#------------------------------------------------------------------------------ #$Date: 2025-07-01 14:30:34 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1272 $ #$URL: svn://localhost/testcod/cif/4/00/00/4000053.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4000053 loop_ _publ_author_name 'Zhou, Yongkai' 'Adams, Stefan' 'Rao, R. Prasada' 'Edwards, Doreen D.' 'Neiman, Arkady' 'Pestereva, N.' _publ_section_title ; Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3 ; _journal_issue 20 _journal_name_full 'Chemistry of Materials' _journal_page_first 6335 _journal_page_last 6345 _journal_paper_doi 10.1021/cm800466y _journal_volume 20 _journal_year 2008 _chemical_formula_moiety ' Sc2(WO4)3 ' _chemical_formula_sum 'O12 Sc2 W3' _chemical_formula_weight 833.45 _chemical_melting_point ' 1913K ' _chemical_name_common ' Scandium Tungstate ' _chemical_name_systematic ' Scandium Tungstate ' _space_group_IT_number 60 _space_group_name_Hall '-P 2a 2n' _space_group_name_H-M_alt 'P n c a' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M 'P n c a' _audit_creation_date 2008-01-25T12:03 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2008-01-25T12:03 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 9.62166(6) _cell_length_b 13.35709(8) _cell_length_c 9.54792(6) _cell_measurement_temperature 1150 _cell_volume 1227.074(13) _computing_structure_refinement GSAS _diffrn_radiation_polarisn_ratio 0.68 _diffrn_radiation_probe x-ray _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _pd_block_id 2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert _pd_calc_method 'Rietveld Refinement' _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.017 _pd_meas_2theta_range_max 119.9874 _pd_meas_2theta_range_min 10.0144 _pd_meas_number_of_points 6470 _pd_proc_2theta_range_inc 0.017 _pd_proc_2theta_range_max 119.9874 _pd_proc_2theta_range_min 10.0144 _pd_proc_info_datetime 2008-01-25T12:31:36 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 12 terms. Shifted Chebyshev function of 1st kind 1: 391.716 2: -17.2727 3: -17.5763 4: 60.8251 5: -7.69767 6: 10.7459 7: -12.1459 8: 5.44036 9: 10.5752 10: -24.9005 11: 20.9706 12: -5.99013 ; _pd_proc_ls_peak_cutoff 0.00250 _pd_proc_ls_pref_orient_corr ; March-Dollase AXIS 1 Ratio= 0.95556 h= 0.000 k= 1.000 l= 0.000 Prefered orientation correction range: Min= 0.93410, Max= 1.14609 ; _pd_proc_ls_profile_function ; CW Profile function number 3 with 19 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. #1(GU) = 8.967 #2(GV) = -7.536 #3(GW) = 2.655 #4(GP) = 0.000 #5(LX) = 0.727 #6(LY) = 5.405 #7(S/L) = 0.0316 #8(H/L) = 0.0250 #9(trns) = 0.00 #10(shft)= -17.8308 #11(stec)= 0.00 #12(ptec)= 0.00 #13(sfec)= 0.00 #14(L11) = 0.000 #15(L22) = 0.000 #16(L33) = 0.000 #17(L12) = 0.000 #18(L13) = 0.000 #19(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0025 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0490 _pd_proc_ls_prof_wR_expected 0.0365 _pd_proc_ls_prof_wR_factor 0.0639 _pd_proc_number_of_points 6470 _pd_spec_mounting ' ?' _refine_ls_goodness_of_fit_all 1.85 _refine_ls_matrix_type full _refine_ls_number_parameters 51 _refine_ls_number_restraints 0 _refine_ls_R_Fsqd_factor 0.07284 _refine_ls_shift/su_max 0.03 _refine_ls_shift/su_mean 0.01 _reflns_d_resolution_high 0.890 _reflns_d_resolution_low 6.679 _reflns_limit_h_max 10 _reflns_limit_h_min 0 _reflns_limit_k_max 15 _reflns_limit_k_min 0 _reflns_limit_l_max 10 _reflns_limit_l_min 0 _reflns_number_total 1823 _cod_data_source_file cm800466y_si_024.cif _cod_data_source_block T1150K _cod_original_cell_volume 1227.073(14) _cod_database_code 4000053 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x+1/2,+y+1/2,+z+1/2 3 +x,-y+1/2,+z+1/2 4 -x+1/2,-y,+z -1 -x,-y,-z -2 +x+1/2,-y+1/2,-z+1/2 -3 -x,+y+1/2,-z+1/2 -4 +x+1/2,+y,-z loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Sc Sc1 0.4712(4) 0.38253(26) 0.2469(5) 1.0 Uiso 0.0284(12) 8 W W1 0.25 0.0 0.47091(17) 1.0 Uiso 0.0335(4) 4 W W2 0.11236(12) 0.35634(9) 0.39043(12) 1.0 Uiso 0.0335(4) 8 O O1 0.0937(14) 0.1277(10) 0.0671(14) 1.0 Uiso 0.0776(22) 8 O O2 0.1529(14) 0.0779(9) 0.3756(15) 1.0 Uiso 0.0776(22) 8 O O3 0.0034(14) 0.2635(11) 0.3131(13) 1.0 Uiso 0.0776(22) 8 O O4 0.3351(14) 0.4063(9) 0.0740(14) 1.0 Uiso 0.0776(22) 8 O O5 0.0512(13) 0.4734(10) 0.3212(14) 1.0 Uiso 0.0776(22) 8 O O6 0.2921(15) 0.3481(10) 0.3393(14) 1.0 Uiso 0.0776(22) 8 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800 51.3531 1.33290 International_Tables_Vol_C W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982 57.0560 9.88750 International_Tables_Vol_C O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C loop_ _diffrn_radiation_wavelength _diffrn_radiation_wavelength_wt _diffrn_radiation_type _diffrn_radiation_wavelength_id 1.540500 1.000 K\a~1~ 1 1.544300 0.000 K\a~2~ 2 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Sc1 O2 91.1(5) -2_666 . -2_666 N O1 Sc1 O3 95.0(5) -2_666 . -2_666 N O1 Sc1 O4 173.1(6) -2_666 . 1_555 N O1 Sc1 O5 80.3(5) -2_666 . 4_565 N O1 Sc1 O6 95.4(6) -2_666 . 1_555 N O2 Sc1 O3 87.7(6) -2_666 . -2_666 N O2 Sc1 O4 92.4(6) -2_666 . 1_555 N O2 Sc1 O5 92.4(5) -2_666 . 4_565 N O2 Sc1 O6 173.5(6) -2_666 . 1_555 N O3 Sc1 O4 91.0(5) -2_666 . 1_555 N O3 Sc1 O5 175.3(6) -2_666 . 4_565 N O3 Sc1 O6 92.0(5) -2_666 . 1_555 N O4 Sc1 O5 93.6(5) 1_555 . 4_565 N O4 Sc1 O6 81.1(5) 1_555 . 1_555 N O5 Sc1 O6 88.4(5) 4_565 . 1_555 N O2 W1 O2 113.9(10) 1_555 . 4_555 N O2 W1 O4 118.7(6) 1_555 . 2_545 N O2 W1 O4 96.9(6) 1_555 . 3_555 N O2 W1 O4 96.9(6) 4_555 . 2_545 N O2 W1 O4 118.7(6) 4_555 . 3_555 N O4 W1 O4 113.3(8) 2_545 . 3_555 N O1 W2 O3 115.7(6) 3_555 . 1_555 N O1 W2 O5 102.7(6) 3_555 . 1_555 N O1 W2 O6 112.1(6) 3_555 . 1_555 N O3 W2 O5 105.1(7) 1_555 . 1_555 N O3 W2 O6 114.2(6) 1_555 . 1_555 N O5 W2 O6 105.5(6) 1_555 . 1_555 N Sc1 O1 W2 152.4(8) -2_466 . 3_554 N Sc1 O2 W1 153.8(8) -2_555 . 1_555 N Sc1 O3 W2 149.7(8) -2_466 . 1_555 N Sc1 O4 W1 144.2(8) 1_555 . 2_554 N Sc1 O5 W2 166.6(8) 4_565 . 1_555 N Sc1 O6 W2 159.7(8) 1_555 . 1_555 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sc1 O1 2.136(14) . -2_555 N Sc1 O2 2.168(14) . -2_555 N Sc1 O3 2.056(14) . -2_555 N Sc1 O4 2.130(13) . 1_555 N Sc1 O5 2.063(13) . 4_565 N Sc1 O6 1.990(14) . 