#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:30:34 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1272 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000053.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000053
loop_
_publ_author_name
'Zhou, Yongkai'
'Adams, Stefan'
'Rao, R. Prasada'
'Edwards, Doreen D.'
'Neiman, Arkady'
'Pestereva, N.'
_publ_section_title
;
 Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3
;
_journal_issue                   20
_journal_name_full               'Chemistry of Materials'
_journal_page_first              6335
_journal_page_last               6345
_journal_paper_doi               10.1021/cm800466y
_journal_volume                  20
_journal_year                    2008
_chemical_formula_moiety         ' Sc2(WO4)3 '
_chemical_formula_sum            'O12 Sc2 W3'
_chemical_formula_weight         833.45
_chemical_melting_point          ' 1913K '
_chemical_name_common            ' Scandium Tungstate '
_chemical_name_systematic        ' Scandium Tungstate '
_space_group_IT_number           60
_space_group_name_Hall           '-P 2a 2n'
_space_group_name_H-M_alt        'P n c a'
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P n c a'
_audit_creation_date             2008-01-25T12:03
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2008-01-25T12:03  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   9.62166(6)
_cell_length_b                   13.35709(8)
_cell_length_c                   9.54792(6)
_cell_measurement_temperature    1150
_cell_volume                     1227.074(13)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.68
_diffrn_radiation_probe          x-ray
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id
2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.017
_pd_meas_2theta_range_max        119.9874
_pd_meas_2theta_range_min        10.0144
_pd_meas_number_of_points        6470
_pd_proc_2theta_range_inc        0.017
_pd_proc_2theta_range_max        119.9874
_pd_proc_2theta_range_min        10.0144
_pd_proc_info_datetime           2008-01-25T12:31:36
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    391.716     2:   -17.2727     3:   -17.5763     4:    60.8251    
      5:   -7.69767     6:    10.7459     7:   -12.1459     8:    5.44036    
      9:    10.5752    10:   -24.9005    11:    20.9706    12:   -5.99013    
;
_pd_proc_ls_peak_cutoff          0.00250
_pd_proc_ls_pref_orient_corr
;   March-Dollase
 AXIS  1 Ratio=   0.95556  h= 0.000  k= 1.000  l= 0.000
 Prefered orientation correction range: Min=   0.93410, Max=   1.14609
;
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =    8.967 #2(GV)   =   -7.536 #3(GW)   =    2.655
 #4(GP)   =    0.000 #5(LX)   =    0.727 #6(LY)   =    5.405
 #7(S/L)  =   0.0316 #8(H/L)  =   0.0250
 #9(trns) =     0.00 #10(shft)= -17.8308
 #11(stec)=     0.00 #12(ptec)=     0.00 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0025 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0490
_pd_proc_ls_prof_wR_expected     0.0365
_pd_proc_ls_prof_wR_factor       0.0639
_pd_proc_number_of_points        6470
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.85
_refine_ls_matrix_type           full
_refine_ls_number_parameters     51
_refine_ls_number_restraints     0
_refine_ls_R_Fsqd_factor         0.07284
_refine_ls_shift/su_max          0.03
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        0.890
_reflns_d_resolution_low         6.679
_reflns_limit_h_max              10
_reflns_limit_h_min              0
