.60651 598.85663
543.0 0.001842 407.66833 599.99066
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658.0 0.001520 409.75983 702.01630
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563.0 0.001776 411.64719 651.76410
585.0 0.001709 411.68552 616.66211
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435.0 . . .