1_555 N W1 O2 1.669(13) . 1_555 N W1 O2 1.669(13) . 4_555 N W1 O4 1.791(12) . 2_545 N W1 O4 1.791(12) . 3_555 N W2 O1 1.710(13) . 3_555 N W2 O3 1.784(13) . 1_555 N W2 O5 1.796(13) . 1_555 N W2 O6 1.800(15) . 1_555 N O1 Sc1 2.136(14) . -2_455 N O1 W2 1.710(13) . 3_554 N O2 Sc1 2.168(14) . -2_455 N O2 W1 1.669(13) . 1_555 N O3 Sc1 2.056(14) . -2_455 N O3 W2 1.784(13) . 1_555 N O4 Sc1 2.130(13) . 1_555 N O4 W1 1.791(12) . 2_554 N O5 Sc1 2.063(13) . 4_565 N O5 W2 1.796(13) . 1_555 N O6 Sc1 1.990(14) . 1_555 N O6 W2 1.800(15) . 1_555 N loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 300.0 0.0 628.72083 . 274.0 0.0 625.02985 . 277.0 0.0 621.36749 . 314.0 0.0 617.73352 . 315.0 0.0 614.12744 . 294.0 0.0 610.54999 . 305.0 0.0 607.00031 . 301.0 0.0 603.47821 . 289.0 0.0 599.98419 . 311.0 0.0 596.51703 . 304.0 0.0 593.07788 . 286.0 0.0 589.66559 . 311.0 0.0 586.28064 . 295.0 0.0 582.92261 . 323.0 0.0 579.59143 . 319.0 0.0 576.28693 . 300.0 0.0 573.00897 . 269.0 0.0 569.75708 . 260.0 0.0 566.53217 . 263.0 0.0 563.33325 . 283.0 0.0 560.16034 . 270.0 0.0 557.01318 . 294.0 0.0 553.89154 . 305.0 0.0 550.79596 . 288.0 0.0 547.72595 . 301.0 0.0 544.68109 . 294.0 0.0 541.66144 . 278.0 0.0 538.66687 . 295.0 0.0 535.69727 . 307.0 0.0 532.75299 . 295.0 0.0 529.83282 . 297.0 0.0 526.93750 . 312.0 0.0 524.06641 . 295.0 0.0 521.22009 . 302.0 0.0 518.39795 . 310.0 0.0 515.59967 . 311.0 0.0 512.82544 . 319.0 0.0 510.07480 . 287.0 0.0 507.34818 . 289.0 0.0 504.64520 . 315.0 0.0 501.96552 . 300.0 0.0 499.30917 . 313.0 0.0 496.67584 . 313.0 0.0 494.06589 . 316.0 0.0 491.47910 . 312.0 0.0 488.91486 . 327.0 0.0 486.37335 . 321.0 0.0 483.85431 . 282.0 0.0 481.35812 . 293.0 0.0 478.88419 . 294.0 0.0 476.43259 . 326.0 0.0 474.00281 . 333.0 0.0 471.59509 . 301.0 0.0 469.20938 . 284.0 0.0 466.84558 . 313.0 0.0 464.50330 . 307.0 0.0 462.18253 . 300.0 0.0 459.88306 . 312.0 0.0 457.60519 . 325.0 0.0 455.34857 . 303.0 0.0 453.11285 . 295.0 0.0 450.89792 . 303.0 0.0 448.70392 . 293.0 0.0 446.53079 . 263.0 0.0 444.37836 . 313.0 0.0 442.24640 . 287.0 0.0 440.13467 . 323.0 0.0 438.04327 . 315.0 0.0 435.97208 . 309.0 0.0 433.92108 . 292.0 0.0 431.89005 . 306.0 0.0 429.87863 . 316.0 0.0 427.88702 . 306.0 0.0 425.91507 . 298.0 0.0 423.96280 . 288.0 0.0 422.02975 . 295.0 0.0 420.11594 . 320.0 0.0 418.22150 . 318.0 0.0 416.34595 . 331.0 0.0 414.48953 . 357.0 0.0 412.65207 . 332.0 0.0 410.83322 . 300.0 0.0 409.03293 . 314.0 0.0 407.25131 . 325.0 0.0 405.48837 . 308.0 0.0 403.74353 . 301.0 0.0 402.01694 . 329.0 0.0 400.30856 . 322.0 0.0 398.61813 . 321.0 0.0 396.94574 . 337.0 0.0 395.29117 . 343.0 0.0 393.65421 . 333.0 0.0 392.03488 . 315.0 0.0 390.43317 . 309.0 0.0 388.84885 . 322.0 0.0 387.28204 . 318.0 0.0 385.73215 . 296.0 0.0 384.19949 . 301.0 0.0 382.68393 . 315.0 0.0 381.18527 . 326.0 0.0 379.70352 . 310.0 0.0 378.23831 . 309.0 0.0 376.78979 . 323.0 0.0 375.35797 . 317.0 0.0 373.94241 . 291.0 0.0 372.54340 . 302.0 0.0 371.16031 . 277.0 0.0 369.79367 . 290.0 0.0 368.44299 . 312.0 0.0 367.10822 . 364.0 0.0 365.78943 . 304.0 0.0 364.48627 . 318.0 0.0 363.19888 . 332.0 0.0 361.92719 . 334.0 0.0 360.67081 . 311.0 0.0 359.42987 . 307.0 0.0 358.20432 . 311.0 0.003215 356.99387 356.99951 303.0 0.003300 355.79861 355.80432 309.0 0.003236 354.61838 354.62402 314.0 0.003185 353.45313 353.45868 315.0 0.003175 352.30273 352.30826 273.0 0.00366 351.16696 351.17242 300.0 0.003333 350.04602 350.05142 343.0 0.002915 348.93967 348.94498 333.0 0.003003 347.84784 347.85297 306.0 0.003268 346.77026 346.77542 323.0 0.003096 345.70697 345.71216 334.0 0.002994 344.65808 344.66321 311.0 0.003215 343.62329 343.62830 309.0 0.003236 342.60260 342.60764 297.0 0.003367 341.59579 341.60080 303.0 0.003300 340.60284 340.60779 306.0 0.003268 339.62375 339.62863 316.0 0.003165 338.65839 338.66321 298.0 0.003356 337.70667 337.71136 298.0 0.003356 336.76849 336.77319 301.0 0.003322 335.84369 335.84830 295.0 0.003390 334.93231 334.93692 312.0 0.003205 334.03430 334.03879 302.0 0.003311 333.14941 333.15387 289.0 0.003460 332.27768 332.28210 307.0 0.003257 331.41882 331.42322 315.0 0.003175 330.57318 330.57739 317.0 0.003155 329.74026 329.74451 303.0 0.003300 328.92014 328.92441 285.0 0.00351 328.11276 328.11694 303.0 0.003300 327.31793 327.32211 321.0 0.003115 326.53583 326.53983 302.0 0.003311 325.76605 325.77014 316.0 0.003165 325.00867 325.01270 343.0 0.002915 324.26370 324.26764 326.0 0.003067 323.53085 323.53473 300.0 0.003333 322.81021 322.81406 308.0 0.003247 322.10162 322.10544 318.0 0.003145 321.40506 321.40881 303.0 0.003300 320.72040 320.72412 300.0 0.003333 320.04745 320.05115 313.0 0.003195 319.38644 319.39017 330.0 0.003030 318.73706 318.74069 298.0 0.003356 318.09927 318.10278 317.0 0.003155 317.47293 317.47653 314.0 0.003185 316.85812 316.86169 340.0 0.002941 316.25473 316.25821 349.0 0.002865 315.66263 315.66602 338.0 0.002959 315.08173 315.08514 352.0 0.002841 314.51196 314.51532 321.0 0.003115 313.95325 313.95657 351.0 0.002849 313.40564 317.15842 318.0 0.003145 312.86884 316.95621 348.0 0.002874 312.34296 318.69366 370.0 0.002703 311.82782 318.80331 362.0 0.002762 311.32343 319.04092 346.0 0.002890 310.82965 319.44720 347.0 0.002882 310.34650 320.09070 381.0 0.002625 309.87384 321.13870 365.0 0.002740 309.41153 323.27301 406.0 0.002463 308.95956 328.61465 400.0 0.002500 308.51785 339.90735 390.0 0.002564 308.08643 357.65182 410.0 0.002439 307.66513 380.94745 442.0 0.002262 307.25381 408.58920 455.0 0.002198 306.85254 439.47409 435.0 0.002299 306.46124 473.33273 491.0 0.002037 306.07974 510.39185 529.0 0.001890 305.70810 551.06256 551.0 0.001815 305.34613 595.92792 590.0 0.001695 304.99371 645.69055 646.0 0.001548 304.65100 701.23376 676.0 0.001479 304.31781 763.78314 751.0 0.001332 303.99405 834.85522 879.0 0.001138 303.67963 916.59308 981.0 0.001019 303.37451 1011.90192 1068.0 0.000936 303.07864 1125.00500 1254.0 0.000797 302.79202 1262.26001 1532.0 0.000653 302.51450 1433.90906 1810.0 0.000552 302.24597 1658.07056 2255.0 0.000443 301.98648 1973.05920 2922.0 0.0003422 301.73590 2473.12671 3660.0 0.0002732 301.49417 3249.82080 3959.0 0.0002526 301.26123 3790.35254 3293.0 0.0003037 301.03705 3146.52002 2202.0 0.000454 300.82141 2176.04297 