_reflns_limit_k_max              15
_reflns_limit_k_min              0
_reflns_limit_l_max              10
_reflns_limit_l_min              0
_reflns_number_total             1823
_cod_data_source_file            cm800466y_si_024.cif
_cod_data_source_block           T1150K
_cod_original_cell_volume        1227.073(14)
_cod_database_code               4000053
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x+1/2,+y+1/2,+z+1/2
3 +x,-y+1/2,+z+1/2
4 -x+1/2,-y,+z
-1 -x,-y,-z
-2 +x+1/2,-y+1/2,-z+1/2
-3 -x,+y+1/2,-z+1/2
-4 +x+1/2,+y,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Sc Sc1 0.4712(4) 0.38253(26) 0.2469(5) 1.0 Uiso 0.0284(12) 8
W W1 0.25 0.0 0.47091(17) 1.0 Uiso 0.0335(4) 4
W W2 0.11236(12) 0.35634(9) 0.39043(12) 1.0 Uiso 0.0335(4) 8
O O1 0.0937(14) 0.1277(10) 0.0671(14) 1.0 Uiso 0.0776(22) 8
O O2 0.1529(14) 0.0779(9) 0.3756(15) 1.0 Uiso 0.0776(22) 8
O O3 0.0034(14) 0.2635(11) 0.3131(13) 1.0 Uiso 0.0776(22) 8
O O4 0.3351(14) 0.4063(9) 0.0740(14) 1.0 Uiso 0.0776(22) 8
O O5 0.0512(13) 0.4734(10) 0.3212(14) 1.0 Uiso 0.0776(22) 8
O O6 0.2921(15) 0.3481(10) 0.3393(14) 1.0 Uiso 0.0776(22) 8
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800
51.3531 1.33290 International_Tables_Vol_C
W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982
57.0560 9.88750 International_Tables_Vol_C
O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_diffrn_radiation_wavelength
_diffrn_radiation_wavelength_wt
_diffrn_radiation_type
_diffrn_radiation_wavelength_id
1.540500 1.000 K\a~1~ 1
1.544300 0.000 K\a~2~ 2
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sc1 O2 91.1(5) -2_666 . -2_666 N
O1 Sc1 O3 95.0(5) -2_666 . -2_666 N
O1 Sc1 O4 173.1(6) -2_666 . 1_555 N
O1 Sc1 O5 80.3(5) -2_666 . 4_565 N
O1 Sc1 O6 95.4(6) -2_666 . 1_555 N
O2 Sc1 O3 87.7(6) -2_666 . -2_666 N
O2 Sc1 O4 92.4(6) -2_666 . 1_555 N
O2 Sc1 O5 92.4(5) -2_666 . 4_565 N
O2 Sc1 O6 173.5(6) -2_666 . 1_555 N
O3 Sc1 O4 91.0(5) -2_666 . 1_555 N
O3 Sc1 O5 175.3(6) -2_666 . 4_565 N
O3 Sc1 O6 92.0(5) -2_666 . 1_555 N
O4 Sc1 O5 93.6(5) 1_555 . 4_565 N
O4 Sc1 O6 81.1(5) 1_555 . 1_555 N
O5 Sc1 O6 88.4(5) 4_565 . 1_555 N
O2 W1 O2 113.9(10) 1_555 . 4_555 N
O2 W1 O4 118.7(6) 1_555 . 2_545 N
O2 W1 O4 96.9(6) 1_555 . 3_555 N
O2 W1 O4 96.9(6) 4_555 . 2_545 N
O2 W1 O4 118.7(6) 4_555 . 3_555 N
O4 W1 O4 113.3(8) 2_545 . 3_555 N
O1 W2 O3 115.7(6) 3_555 . 1_555 N
O1 W2 O5 102.7(6) 3_555 . 1_555 N
O1 W2 O6 112.1(6) 3_555 . 1_555 N
O3 W2 O5 105.1(7) 1_555 . 1_555 N
O3 W2 O6 114.2(6) 1_555 . 1_555 N
O5 W2 O6 105.5(6) 1_555 . 1_555 N
Sc1 O1 W2 152.4(8) -2_466 . 3_554 N
Sc1 O2 W1 153.8(8) -2_555 . 1_555 N
Sc1 O3 W2 149.7(8) -2_466 . 1_555 N
Sc1 O4 W1 144.2(8) 1_555 . 2_554 N
Sc1 O5 W2 166.6(8) 4_565 . 1_555 N
Sc1 O6 W2 159.7(8) 1_555 . 1_555 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sc1 O1 2.136(14) . -2_555 N
Sc1 O2 2.168(14) . -2_555 N
Sc1 O3 2.056(14) . -2_555 N
Sc1 O4 2.130(13) . 1_555 N
Sc1 O5 2.063(13) . 4_565 N
Sc1 O6 1.990(14) . 1_555 N
W1 O2 1.669(13) . 1_555 N
W1 O2 1.669(13) . 4_555 N
W1 O4 1.791(12) . 2_545 N
W1 O4 1.791(12) . 3_555 N
W2 O1 1.710(13) . 3_555 N
W2 O3 1.784(13) . 1_555 N
W2 O5 1.796(13) . 1_555 N
W2 O6 1.800(15) . 1_555 N
O1 Sc1 2.136(14) . -2_455 N
O1 W2 1.710(13) . 3_554 N
O2 Sc1 2.168(14) . -2_455 N
O2 W1 1.669(13) . 1_555 N
O3 Sc1 2.056(14) . -2_455 N
O3 W2 1.784(13) . 1_555 N
O4 Sc1 2.130(13) . 1_555 N
O4 W1 1.791(12) . 2_554 N
O5 Sc1 2.063(13) . 4_565 N
O5 W2 1.796(13) . 1_555 N
O6 Sc1 1.990(14) . 1_555 N
O6 W2 1.800(15) . 1_555 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
300.0 0.0 628.72083 .
274.0 0.0 625.02985 .
277.0 0.0 621.36749 .
314.0 0.0 617.73352 .
315.0 0.0 614.12744 .
294.0 0.0 610.54999 .
305.0 0.0 607.00031 .
301.0 0.0 603.47821 .
289.0 0.0 599.98419 .
311.0 0.0 596.51703 .
304.0 0.0 593.07788 .
286.0 0.0 589.66559 .
311.0 0.0 586.28064 .
295.0 0.0 582.92261 .
323.0 0.0 579.59143 .
319.0 0.0 576.28693 .
300.0 0.0 573.00897 .
269.0 0.0 569.75708 .
260.0 0.0 566.53217 .
263.0 0.0 563.33325 .
283.0 0.0 560.16034 .
270.0 0.0 557.01318 .
294.0 0.0 553.89154 .
305.0 0.0 550.79596 .
288.0 0.0 547.72595 .
301.0 0.0 544.68109 .
294.0 0.0 541.66144 .
278.0 0.0 538.66687 .
295.0 0.0 535.69727 .
307.0 0.0 532.75299 .
295.0 0.0 529.83282 .
297.0 0.0 526.93750 .
312.0 0.0 524.06641 .
295.0 0.0 521.22009 .
302.0 0.0 518.39795 .
310.0 0.0 515.59967 .
311.0 0.0 512.82544 .
319.0 0.0 510.07480 .
287.0 0.0 507.34818 .
289.0 0.0 504.64520 .
315.0 0.0 501.96552 .
300.0 0.0 499.30917 .
313.0 0.0 496.67584 .
313.0 0.0 494.06589 .
316.0 0.0 491.47910 .
312.0 0.0 488.91486 .
327.0 0.0 486.37335 .
321.0 0.0 483.85431 .
282.0 0.0 481.35812 .
293.0 0.0 478.88419 .
294.0 0.0 476.43259 .
326.0 0.0 474.00281 .
333.0 0.0 471.59509 .
301.0 0.0 469.20938 .
284.0 0.0 466.84558 .
313.0 0.0 464.50330 .
307.0 0.0 462.18253 .
300.0 0.0 459.88306 .
312.0 0.0 457.60519 .
325.0 0.0 455.34857 .
303.0 0.0 453.11285 .
295.0 0.0 450.89792 .
303.0 0.0 448.70392 .
293.0 0.0 446.53079 .
263.0 0.0 444.37836 .
313.0 0.0 442.24640 .
287.0 0.0 440.13467 .
323.0 0.0 438.04327 .
315.0 0.0 435.97208 .
309.0 0.0 433.92108 .
292.0 0.0 431.89005 .
306.0 0.0 429.87863 .
316.0 0.0 427.88702 .
306.0 0.0 425.91507 .
298.0 0.0 423.96280 .