1311.0 0.000763 300.61444 1265.11316 710.0 0.001408 300.41599 654.17969 439.0 0.002278 300.22607 447.03110 384.0 0.002604 300.04449 390.41238 381.0 0.002625 299.87128 365.07343 354.0 0.002825 299.70639 349.46155 341.0 0.002933 299.54965 338.92169 365.0 0.002740 299.40103 331.41989 358.0 0.002793 299.26065 325.86227 367.0 0.002725 299.12817 321.61319 346.0 0.002890 299.00372 318.28094 332.0 0.003012 298.88730 315.61197 342.0 0.002924 298.77856 313.43665 323.0 0.003096 298.67767 311.63696 319.0 0.003135 298.58447 310.12955 302.0 0.003311 298.49902 308.85342 345.0 0.002899 298.42120 307.76303 366.0 0.002732 298.35086 306.82404 336.0 0.002976 298.28802 306.01004 328.0 0.003049 298.23267 300.85608 321.0 0.003115 298.18472 300.58432 357.0 0.002801 298.14407 298.14609 390.0 0.002564 298.11063 298.11267 323.0 0.003096 298.08447 298.08643 337.0 0.002967 298.06543 298.06738 283.0 0.00353 298.05347 298.05545 308.0 0.003247 298.04855 298.05054 331.0 0.003021 298.05063 298.05258 372.0 0.002688 298.05963 298.06161 356.0 0.002809 298.07553 298.07742 332.0 0.003012 298.09814 298.10013 345.0 0.002899 298.12762 298.12958 357.0 0.002801 298.16376 298.16565 298.0 0.003356 298.20660 298.20847 308.0 0.003247 298.25595 298.25784 326.0 0.003067 298.31186 298.31378 357.0 0.002801 298.37433 298.37616 328.0 0.003049 298.44318 298.44495 332.0 0.003012 298.51837 298.52020 335.0 0.002985 298.59991 298.60175 357.0 0.002801 298.68777 298.68954 340.0 0.002941 298.78177 298.78354 349.0 0.002865 298.88199 298.88382 359.0 0.002786 298.98828 298.99014 334.0 0.002994 299.10074 299.10245 323.0 0.003096 299.21912 299.22086 326.0 0.003067 299.34351 299.34521 326.0 0.003067 299.47372 304.27646 328.0 0.003049 299.60986 304.80487 339.0 0.002950 299.75180 307.75711 363.0 0.002755 299.89948 308.60913 370.0 0.002703 300.05289 309.57486 361.0 0.002770 300.21191 310.68124 379.0 0.002639 300.37656 311.96588 404.0 0.002475 300.54678 313.48389 376.0 0.002660 300.72247 315.32111 389.0 0.002571 300.90363 317.63535 410.0 0.002439 301.09018 320.90405 415.0 0.002410 301.28217 327.02591 434.0 0.002304 301.47949 340.40656 462.0 0.002165 301.68195 364.31525 487.0 0.002053 301.88968 398.11053 509.0 0.001965 302.10263 440.71088 534.0 0.001873 302.32062 490.56851 587.0 0.001704 302.54373 546.35443 605.0 0.001653 302.77185 608.04346 654.0 0.001529 303.00494 676.43610 712.0 0.001404 303.24301 752.72058 782.0 0.001279 303.48593 838.34521 901.0 0.001110 303.73376 935.32922 998.0 0.001002 303.98627 1046.45508 1078.0 0.000928 304.24356 1175.35791 1241.0 0.000806 304.50555 1327.47644 1489.0 0.000672 304.77231 1510.73169 1770.0 0.000565 305.04361 1737.69189 2069.0 0.000483 305.31940 2029.88208 2549.0 0.000392 305.59979 2430.39307 3319.0 0.0003013 305.88464 3044.63135 4172.0 0.0002397 306.17395 4039.21558 4863.0 0.0002056 306.46765 5002.03613 4096.0 0.0002441 306.76569 4472.37744 2910.0 0.0003436 307.06805 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644.60815 694.0 0.001441 498.26807 629.91241 666.0 0.001502 498.41690 620.66980 656.0 0.001524 498.56396 610.91888 637.0 0.001570 498.70944 602.93335 631.0 0.001585 498.85330 549.68805 673.0 0.001486 498.99542 548.55005 668.0 0.001497 499.13580 548.13367 655.0 0.001527 499.27460 523.96155 673.0 0.001486 499.41174 527.07501 708.0 0.001412 499.54736 530.83276 649.0 0.001541 499.68118 535.46997 721.0 0.001387 499.81335 541.38507 659.0 0.001517 499.94394 549.44928 727.0 0.001376 500.07285 562.67230 774.0 0.001292 500.20010 589.49951 775.0 0.001290 500.32578 639.30518 791.0 0.001264 500.44977 712.48157 888.0 0.001126 500.57208 806.76135 973.0 0.001028 500.69290 927.09991 1069.0 0.000935 500.81201 1079.24500 1292.0 0.000774 500.92947 1268.49365 1523.0 0.000657 501.04535 1508.89050 1715.0 0.000583 501.15964 1823.51868 2211.0 0.000452 501.27228 2245.24194 2925.0 0.0003419 501.38336 2846.94019 4198.0 0.0002382 501.49274 3790.72388 5160.0 0.0001938 501.60065 5008.10596 5115.0 0.0001955 501.70679 5168.28564 3942.0 0.0002537 501.81146 3866.46436 3396.0 0.0002945 501.91455 3460.04761 3561.0 0.0002808 502.01596 3639.23950 3189.0 0.0003136 502.11578 3191.58667 2914.0 0.0003432 502.21414 3013.33936 3235.0 0.0003091 502.31079 3455.38330 3101.0 0.0003225 502.40591 3278.16821 2304.0 0.000434 502.49945 2297.46948 1819.0 0.000550 502.59146 1956.91003 1717.0 0.000582 502.68182 1882.12891 1314.0 0.000761 502.77066 1315.85205 829.0 0.001206 502.85794 837.72607 664.0 0.001506 502.94370 671.67145 647.0 0.001546 503.02789 618.50067 623.0 0.001605 503.11044 591.24231 623.0 0.001605 503.19162 573.60205 589.0 0.001698 503.27112 561.25134 554.0 0.001805 503.34915 552.17346 562.0 0.001779 503.42557 545.24951 570.0 0.001754 503.50049 539.82245 563.0 0.001776 503.57385 527.77136 570.0 0.001754 503.64575 524.85962 578.0 0.001730 503.71616 522.48260 568.0 0.001761 503.78497 520.51477 563.0 0.001776 503.85223 515.24335 523.0 0.001912 503.91803 514.14368 521.0 0.001919 503.98233 513.21472 553.0 0.001808 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505.28217 584.52545 591.0 0.001692 505.26584 584.38153 604.0 0.001656 505.24823 585.41003 592.0 0.001689 505.22940 587.63904 631.0 0.001585 505.20923 576.51288 678.0 0.001475 505.18777 582.62616 697.0 0.001435 505.16522 590.25903 719.0 0.001391 505.14133 592.18250 730.0 0.001370 505.11621 604.88171 747.0 0.001339 505.08984 620.92218 807.0 0.001239 505.06226 641.84113 870.0 0.001149 505.03348 670.68726 1021.0 0.000979 505.00342 717.04767 1171.0 0.000854 504.97217 811.35687 1336.0 0.000749 504.93970 1001.14001 1612.0 0.000620 504.90610 1299.58606 1831.0 0.000546 504.87119 1691.65662 2186.0 0.000457 504.83502 2192.87109 2714.0 0.000368 504.79776 2841.32153 3401.0 0.0002940 504.75934 3667.70288 4270.0 0.0002342 504.71970 4719.56055 5684.0 0.0001759 504.67889 6103.98291 7773.0 0.0001287 504.63693 8066.99414 11298.0 0.0000885 504.59375 11170.47559 16277.0 0.0000614 504.54944 15520.77148 17990.0 0.0000556 504.50391 16863.37695 11472.0 0.0000872 504.45728 11447.21582 8174.0 0.0001223 504.40945 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483.76596 498.49850 489.0 0.002045 483.59030 496.34738 444.0 0.002252 483.41425 494.57932 437.0 0.002288 483.23776 492.12207 412.0 0.002427 483.06104 490.94312 433.0 0.002309 482.88385 489.92691 417.0 0.002398 482.70639 489.03970 470.0 0.002128 482.52850 484.96735 453.0 0.002208 482.35022 484.54230 421.0 0.002375 482.17169 484.15289 432.0 0.002315 481.99283 483.79218 470.0 0.002128 481.81366 481.81186 427.0 0.002342 481.63406 481.63232 441.0 0.002268 481.45422 481.45236 405.0 0.002469 481.27402 481.27216 437.0 0.002288 481.09351 481.09167 444.0 0.002252 480.91272 480.91086 456.0 0.002193 480.73169 480.72974 466.0 0.002146 480.55020 480.54825 452.0 0.002212 480.36847 480.36652 450.0 0.002222 480.18643 480.18448 479.0 0.002088 480.00421 480.00217 455.0 0.002198 479.82159 479.81955 437.0 0.002288 479.63867 479.63669 438.0 0.002283 479.45566 479.45355 412.0 0.002427 479.27216 479.27008 425.0 0.002353 479.08847 479.08636 455.0 0.002198 478.90454 478.90240 442.0 0.002262 478.72025 478.71817 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3048.29321 2000.0 0.000500 467.91595 1857.53064 1680.0 0.000595 467.72333 1546.99158 1709.0 0.000585 467.53055 1579.99890 1444.0 0.000693 467.33777 1328.96350 974.0 0.001027 467.14490 899.27228 684.0 0.001462 466.95212 694.38287 599.0 0.001669 466.75928 625.65796 592.0 0.001689 466.56638 591.79590 557.0 0.001795 466.37344 570.12054 539.0 0.001855 466.18060 554.92493 535.0 0.001869 465.98770 543.78870 549.0 0.001821 465.79477 535.42194 559.0 0.001789 465.60187 529.05884 528.0 0.001894 465.40891 514.43195 525.0 0.001905 465.21603 511.66006 521.0 0.001919 465.02307 509.84723 527.0 0.001898 464.83023 503.42590 503.0 0.001988 464.63736 500.21658 536.0 0.001866 464.44449 501.96652 547.0 0.001828 464.25168 504.67578 529.0 0.001890 464.05881 502.16254 530.0 0.001887 463.86609 508.31216 574.0 0.001742 463.67337 517.67877 577.0 0.001733 463.48056 531.10327 685.0 0.001460 463.28793 554.90027 697.0 0.001435 463.09531 608.69574 772.0 0.001295 462.90268 698.99542 873.0 0.001145 462.71024 829.94318 1030.0 0.000971 462.51770 1001.41876 1225.0 0.000816 462.32532 1226.40259 1495.0 0.000669 462.13281 1537.13599 1957.0 0.000511 461.94058 1987.73926 2721.0 0.000368 461.74838 2687.42432 3911.0 0.0002557 461.55615 3688.81470 4220.0 0.0002370 461.36411 4160.64111 2923.0 0.0003421 461.17200 2967.11304 1923.0 0.000520 460.98007 2028.90332 2000.0 0.000500 460.78821 2033.11401 2255.0 0.000443 460.59641 2294.68384 1851.0 0.000540 460.40472 1861.18481 1071.0 0.000934 460.21304 1098.28857 718.0 0.001393 460.02158 775.03668 658.0 0.001520 459.83014 706.23859 659.0 0.001517 459.63882 712.82574 664.0 0.001506 459.44760 753.72754 761.0 0.001314 459.25647 825.54535 870.0 0.001149 459.06555 936.53796 1082.0 0.000924 458.87463 1109.06580 1372.0 0.000729 458.68381 1387.17993 1689.0 0.000592 458.49316 1739.84912 1700.0 0.000588 458.30264 1741.30420 1224.0 0.000817 458.11227 1253.58081 1022.0 0.000978 457.92197 1022.23474 1076.0 0.000929 457.73175 1079.56763 1118.0 0.000894 457.54181 1144.74280 931.0 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1314.64001 1181.0 0.000847 417.93857 1148.15015 1278.0 0.000782 418.00308 1214.68030 1610.0 0.000621 418.06812 1455.11841 2044.0 0.000489 418.13336 1756.33447 2012.0 0.000497 418.19901 1656.41699 1363.0 0.000734 418.26498 1180.97290 995.0 0.001005 418.33130 912.97906 964.0 0.001037 418.39798 875.99799 1053.0 0.000950 418.46500 949.92883 1230.0 0.000813 418.53241 1058.88074 1151.0 0.000869 418.60010 1022.63397 1075.0 0.000930 418.66809 949.59857 1120.0 0.000893 418.73654 1051.74194 1407.0 0.000711 418.80524 1332.98230 1852.0 0.000540 418.87433 1797.76379 2383.0 0.000420 418.94366 2363.52197 2558.0 0.000391 419.01337 2562.41211 2574.0 0.000389 419.08350 2634.89771 3057.0 0.0003271 419.15390 3120.83228 3108.0 0.0003218 419.22455 3220.34180 2785.0 0.000359 419.29565 2822.10986 2779.0 0.000360 419.36700 2837.87329 2458.0 0.000407 419.43872 2511.52588 1921.0 0.000521 419.51071 1965.66187 1759.0 0.000569 419.58307 1894.12598 1660.0 0.000602 419.65573 1775.54919 1461.0 0.000684 419.72870 1418.77979 1244.0 0.000804 419.80200 1265.78577 1028.0 0.000973 419.87558 1053.90710 811.0 0.001233 419.94952 770.05042 681.0 0.001468 420.02383 636.29767 607.0 0.001647 420.09836 597.02203 631.0 0.001585 420.17325 604.71497 712.0 0.001404 420.24835 648.49847 758.0 0.001319 420.32382 734.45459 905.0 0.001105 420.39966 866.91144 1181.0 0.000847 420.47577 1085.29639 1568.0 0.000638 420.55219 1385.44141 1679.0 0.000596 420.62897 1532.16479 1270.0 0.000787 420.70593 1188.51025 883.0 0.001133 420.78326 877.92303 852.0 0.001174 420.86081 830.22095 984.0 0.001016 420.93872 940.69159 1213.0 0.000824 421.01697 1140.91223 1414.0 0.000707 421.09549 1328.39734 1383.0 0.000723 421.17422 1311.77380 1175.0 0.000851 421.25330 1187.31433 903.0 0.001107 421.33276 907.61884 712.0 0.001404 421.41238 710.16870 674.0 0.001484 421.49231 660.41888 731.0 0.001368 421.57254 693.19495 792.0 0.001263 421.65308 767.62512 897.0 0.001115 421.73392 813.48553 843.0 0.001186 421.81491 734.70795 767.0 0.001304 421.89636 677.04480 775.0 0.001290 421.97797 731.76569 971.0 0.001030 422.05991 890.98260 1268.0 0.000789 422.14212 1166.44055 1655.0 0.000604 422.22458 1598.77087 2319.0 0.000431 422.30740 2240.63721 3208.0 0.0003117 422.39035 3008.61230 3493.0 0.0002863 422.47366 3224.22241 3021.0 0.0003310 422.55725 2704.25879 2016.0 0.000496 422.64105 1842.29077 1365.0 0.000733 422.72525 1421.89514 1455.0 0.000687 422.80951 1492.98999 1800.0 0.000556 422.89410 1784.95630 1888.0 0.000530 422.97906 1881.83350 1709.0 0.000585 423.06421 1595.09998 1257.0 0.000796 423.14957 1089.07129 757.0 0.001321 423.23529 734.70935 575.0 0.001739 423.32114 594.47131 540.0 0.001852 423.40741 540.28448 500.0 0.002000 423.49377 511.87698 464.0 0.002155 423.58044 494.11832 495.0 0.002020 423.66742 481.75934 501.0 0.001996 423.75458 473.69449 482.0 0.002075 423.84204 467.36319 474.0 0.002110 423.92966 463.92236 450.0 0.002222 424.01761 461.84323 454.0 0.002203 424.10577 461.33557 445.0 0.002247 424.19418 462.82913 432.0 0.002315 424.28287 468.01602 466.0 0.002146 424.37170 481.01370 492.0 0.002033 424.46088 507.83121 560.0 0.001786 424.55023 552.26947 648.0 0.001543 424.63983 619.36163 762.0 0.001312 424.72961 725.96539 921.0 0.001086 424.81976 874.18268 979.0 0.001021 424.91003 