288.0 0.0 422.02975 .
295.0 0.0 420.11594 .
320.0 0.0 418.22150 .
318.0 0.0 416.34595 .
331.0 0.0 414.48953 .
357.0 0.0 412.65207 .
332.0 0.0 410.83322 .
300.0 0.0 409.03293 .
314.0 0.0 407.25131 .
325.0 0.0 405.48837 .
308.0 0.0 403.74353 .
301.0 0.0 402.01694 .
329.0 0.0 400.30856 .
322.0 0.0 398.61813 .
321.0 0.0 396.94574 .
337.0 0.0 395.29117 .
343.0 0.0 393.65421 .
333.0 0.0 392.03488 .
315.0 0.0 390.43317 .
309.0 0.0 388.84885 .
322.0 0.0 387.28204 .
318.0 0.0 385.73215 .
296.0 0.0 384.19949 .
301.0 0.0 382.68393 .
315.0 0.0 381.18527 .
326.0 0.0 379.70352 .
310.0 0.0 378.23831 .
309.0 0.0 376.78979 .
323.0 0.0 375.35797 .
317.0 0.0 373.94241 .
291.0 0.0 372.54340 .
302.0 0.0 371.16031 .
277.0 0.0 369.79367 .
290.0 0.0 368.44299 .
312.0 0.0 367.10822 .
364.0 0.0 365.78943 .
304.0 0.0 364.48627 .
318.0 0.0 363.19888 .
332.0 0.0 361.92719 .
334.0 0.0 360.67081 .
311.0 0.0 359.42987 .
307.0 0.0 358.20432 .
311.0 0.003215 356.99387 356.99951
303.0 0.003300 355.79861 355.80432
309.0 0.003236 354.61838 354.62402
314.0 0.003185 353.45313 353.45868
315.0 0.003175 352.30273 352.30826
273.0 0.00366 351.16696 351.17242
300.0 0.003333 350.04602 350.05142
343.0 0.002915 348.93967 348.94498
333.0 0.003003 347.84784 347.85297
306.0 0.003268 346.77026 346.77542
323.0 0.003096 345.70697 345.71216
334.0 0.002994 344.65808 344.66321
311.0 0.003215 343.62329 343.62830
309.0 0.003236 342.60260 342.60764
297.0 0.003367 341.59579 341.60080
303.0 0.003300 340.60284 340.60779
306.0 0.003268 339.62375 339.62863
316.0 0.003165 338.65839 338.66321
298.0 0.003356 337.70667 337.71136
298.0 0.003356 336.76849 336.77319
301.0 0.003322 335.84369 335.84830
295.0 0.003390 334.93231 334.93692
312.0 0.003205 334.03430 334.03879
302.0 0.003311 333.14941 333.15387
289.0 0.003460 332.27768 332.28210
307.0 0.003257 331.41882 331.42322
315.0 0.003175 330.57318 330.57739
317.0 0.003155 329.74026 329.74451
303.0 0.003300 328.92014 328.92441
285.0 0.00351 328.11276 328.11694
303.0 0.003300 327.31793 327.32211
321.0 0.003115 326.53583 326.53983
302.0 0.003311 325.76605 325.77014
316.0 0.003165 325.00867 325.01270
343.0 0.002915 324.26370 324.26764
326.0 0.003067 323.53085 323.53473
300.0 0.003333 322.81021 322.81406
308.0 0.003247 322.10162 322.10544
318.0 0.003145 321.40506 321.40881
303.0 0.003300 320.72040 320.72412
300.0 0.003333 320.04745 320.05115
313.0 0.003195 319.38644 319.39017
330.0 0.003030 318.73706 318.74069
298.0 0.003356 318.09927 318.10278
317.0 0.003155 317.47293 317.47653
314.0 0.003185 316.85812 316.86169
340.0 0.002941 316.25473 316.25821
349.0 0.002865 315.66263 315.66602
338.0 0.002959 315.08173 315.08514
352.0 0.002841 314.51196 314.51532
321.0 0.003115 313.95325 313.95657
351.0 0.002849 313.40564 317.15842
318.0 0.003145 312.86884 316.95621
348.0 0.002874 312.34296 318.69366
370.0 0.002703 311.82782 318.80331
362.0 0.002762 311.32343 319.04092
346.0 0.002890 310.82965 319.44720
347.0 0.002882 310.34650 320.09070
381.0 0.002625 309.87384 321.13870
365.0 0.002740 309.41153 323.27301
406.0 0.002463 308.95956 328.61465
400.0 0.002500 308.51785 339.90735
390.0 0.002564 308.08643 357.65182
410.0 0.002439 307.66513 380.94745
442.0 0.002262 307.25381 408.58920
455.0 0.002198 306.85254 439.47409
435.0 0.002299 306.46124 473.33273
491.0 0.002037 306.07974 510.39185
529.0 0.001890 305.70810 551.06256
551.0 0.001815 305.34613 595.92792
590.0 0.001695 304.99371 645.69055
646.0 0.001548 304.65100 701.23376
676.0 0.001479 304.31781 763.78314
751.0 0.001332 303.99405 834.85522
879.0 0.001138 303.67963 916.59308
981.0 0.001019 303.37451 1011.90192
1068.0 0.000936 303.07864 1125.00500
1254.0 0.000797 302.79202 1262.26001
1532.0 0.000653 302.51450 1433.90906
1810.0 0.000552 302.24597 1658.07056
2255.0 0.000443 301.98648 1973.05920
2922.0 0.0003422 301.73590 2473.12671
3660.0 0.0002732 301.49417 3249.82080
3959.0 0.0002526 301.26123 3790.35254
3293.0 0.0003037 301.03705 3146.52002
2202.0 0.000454 300.82141 2176.04297
1311.0 0.000763 300.61444 1265.11316
710.0 0.001408 300.41599 654.17969
439.0 0.002278 300.22607 447.03110
384.0 0.002604 300.04449 390.41238
381.0 0.002625 299.87128 365.07343
354.0 0.002825 299.70639 349.46155
341.0 0.002933 299.54965 338.92169
365.0 0.002740 299.40103 331.41989
358.0 0.002793 299.26065 325.86227
367.0 0.002725 299.12817 321.61319
346.0 0.002890 299.00372 318.28094
332.0 0.003012 298.88730 315.61197
342.0 0.002924 298.77856 313.43665
323.0 0.003096 298.67767 311.63696
319.0 0.003135 298.58447 310.12955
302.0 0.003311 298.49902 308.85342
345.0 0.002899 298.42120 307.76303
366.0 0.002732 298.35086 306.82404
336.0 0.002976 298.28802 306.01004
328.0 0.003049 298.23267 300.85608
321.0 0.003115 298.18472 300.58432
357.0 0.002801 298.14407 298.14609
390.0 0.002564 298.11063 298.11267
323.0 0.003096 298.08447 298.08643
337.0 0.002967 298.06543 298.06738
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1401.0 0.000714 461.60971 1396.00220
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480.0 0.002083 463.88953 490.76096
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483.0 0.002070 464.27698 507.33124
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532.0 0.001880 464.43018 555.23145
557.0 0.001795 464.50644 600.58789
574.0 0.001742 464.58243 638.27356
534.0 0.001873 464.65817 606.74957
523.0 0.001912 464.73367 557.97894
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624.0 0.001603 464.95862 630.35034
697.0 0.001435 465.03314 696.00964
729.0 0.001372 465.10739 711.49445
667.0 0.001499 465.18134 658.68988
583.0 0.001715 465.25507 618.21021
579.0 0.001727 465.32852 634.07391
682.0 0.001466 465.40179 706.48718
783.0 0.001277 465.47470 809.37720
844.0 0.001185 465.54736 859.43878
821.0 0.001218 465.61981 770.79431
724.0 0.001381 465.69193 674.27698
665.0 0.001504 465.76379 660.87439
734.0 0.001362 465.83545 735.07941
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849.0 0.001178 466.25977 873.41486