958.31512 829.0 0.001206 425.00055 792.34637 633.0 0.001580 425.09122 619.03143 592.0 0.001689 425.18228 573.49738 591.0 0.001692 425.27347 594.27777 622.0 0.001608 425.36493 653.49445 709.0 0.001410 425.45654 704.20410 662.0 0.001511 425.54834 637.98431 560.0 0.001786 425.64053 532.33734 508.0 0.001969 425.73282 490.36523 486.0 0.002058 425.82532 487.89767 512.0 0.001953 425.91803 506.11334 552.0 0.001812 426.01102 542.65210 575.0 0.001739 426.10413 601.55524 700.0 0.001429 426.19757 690.93610 748.0 0.001337 426.29108 772.21741 717.0 0.001395 426.38483 706.78497 573.0 0.001745 426.47882 574.16620 546.0 0.001832 426.57309 523.35913 531.0 0.001883 426.66745 526.93726 524.0 0.001908 426.76212 558.88092 581.0 0.001721 426.85687 599.88763 535.0 0.001869 426.95187 584.79187 450.0 0.002222 427.04709 508.86945 462.0 0.002165 427.14249 464.01492 423.0 0.002364 427.23810 448.03842 407.0 0.002457 427.33386 441.76755 389.0 0.002571 427.42981 438.37799 421.0 0.002375 427.52597 436.23938 421.0 0.002375 427.62238 434.79129 399.0 0.002506 427.71890 433.03558 407.0 0.002457 427.81564 432.32730 384.0 0.002604 427.91251 431.80130 444.0 0.002252 428.00958 431.40439 432.0 0.002315 428.10687 431.10208 414.0 0.002415 428.20438 430.87085 404.0 0.002475 428.30200 430.69455 442.0 0.002262 428.39978 430.21738 430.0 0.002326 428.49783 430.14026 402.0 0.002488 428.59592 430.08914 414.0 0.002415 428.69427 430.11105 393.0 0.002545 428.79272 430.10220 407.0 0.002457 428.89145 430.10864 430.0 0.002326 428.99030 430.26877 427.0 0.002342 429.08926 430.30896 435.0 0.002299 429.18848 430.36023 445.0 0.002247 429.28775 429.95615 441.0 0.002268 429.38724 430.08252 423.0 0.002364 429.48697 430.19104 427.0 0.002342 429.58673 430.37579 440.0 0.002273 429.68674 430.50537 445.0 0.002247 429.78693 430.64548 429.0 0.002331 429.88721 430.56268 432.0 0.002315 429.98758 430.74667 438.0 0.002283 430.08823 430.95145 402.0 0.002488 430.18900 431.18777 396.0 0.002525 430.28992 431.48099 404.0 0.002475 430.39087 431.90347 424.0 0.002358 430.49207 432.58994 444.0 0.002252 430.59344 433.59079 425.0 0.002353 430.69498 435.15558 411.0 0.002433 430.79648 437.32532 432.0 0.002315 430.89828 440.57965 432.0 0.002315 431.00021 443.46896 429.0 0.002331 431.10223 442.12064 444.0 0.002252 431.20438 438.81458 428.0 0.002336 431.30670 438.29559 434.0 0.002304 431.40915 440.16849 440.0 0.002273 431.51175 444.32214 439.0 0.002278 431.61447 451.06067 465.0 0.002151 431.71732 461.11121 468.0 0.002137 431.82022 474.04498 530.0 0.001887 431.92331 496.71744 588.0 0.001701 432.02655 522.67560 576.0 0.001736 432.12994 540.39990 611.0 0.001637 432.23334 549.63757 560.0 0.001786 432.33691 527.51843 507.0 0.001972 432.44058 489.96582 454.0 0.002203 432.54443 479.47501 486.0 0.002058 432.64838 486.01920 481.0 0.002079 432.75244 494.21127 516.0 0.001938 432.85654 498.75201 503.0 0.001988 432.96091 495.33328 433.0 0.002309 433.06519 472.35153 428.0 0.002336 433.16977 457.73248 450.0 0.002222 433.27435 453.04712 398.0 0.002513 433.37909 452.18246 420.0 0.002381 433.48380 452.70618 436.0 0.002294 433.58878 454.12189 460.0 0.002174 433.69379 456.48926 468.0 0.002137 433.79895 460.44620 442.0 0.002262 433.90414 467.65268 455.0 0.002198 434.00943 479.76895 491.0 0.002037 434.11487 499.03076 541.0 0.001848 434.22034 527.50592 589.0 0.001698 434.32593 570.09027 641.0 0.001560 434.43161 617.63635 628.0 0.001592 434.53741 618.25323 591.0 0.001692 434.64331 567.23633 562.0 0.001779 434.74927 548.60181 556.0 0.001799 434.85529 566.96600 644.0 0.001553 434.96133 610.87067 738.0 0.001355 435.06763 688.95343 860.0 0.001163 435.17392 811.29144 1024.0 0.000977 435.28030 982.44995 1312.0 0.000762 435.38675 1282.29407 1865.0 0.000536 435.49332 1777.66724 2630.0 0.000380 435.59988 2555.61255 3218.0 0.0003108 435.70654 3311.95190 2847.0 0.000351 435.81329 2934.33521 1807.0 0.000553 435.92014 1756.86768 1173.0 0.000853 436.02707 1211.74255 1108.0 0.000903 436.13397 1191.90588 1362.0 0.000734 436.24103 1408.61450 1752.0 0.000571 436.34821 1785.04297 1861.0 0.000537 436.45529 1931.73352 1451.0 0.000689 436.56250 1382.77686 926.0 0.001080 436.66977 870.17450 658.0 0.001520 436.77716 666.24152 595.0 0.001681 436.88458 601.51495 612.0 0.001634 436.99210 588.64154 624.0 0.001603 437.09958 604.48114 672.0 0.001488 437.20718 651.50226 794.0 0.001259 437.31479 735.19849 992.0 0.001008 437.42255 870.70117 1223.0 0.000818 437.53021 996.47894 1139.0 0.000878 437.63800 910.37115 802.0 0.001247 437.74582 701.70825 638.0 0.001567 437.85370 610.17743 635.0 0.001575 437.96170 609.04077 654.0 0.001529 438.06961 649.32129 802.0 0.001247 438.17767 717.42548 836.0 0.001196 438.28571 744.96539 701.0 0.001427 438.39374 649.73730 564.0 0.001773 438.50192 563.52441 498.0 0.002008 438.61011 533.31580 523.0 0.001912 438.71832 529.51007 560.0 0.001786 438.82657 536.69525 559.0 0.001789 438.93484 553.11096 644.0 0.001553 439.04315 579.76343 701.0 0.001427 439.15152 643.56152 807.0 0.001239 439.25983 778.75818 987.0 0.001013 439.36819 1011.37354 1315.0 0.000760 439.47668 1403.68152 1874.0 0.000534 439.58508 1989.62671 2785.0 0.000359 439.69360 2854.69922 3494.0 0.0002862 439.80203 3473.37451 2819.0 0.000355 439.91052 2698.17383 1639.0 0.000610 440.01910 1633.64270 1206.0 0.000829 440.12766 1286.00525 1259.0 0.000794 440.23618 1399.97058 1563.0 0.000640 440.34479 1699.02454 1900.0 0.000526 440.45334 2016.53503 1988.0 0.000503 440.56195 1991.53870 1441.0 0.000694 440.67056 1346.48389 894.0 0.001119 440.77921 878.43488 668.0 0.001497 440.88788 715.54041 633.0 0.001580 440.99649 675.20734 599.0 0.001669 441.10513 638.83374 561.0 0.001783 441.21384 573.02600 568.0 0.001761 441.32248 531.93286 520.0 0.001923 441.43112 517.21375 516.0 0.001938 441.53976 519.31097 537.0 0.001862 441.64841 531.30353 548.0 0.001825 441.75711 556.65112 587.0 0.001704 441.86575 598.65717 635.0 0.001575 441.97437 633.35278 577.0 0.001733 442.08298 596.77881 497.0 0.002012 442.19165 532.61462 469.0 0.002132 442.30026 505.83298 478.0 0.002092 442.40887 505.55630 463.0 0.002160 442.51746 517.85004 500.0 0.002000 442.62598 539.01654 538.0 0.001859 442.73462 548.62537 500.0 0.002000 442.84317 519.43323 454.0 0.002203 442.95169 493.03601 469.0 0.002132 443.06024 486.54977 484.0 0.002066 443.16873 486.97189 481.0 0.002079 443.27734 500.27716 546.0 0.001832 443.38568 521.55328 585.0 0.001709 443.49417 549.07141 598.0 0.001672 443.60257 555.24091 552.0 0.001812 443.71094 523.26996 483.0 0.002070 443.81931 501.38907 483.0 0.002070 443.92761 502.28580 531.0 0.001883 444.03595 515.54639 555.0 0.001802 444.14417 539.67493 635.0 0.001575 444.25241 575.79211 675.0 0.001481 444.36063 619.65448 718.0 0.001393 444.46872 691.38641 854.0 0.001171 444.57700 843.65356 1042.0 0.000960 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485.22183 549.0 0.001821 372.82425 497.50089 618.0 0.001618 372.90634 510.61557 619.0 0.001616 372.98856 520.26257 537.0 0.001862 373.07074 521.86383 514.0 0.001946 373.15320 513.22968 449.0 0.002227 373.23553 496.44031 421.0 0.002375 373.31802 476.23849 427.0 0.002342 373.40057 456.77332 377.0 0.002653 373.48309 440.29391 413.0 0.002421 373.56589 427.42078 394.0 0.002538 373.64859 418.11380 393.0 0.002545 373.73148 411.80396 402.0 0.002488 373.81436 408.00281 408.0 0.002451 373.89728 406.23969 432.0 0.002315 373.98038 405.99026 425.0 0.002353 374.06348 407.04553 418.0 0.002392 374.14676 408.98874 416.0 0.002404 374.23004 411.82672 427.0 0.002342 374.31323 415.28613 447.0 0.002237 374.39670 418.85336 456.0 0.002193 374.48019 421.71985 437.0 0.002288 374.56381 423.57669 429.0 0.002331 374.64740 425.02609 444.0 0.002252 374.73105 427.08734 428.0 0.002336 374.81488 430.32471 437.0 0.002288 374.89880 434.65405 452.0 0.002212 374.98273 439.35651 456.0 0.002193 375.06677 442.93188 442.0 0.002262 375.15076 444.03601 438.0 0.002283 375.23502 441.18817 438.0 0.002283 375.31927 434.47928 428.0 0.002336 375.40359 425.65421 405.0 0.002469 375.48807 416.71008 393.0 0.002545 375.57242 408.83740 389.0 0.002571 375.65704 402.54984 385.0 0.002597 375.74170 397.94955 404.0 0.002475 375.82642 394.88135 407.0 0.002457 375.91125 393.06790 387.0 0.002584 375.99609 392.23602 390.0 0.002564 376.08112 392.03494 372.0 0.002688 376.16611 392.23428 380.0 0.002632 376.25131 392.51520 354.0 0.002825 376.33655 392.66766 380.0 0.002632 376.42169 393.04205 399.0 0.002506 376.50717 393.67996 396.0 0.002525 376.59259 394.59412 390.0 0.002564 376.67819 395.67123 385.0 0.002597 376.76389 396.75882 382.0 0.002618 376.84949 397.78271 408.0 0.002451 376.93533 398.59171 391.0 0.002558 377.02118 398.82281 422.0 0.002370 377.10721 398.14862 433.0 0.002309 377.19324 396.63232 406.0 0.002463 377.27939 394.88007 383.0 0.002611 377.36563 393.16382 393.0 0.002545 377.45187 391.65244 371.0 0.002695 377.53839 390.50595 355.0 0.002817 377.62482 389.74722 389.0 0.002571 377.71130 389.40414 394.0 0.002538 377.79813 389.33627 397.0 0.002519 377.88474 389.63098 399.0 0.002506 377.97174 390.41046 386.0 0.002591 378.05869 391.81216 382.0 0.002618 378.14560 393.89160 426.0 0.002347 378.23279 396.62488 435.0 0.002299 378.31998 399.79773 413.0 0.002421 378.40732 402.96640 435.0 0.002299 378.49475 405.22760 409.0 0.002445 378.58212 405.88495 362.0 0.002762 378.66974 404.87274 383.0 0.002611 378.75739 402.85181 405.0 0.002469 378.84521 400.57629 397.0 0.002519 378.93314 398.50034 379.0 0.002639 379.02103 396.81940 385.0 0.002597 379.10910 395.58173 396.0 0.002525 379.19714 394.53830 414.0 0.002415 379.28549 393.80768 383.0 0.002611 379.37384 393.09183 375.0 0.002667 379.46222 392.44073 369.0 0.002710 379.55084 391.99655 371.0 0.002695 379.63943 391.88055 386.0 0.002591 379.72818 392.18494 404.0 0.002475 379.81702 393.00220 385.0 0.002597 379.90585 394.41791 399.0 0.002506 379.99496 396.49109 419.0 0.002387 380.08411 399.03564 431.0 0.002320 380.17334 401.99582 410.0 0.002439 380.26263 404.91824 383.0 0.002611 380.35208 407.35925 386.0 0.002591 380.44162 409.02441 379.0 0.002639 380.53122 409.97128 410.0 0.002439 380.62103 410.32626 410.0 0.002439 380.71082 410.06552 396.0 0.002525 380.80078 409.03653 418.0 0.002392 380.89084 407.30161 422.0 0.002370 380.98096 405.17865 407.0 0.002457 381.07135 403.01755 405.0 0.002469 381.16168 401.57382 414.0 0.002415 381.25204 400.97748 385.0 0.002597 381.34274 401.47760 391.0 0.002558 381.43341 403.14905 417.0 0.002398 381.52426 406.21127 413.0 0.002421 381.61508 410.67123 439.0 0.002278 381.70605 416.31879 456.0 0.002193 381.79727 422.59930 456.0 0.002193 381.88846 428.46484 483.0 0.002070 381.97983 432.54352 447.0 0.002237 382.07135 433.88843 450.0 0.002222 382.16278 432.44370 404.0 0.002475 382.25458 429.29221 388.0 0.002577 382.34637 425.72861 443.0 0.002257 382.43826 423.05771 408.0 0.002451 382.53030 421.68793 425.0 0.002353 382.62228 421.51328 424.0 0.002358 382.71466 421.86237 418.0 0.002392 382.80692 421.99542 417.0 0.002398 382.89954 421.40311 439.0 0.002278 382.99219 419.83035 424.0 0.002358 383.08475 417.24265 402.0 0.002488 383.17764 413.82416 374.0 0.002674 383.27060 410.09842 431.0 0.002320 383.36374 406.65878 375.0 0.002667 383.45688 403.89102 389.0 0.002571 383.55014 402.01849 398.0 0.002513 383.64355 400.96451 374.0 0.002674 383.73709 400.78717 401.0 0.002494 383.83087 401.52112 406.0 0.002463 383.92459 403.18970 416.0 0.002404 384.01840 405.73532 441.0 0.002268 384.11258 409.18600 427.0 0.002342 384.20667 413.35449 431.0 0.002320 384.30109 417.98752 466.0 0.002146 384.39542 422.56335 459.0 0.002179 384.48981 426.76782 454.0 0.002203 384.58463 430.68967 462.0 0.002165 384.67935 434.83438 461.0 0.002169 384.77429 439.75021 467.0 0.002141 384.86932 445.59915 472.0 0.002119 384.96439 451.67966 466.0 0.002146 385.05981 456.38876 474.0 0.002110 385.15509 457.92984 468.0 0.002137 385.25082 455.74838 451.0 0.002217 385.34650 451.03506 456.0 0.002193 385.44214 445.62930 467.0 0.002141 385.53818 440.73483 462.0 0.002165 385.63422 436.97888 461.0 0.002169 385.73056 434.47458 468.0 0.002137 385.82681 432.93524 443.0 0.002257 385.92319 431.66425 432.0 0.002315 386.01987 429.56870 420.0 0.002381 386.11655 426.11053 421.0 0.002375 386.21356 421.60486 414.0 0.002415 386.31061 416.92844 376.0 0.002660 386.40759 412.78494 402.0 0.002488 386.50494 409.49664 404.0 0.002475 386.60229 407.19928 401.0 0.002494 386.69998 406.00803 381.0 0.002625 386.79767 405.84720 364.0 0.002747 386.89542 406.81625 396.0 0.002525 386.99344 409.02634 409.0 0.002445 