752.0 0.001330 466.32956 795.65900
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1017.0 0.000983 466.46838 1089.04395
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1535.0 0.000651 466.67450 1567.84204
1145.0 0.000873 466.74271 1147.12708
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1126.0 0.000888 466.87830 1086.52490
1206.0 0.000829 466.94562 1136.26904
1020.0 0.000980 467.01263 1029.02515
974.0 0.001027 467.07953 975.37354
927.0 0.001079 467.14609 937.28558
823.0 0.001215 467.21228 796.65356
703.0 0.001422 467.27823 717.60706
752.0 0.001330 467.34402 730.45575
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734.0 0.001362 467.47470 704.38019
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534.0 0.001873 467.60410 552.76709
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544.0 0.001838 467.73257 533.86060
566.0 0.001767 467.79633 543.33728
618.0 0.001618 467.85977 569.77905
658.0 0.001520 467.92300 628.89270
825.0 0.001212 467.98593 731.09723
1041.0 0.000961 468.04865 908.39697
1313.0 0.000762 468.11099 1120.00549
1398.0 0.000715 468.17310 1182.26453
1098.0 0.000911 468.23486 919.08545
766.0 0.001305 468.29639 694.65900
602.0 0.001661 468.35764 618.17780
597.0 0.001675 468.41858 622.13586
688.0 0.001453 468.47922 674.28827
841.0 0.001189 468.53964 766.26849
958.0 0.001044 468.59967 849.30328
917.0 0.001091 468.65948 786.58600
726.0 0.001377 468.71899 639.99512
570.0 0.001754 468.77823 562.26337
509.0 0.001965 468.83710 536.90411
514.0 0.001946 468.89575 536.02106
554.0 0.001805 468.95419 553.82397
560.0 0.001786 469.01221 592.22528
612.0 0.001634 469.06995 664.49036
722.0 0.001385 469.12744 762.70740
727.0 0.001376 469.18463 828.06830
693.0 0.001443 469.24158 737.59741
606.0 0.001650 469.29816 620.66125
552.0 0.001812 469.35449 578.22772
565.0 0.001770 469.41049 589.08032
624.0 0.001603 469.46625 642.23566
732.0 0.001366 469.52173 751.00214
890.0 0.001124 469.57678 915.21771
1025.0 0.000976 469.63162 1101.96277
1171.0 0.000854 469.68613 1224.00562
1118.0 0.000894 469.74048 1121.64783
785.0 0.001274 469.79437 826.61920
604.0 0.001656 469.84805 657.26807
615.0 0.001626 469.90143 610.56866
579.0 0.001727 469.95441 625.06207
608.0 0.001645 470.00717 686.02655
689.0 0.001451 470.05963 777.62115
805.0 0.001242 470.11182 835.70087
777.0 0.001287 470.16364 736.44391
608.0 0.001645 470.21521 608.81183
497.0 0.002012 470.26645 549.87921
546.0 0.001832 470.31747 530.22955
507.0 0.001972 470.36810 527.45941
509.0 0.001965 470.41846 536.54272
547.0 0.001828 470.46844 558.92987
600.0 0.001667 470.51816 600.90985
694.0 0.001441 470.56766 659.60706
689.0 0.001451 470.61682 703.36334
684.0 0.001462 470.66559 671.13531
638.0 0.001567 470.71417 643.91425
734.0 0.001362 470.76236 689.44702
817.0 0.001224 470.81030 812.62152
1061.0 0.000943 470.85788 1006.42682
1237.0 0.000808 470.90521 1181.26843
1156.0 0.000865 470.95224 1091.98511
885.0 0.001130 470.99887 872.29053
763.0 0.001311 471.04523 762.41516