387.09155 412.55972 417.0 0.002398 387.18982 417.55396 428.0 0.002336 387.28833 424.01813 446.0 0.002242 387.38675 431.73972 475.0 0.002105 387.48547 440.16519 465.0 0.002151 387.58435 447.95007 439.0 0.002278 387.68329 453.58505 484.0 0.002066 387.78253 456.15292 466.0 0.002146 387.88165 455.98087 444.0 0.002252 387.98114 453.87350 487.0 0.002053 388.08063 450.35913 459.0 0.002179 388.18045 445.76965 421.0 0.002375 388.28024 440.77667 430.0 0.002326 388.38016 436.30469 446.0 0.002242 388.48038 432.80847 437.0 0.002288 388.58063 430.17218 405.0 0.002469 388.68121 428.07611 423.0 0.002364 388.78186 426.44293 438.0 0.002283 388.88245 425.48117 422.0 0.002370 388.98343 425.37787 415.0 0.002410 389.08441 426.07925 405.0 0.002469 389.18579 427.17838 411.0 0.002433 389.28714 428.00986 404.0 0.002475 389.38855 427.98596 417.0 0.002398 389.49030 427.04623 454.0 0.002203 389.59210 425.90714 431.0 0.002320 389.69412 425.34821 479.0 0.002088 389.79623 425.94492 437.0 0.002288 389.89847 427.87073 419.0 0.002387 390.00104 430.86343 459.0 0.002179 390.10358 434.24869 431.0 0.002320 390.20648 437.08438 440.0 0.002273 390.30945 438.65948 438.0 0.002283 390.41248 438.85431 419.0 0.002387 390.51578 438.25577 440.0 0.002273 390.61917 437.57153 440.0 0.002273 390.72281 437.05551 415.0 0.002410 390.82663 436.66971 412.0 0.002427 390.93048 436.34534 432.0 0.002315 391.03458 436.24811 441.0 0.002268 391.13876 436.65527 447.0 0.002237 391.24329 437.90060 453.0 0.002208 391.34790 440.15918 459.0 0.002179 391.45258 443.17694 460.0 0.002174 391.55750 446.23169 451.0 0.002217 391.66266 448.60703 458.0 0.002183 391.76788 450.09421 439.0 0.002278 391.87335 450.75925 437.0 0.002288 391.97891 450.76282 444.0 0.002252 392.08475 449.63245 459.0 0.002179 392.19058 447.01950 447.0 0.002237 392.29678 443.32513 429.0 0.002331 392.40308 439.40286 421.0 0.002375 392.50946 435.90244 420.0 0.002381 392.61621 432.98056 430.0 0.002326 392.72293 430.58289 409.0 0.002445 392.82996 428.67783 412.0 0.002427 392.93716 427.25089 379.0 0.002639 393.04440 426.01886 395.0 0.002532 393.15204 424.88614 412.0 0.002427 393.25967 424.05438 407.0 0.002457 393.36761 423.74274 420.0 0.002381 393.47571 424.26776 406.0 0.002463 393.58383 425.64581 427.0 0.002342 393.69235 427.67773 422.0 0.002370 393.80090 430.03232 432.0 0.002315 393.90979 432.25015 410.0 0.002439 394.01874 433.94067 385.0 0.002597 394.12784 435.29190 439.0 0.002278 394.23724 436.77451 447.0 0.002237 394.34665 438.87430 422.0 0.002370 394.45648 441.55594 432.0 0.002315 394.56641 444.62009 455.0 0.002198 394.67636 448.05264 470.0 0.002128 394.78668 451.56900 426.0 0.002347 394.89709 455.02740 466.0 0.002146 395.00787 458.15274 513.0 0.001949 395.11871 460.88406 516.0 0.001938 395.22952 463.24591 494.0 0.002024 395.34094 464.90421 457.0 0.002188 395.45224 465.17944 447.0 0.002237 395.56390 463.83472 475.0 0.002105 395.67578 461.48123 464.0 0.002155 395.78766 459.28320 451.0 0.002217 395.89993 458.19958 416.0 0.002404 396.01227 458.60239 436.0 0.002294 396.12491 460.00754 445.0 0.002247 396.23770 461.36560 464.0 0.002155 396.35059 461.74316 457.0 0.002188 396.46381 460.70258 433.0 0.002309 396.57712 458.84216 405.0 0.002469 396.69073 456.69858 410.0 0.002439 396.80457 454.30670 419.0 0.002387 396.91843 451.20056 428.0 0.002336 397.03265 447.04095 422.0 0.002370 397.14703 442.11755 416.0 0.002404 397.26166 437.27383 422.0 0.002370 397.37637 433.18732 424.0 0.002358 397.49127 430.20581 422.0 0.002370 397.60648 428.40027 450.0 0.002222 397.72189 427.68951 446.0 0.002242 397.83755 427.85846 426.0 0.002347 397.95331 428.59500 422.0 0.002370 398.06915 429.75598 420.0 0.002381 398.18555 431.22501 438.0 0.002283 398.30194 432.91827 449.0 0.002227 398.41858 434.66342 453.0 0.002208 398.53543 436.09726 450.0 0.002222 398.65234 436.91370 442.0 0.002262 398.76974 437.39789 444.0 0.002252 398.88712 438.10843 447.0 0.002237 399.00491 439.57733 446.0 0.002242 399.12280 442.08038 475.0 0.002105 399.24078 445.63120 444.0 0.002252 399.35928 449.74319 487.0 0.002053 399.47763 453.85040 484.0 0.002066 399.59653 457.23111 455.0 0.002198 399.71555 459.73193 453.0 0.002208 399.83459 461.34726 460.0 0.002174 399.95404 462.40341 440.0 0.002273 400.07358 463.58594 485.0 0.002062 400.19354 465.64355 507.0 0.001972 400.31363 469.30270 474.0 0.002110 400.43381 475.09995 479.0 0.002088 400.55429 483.12088 559.0 0.001789 400.67508 492.67645 561.0 0.001783 400.79599 502.05673 578.0 0.001730 400.91718 509.18491 572.0 0.001748 401.03845 511.86438 534.0 0.001873 401.16013 508.78085 476.0 0.002101 401.28192 500.38025 458.0 0.002183 401.40402 488.86499 496.0 0.002016 401.52637 476.85471 452.0 0.002212 401.64874 466.26840 415.0 0.002410 401.77158 458.08569 452.0 0.002212 401.89441 452.70166 455.0 0.002198 402.01776 449.91760 473.0 0.002114 402.14111 449.28717 479.0 0.002088 402.26465 450.01660 448.0 0.002232 402.38870 451.07040 442.0 0.002262 402.51270 451.54065 453.0 0.002208 402.63708 451.24545 461.0 0.002169 402.76166 450.55606 463.0 0.002160 402.88632 450.20197 459.0 0.002179 403.01141 450.48166 460.0 0.002174 403.13660 451.13831 480.0 0.002083 403.26224 451.91617 470.0 0.002128 403.38794 452.68652 455.0 0.002198 403.51376 453.47858 444.0 0.002252 403.64011 454.45767 480.0 0.002083 403.76645 455.88788 490.0 0.002041 403.89322 458.08914 481.0 0.002079 404.02008 461.25595 487.0 0.002053 404.14716 465.11316 498.0 0.002008 404.27460 468.96600 508.0 0.001969 404.40216 471.65701 487.0 0.002053 404.53015 472.19827 477.0 0.002096 404.65820 470.22296 464.0 0.002155 404.78638 466.23401 431.0 0.002320 404.91510 461.32999 426.0 0.002347 405.04385 456.87534 469.0 0.002132 405.17307 453.52423 457.0 0.002188 405.30231 451.40198 457.0 0.002188 405.43185 450.20853 460.0 0.002174 405.56161 449.36792 423.0 0.002364 405.69156 448.41031 418.0 0.002392 405.82199 447.05679 431.0 0.002320 405.95251 445.10059 418.0 0.002392 406.08319 442.59225 426.0 0.002347 406.21429 439.73843 442.0 0.002262 406.34549 436.99179 430.0 0.002326 406.47705 434.74625 417.0 0.002398 406.60889 433.23560 399.0 0.002506 406.74075 432.43146 408.0 0.002451 406.87314 432.23599 408.0 0.002451 407.00558 432.55203 426.0 0.002347 407.13834 433.17197 417.0 0.002398 407.27139 433.99380 441.0 0.002268 407.40454 434.98737 414.0 0.002415 407.53812 436.25928 456.0 0.002193 407.67178 437.95059 465.0 0.002151 407.80588 440.22406 462.0 0.002165 407.94019 442.89914 452.0 0.002212 408.07452 445.88312 446.0 0.002242 408.20944 449.03079 438.0 0.002283 408.34436 452.19724 463.0 0.002160 408.47974 455.34647 508.0 0.001969 408.61526 458.57312 466.0 0.002146 408.75098 461.76831 487.0 0.002053 408.88705 464.62482 459.0 0.002179 409.02335 466.64529 439.0 0.002278 409.15994 467.27316 459.0 0.002179 409.29678 466.41064 462.0 0.002165 409.43372 464.49786 437.0 0.002288 409.57120 462.30588 481.0 0.002079 409.70865 460.55084 483.0 0.002070 409.84662 459.76019 499.0 0.002004 409.98471 459.90665 458.0 0.002183 410.12299 460.44739 427.0 0.002342 410.26169 460.70404 436.0 0.002294 410.40048 459.71674 440.0 0.002273 410.53973 457.58649 425.0 0.002353 410.67920 454.98822 445.0 0.002247 410.81870 452.82535 441.0 0.002268 410.95868 451.51651 460.0 0.002174 411.09882 451.23761 469.0 0.002132 411.23935 451.77478 459.0 0.002179 411.38010 452.67615 424.0 0.002358 411.52103 453.18597 424.0 0.002358 411.66235 453.08542 444.0 0.002252 411.80380 452.83838 446.0 0.002242 411.94565 452.65991 447.0 0.002237 412.08768 452.94833 446.0 0.002242 412.22989 453.92554 454.0 0.002203 412.37250 455.75851 469.0 0.002132 412.51529 458.61511 475.0 0.002105 412.65848 462.68045 473.0 0.002114 412.80188 468.06104 475.0 0.002105 412.94537 474.69995 492.0 0.002033 413.08942 482.42816 482.0 0.002075 413.23349 490.88937 516.0 0.001938 413.37802 499.91592 529.0 0.001890 413.52274 509.17010 548.0 0.001825 413.66760 518.11938 590.0 0.001695 413.81299 525.63214 547.0 0.001828 413.95831 529.98492 518.0 0.001931 414.10422 529.74988 552.0 0.001812 414.25037 524.82373 533.0 0.001876 414.39648 516.34338 497.0 0.002012 414.54315 505.88730 460.0 0.002174 414.68997 495.20883 425.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 0 2 0 1 o 41692.24 38568.67 0.00 6.67854 14.95 0 2 0 2 o 41344.25 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1928.579 180.00 0.91837 0.02 0 4 10 2 o 6768.231 8622.885 180.00 0.91800 0.03 3 6 9 2 o 244.605 447.760 0.00 0.91766 0.01 9 7 2 1 o 13.058 17.501 0.00 0.91536 0.00 3 0 10 1 o 1.664 2.022 180.00 0.91510 0.00 7 10 3 2 o 535.339 577.804 0.00 0.91727 0.01 8 9 2 2 o 49.184 50.682 0.00 0.91701 0.00 3 10 7 1 o 3376.828 3686.962 0.00 0.91470 0.11 6 12 0 1 o 4348.924 4696.358 180.00 0.91440 0.07 9 5 4 2 o 3242.575 3276.837 180.00 0.91647 0.04 2 3 10 2 o 3653.668 3692.459 180.00 0.91647 0.05 1 4 10 1 o 483.048 455.189 0.00 0.91385 0.01 7 7 6 1 o 28.235 23.063 180.00 0.91331 0.00 9 7 2 2 o 19.948 17.501 0.00 0.91536 0.00 2 9 8 1 o 9409.134 8142.455 180.00 0.91315 0.26 9 3 5 1 o 7144.541 6345.141 180.00 0.91301 0.21 3 1 10 1 o 1264.039 1158.945 180.00 0.91296 0.03 3 0 10 2 o 2.181 2.022 180.00 0.91510 0.00 6 7 7 1 o 305.493 311.057 0.00 0.91249 0.01 10 2 3 1 o 2427.958 2498.037 0.00 0.91236 0.06 3 10 7 2 o 3597.702 3686.962 0.00 0.91470 0.06 4 5 9 1 o 1177.423 1220.563 0.00 0.91231 0.03 6 12 0 2 o 4367.171 4696.358 180.00 0.91440 0.03 0 12 6 1 o 5333.811 5883.141 0.00 0.91210 0.09 1 4 10 2 o 397.734 455.189 0.00 0.91385 0.00 7 7 6 2 o 30.328 23.063 180.00 0.91331 0.00 2 9 8 2 o 10436.547 8142.455 180.00 0.91315 0.15 9 3 5 2 o 8453.032 6345.141 180.00 0.91301 0.13 3 1 10 2 o 1491.741 1158.945 180.00 0.91296 0.02 2 7 9 1 o 334.733 273.788 0.00 0.91046 0.01 7 5 7 1 o 6021.453 4938.923 0.00 0.91025 0.19 6 7 7 2 o 373.138 311.057 0.00 0.91249 0.01 10 2 3 2 o 2939.481 2498.037 0.00 0.91236 0.04 3 14 1 1 o 816.745 631.285 0.00 0.91031 0.04 6 12 1 1 o 12539.114 10557.163 180.00 0.91024 0.39 4 5 9 2 o 1434.991 1220.563 0.00 0.91231 0.02 0 12 6 2 o 7004.123 5883.141 0.00 0.91210 0.06 1 14 3 1 o 487.990 388.383 180.00 0.90980 0.02 5 3 9 1 o 9411.716 9173.849 180.00 0.90946 0.27 2 7 9 2 o 272.555 273.788 0.00 0.91046 0.00 7 5 7 2 o 5198.706 4938.923 0.00 0.91025 0.08 1 12 6 1 o 6231.104 5977.435 0.00 0.90803 0.19 3 14 1 2 o 666.391 631.285 0.00 0.91031 0.02 6 12 1 2 o 11053.736 10557.163 180.00 0.91024 0.17 10 4 2 1 o 9445.770 9080.688 180.00 0.90769 0.26 1 14 3 2 o 401.950 388.383 180.00 0.90980 0.01 5 3 9 2 o 8859.742 9173.849 180.00 0.90946 0.12 0 11 7 1 o 997.195 1067.043 180.00 0.90695 0.01 3 2 10 1 o 7770.983 8094.887 180.00 0.90663 0.20 7 11 1 1 o 7207.109 6969.521 0.00 0.90593 0.20 1 12 6 2 o 5983.857 5977.435 0.00 0.90803 0.09 4 13 3 1 o 556.264 555.008 180.00 0.90580 0.02 10 4 2 2 o 8613.348 9080.688 180.00 0.90769 0.12 10 5 0 1 o 6512.313 6687.492 0.00 0.90524 0.08 3 13 4 1 o 268.069 279.961 0.00 0.90537 0.01 0 13 5 1 o 17252.563 17209.070 180.00 0.90481 0.26 0 11 7 2 o 1056.582 1067.043 180.00 0.90695 0.01 3 2 10 2 o 7453.150 8094.887 180.00 0.90663 0.10 5 11 5 1 o 6035.194 6507.581 180.00 0.90444 0.18 6 10 5 1 o 2312.651 2946.385 180.00 0.90402 0.06 7 11 1 2 o 4895.019 6969.521 0.00 0.90593 0.06 4 13 3 2 o 366.412 555.008 180.00 0.90580 0.01 8 8 4 1 o 26.474 32.818 180.00 0.90330 0.00 5 10 6 1 o 358.027 491.319 0.00 0.90334 0.01 10 5 0 2 o 5383.100 6687.492 0.00 0.90524 0.03 8 5 6 1 o 3269.053 4295.813 0.00 0.90301 0.09 3 13 4 2 o 219.768 279.961 0.00 0.90537 0.00 1 11 7 1 o 151.526 192.347 0.00 0.90295 0.00 0 13 5 2 o 15634.220 17209.070 180.00 0.90481 0.11 5 13 1 1 o 3724.254 3705.849 180.00 0.90231 0.13 5 11 5 2 o 6711.646 6507.581 180.00 0.90444 0.10 10 3 3 1 o 12635.838 12378.342 0.00 0.90190 0.34 6 10 5 2 o 2912.318 2946.385 180.00 0.90402 0.04 2 4 10 1 o 967.445 1016.032 0.00 0.90173 0.04 6 5 8 1 o 8383.583 10229.999 180.00 0.90129 0.22 10 5 1 1 o 2122.371 2615.600 0.00 0.90120 0.05 7 0 8 1 o 902.250 1147.704 0.00 0.90118 0.01 8 8 4 2 o 27.563 32.818 180.00 0.90330 0.00 5 10 6 2 o 388.221 491.319 0.00 0.90334 0.01 8 5 6 2 o 3211.690 4295.813 0.00 0.90301 0.05 1 13 5 1 o 5067.874 6660.106 180.00 0.90083 0.15 1 11 7 2 o 149.719 192.347 0.00 0.90295 0.00 4 8 8 1 o 707.711 737.592 180.00 0.90036 0.01 8 1 7 1 o 215.144 208.154 180.00 0.90005 0.01 5 13 1 2 o 3817.800 3705.849 180.00 0.90231 0.07 10 3 3 2 o 13688.887 12378.342 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0.89046 0.32 5 9 7 1 o 11662.423 10872.342 180.00 0.89032 0.37 10 0 4 2 o 24317.551 23272.449 180.00 0.89239 0.17