789.0 0.001267 471.09140 788.89624
975.0 0.001026 471.13712 936.07745
1231.0 0.000812 471.18259 1166.32349
1373.0 0.000728 471.22766 1323.94983
1218.0 0.000821 471.27249 1165.14087
879.0 0.001138 471.31708 863.51343
693.0 0.001443 471.36133 680.51324
631.0 0.001585 471.40521 628.87976
606.0 0.001650 471.44879 641.96643
659.0 0.001517 471.49207 701.08771
778.0 0.001285 471.53503 771.84882
783.0 0.001277 471.57773 758.08936
654.0 0.001529 471.62003 638.32153
541.0 0.001848 471.66211 555.89288
507.0 0.001972 471.70386 521.98657
487.0 0.002053 471.74521 509.39734
473.0 0.002114 471.78629 502.24786
488.0 0.002049 471.82709 497.91254
479.0 0.002088 471.86755 495.14932
474.0 0.002110 471.90775 493.39050
495.0 0.002020 471.94754 492.02670
487.0 0.002053 471.98709 491.53470
488.0 0.002049 472.02628 494.44052
497.0 0.002012 472.06522 495.01129
469.0 0.002132 472.10382 496.02130
475.0 0.002105 472.14206 497.51074
500.0 0.002000 472.17999 498.48526
464.0 0.002155 472.21759 501.28897
485.0 0.002062 472.25491 505.99731
518.0 0.001931 472.29190 510.98785
477.0 0.002096 472.32864 519.20081
516.0 0.001938 472.36493 528.64447
533.0 0.001876 472.40094 542.30640
534.0 0.001873 472.43668 564.85187
635.0 0.001575 472.47205 601.93384
700.0 0.001429 472.50720 683.12604
856.0 0.001168 472.54190 849.99811
1024.0 0.000977 472.57639 1112.07458
1453.0 0.000688 472.61050 1557.49646
1889.0 0.000529 472.64429 2017.63757
1963.0 0.000509 472.67776 1953.52722
1289.0 0.000776 472.71094 1314.82422
900.0 0.001111 472.74377 908.83453
730.0 0.001370 472.77628 788.97528
778.0 0.001285 472.80850 820.81055
888.0 0.001126 472.84039 936.96747
1107.0 0.000903 472.87192 1168.89014
1272.0 0.000786 472.90317 1364.07629
1248.0 0.000801 472.93411 1260.04871
985.0 0.001015 472.96463 969.63824
918.0 0.001089 472.99490 862.05902
998.0 0.001002 473.02484 952.78308
1200.0 0.000833 473.05444 1206.89209
1639.0 0.000610 473.08377 1641.11658
2337.0 0.000428 473.11273 2263.34692
2614.0 0.000383 473.14142 2474.07007
1974.0 0.000507 473.16974 1852.35303
1339.0 0.000747 473.19769 1308.34387
1183.0 0.000845 473.22537 1199.30859
1354.0 0.000739 473.25275 1409.42859
1663.0 0.000601 473.27969 1722.59497
1900.0 0.000526 473.30652 1899.95789
1994.0 0.000502 473.33279 1974.33215
1952.0 0.000512 473.35883 1970.34351
1793.0 0.000558 473.38458 1791.03821
1695.0 0.000590 473.41003 1698.55884
1468.0 0.000681 473.43509 1494.68542
1235.0 0.000810 473.45981 1253.67603
1165.0 0.000858 473.48425 1169.93713
1096.0 0.000912 473.50836 1086.31458
1018.0 0.000982 473.53217 1034.94324
1163.0 0.000860 473.55554 1147.66504
1519.0 0.000658 473.57867 1455.65723
1753.0 0.000570 473.60147 1708.80383
1575.0 0.000635 473.62390 1526.12024
1182.0 0.000846 473.64603 1114.62671
1024.0 0.000977 473.66782 961.59186
1114.0 0.000898 473.68936 1064.10632
1371.0 0.000729 473.71045 1349.45984
2039.0 0.000490 473.73126 1867.27136
2582.0 0.000387 473.75177 2323.58496
2234.0 0.000448 473.77194 2128.50293
1559.0 0.000641 473.79175 1450.79919
1062.0 0.000942 473.81134 990.59528
835.0 0.001198 473.83047 832.73926
890.0 0.001124 473.84933 847.00562
977.0 0.001024 473.86786 966.91650
1172.0 0.000853 473.88608 1205.88782
1459.0 0.000685 473.90396 1379.97107
1267.0 0.000789 473.92142 1206.17786
882.0 0.001134 473.93869 866.77496
648.0 0.001543 473.95557 680.01044
609.0 0.001642 473.97205 613.42621
501.0 0.001996 473.98834 592.86938
572.0 0.001748 474.00427 583.69385
541.0 0.001848 474.01978 572.55487
591.0 0.001692 474.03503 569.00543
550.0 0.001818 474.04993 561.00854
519.0 0.001927 474.06448 537.90851
567.0 0.001764 474.07874 520.63367
516.0 0.001938 474.09268 515.43561
507.0 0.001972 474.10623 515.78979
489.0 0.002045 474.11945 515.99774
477.0 0.002096 474.13242 508.28006
540.0 0.001852 474.14502 500.70880
503.0 0.001988 474.15723 498.41498
552.0 0.001812 474.16913 497.81711
506.0 0.001976 474.18082 498.10141
496.0 0.002016 474.19208 499.32300
525.0 0.001905 474.20300 501.37662
521.0 0.001919 474.21365 506.36353
526.0 0.001901 474.22397 510.07675
502.0 0.001992 474.23392 519.56860
542.0 0.001845 474.24350 532.85217
561.0 0.001783 474.25281 542.18500
535.0 0.001869 474.26178 543.01031
553.0 0.001808 474.27036 550.53418
592.0 0.001689 474.27869 574.24878
654.0 0.001529 474.28662 630.04889
788.0 0.001269 474.29431 746.00903
973.0 0.001028 474.30164 940.05640
1330.0 0.000752 474.30856 1256.41138
1680.0 0.000595 474.31519 1545.92847
1582.0 0.000632 474.32150 1432.36316
1121.0 0.000892 474.32751 1008.11029
775.0 0.001290 474.33322 765.00116
694.0 0.001441 474.33850 695.93793
702.0 0.001425 474.34354 720.82581
791.0 0.001264 474.34821 808.87640
987.0 0.001013 474.35251 974.61993
1197.0 0.000835 474.35648 1165.44177
1277.0 0.000783 474.36020 1227.85181
1264.0 0.000791 474.36356 1233.24866
1442.0 0.000693 474.36658 1449.83289
1822.0 0.000549 474.36923 1921.13354
1968.0 0.000508 474.37158 2145.02881
1597.0 0.000626 474.37363 1659.16296
1095.0 0.000913 474.37531 1102.95166
883.0 0.001133 474.37662 874.93652
851.0 0.001175 474.37769 861.40527
975.0 0.001026 474.37842 964.55487
1134.0 0.000882 474.37878 1126.26819
1400.0 0.000714 474.37885 1378.54431
1545.0 0.000647 474.37851 1567.71521
1495.0 0.000669 474.37793 1455.54175
1245.0 0.000803 474.37701 1214.91797
1041.0 0.000961 474.37567 1027.51990
1053.0 0.000950 474.37402 1002.13409
1172.0 0.000853 474.37213 1086.88501
1118.0 0.000894 474.36987 1057.44885
864.0 0.001157 474.36731 868.88843
743.0 0.001346 474.36432 761.53461
754.0 0.001326 474.36108 762.97565
824.0 0.001214 474.35751 782.33337
714.0 0.001401 474.35358 775.78693
825.0 0.001212 474.34933 818.11859
904.0 0.001106 474.34482 938.82660
1113.0 0.000898 474.33987 1016.53387
886.0 0.001129 474.33466 906.08417
691.0 0.001447 474.32907 719.65802
589.0 0.001698 474.32321 617.28772
576.0 0.001736 474.31699 582.41302
567.0 0.001764 474.31052 582.68195
588.0 0.001701 474.30362 606.19080
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425.0 . . .
