#------------------------------------------------------------------------------ #$Date: 2025-07-01 14:29:40 +0300 (Tue, 01 Jul 2025) $ #$Revision: 1267 $ #$URL: svn://localhost/testcod/cif/4/00/00/4000048.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4000048 loop_ _publ_author_name 'Zhou, Yongkai' 'Adams, Stefan' 'Rao, R. Prasada' 'Edwards, Doreen D.' 'Neiman, Arkady' 'Pestereva, N.' _publ_section_title ; Charge Transport by Polyatomic Anion Diffusion in Sc2(WO4)3 ; _journal_issue 20 _journal_name_full 'Chemistry of Materials' _journal_page_first 6335 _journal_page_last 6345 _journal_paper_doi 10.1021/cm800466y _journal_volume 20 _journal_year 2008 _chemical_formula_moiety ' Sc2(WO4)3 ' _chemical_formula_sum 'O12 Sc2 W3' _chemical_formula_weight 833.45 _chemical_melting_point ' 1913K ' _chemical_name_common ' Scandium Tungstate ' _chemical_name_systematic ' Scandium Tungstate ' _space_group_IT_number 60 _space_group_name_Hall '-P 2a 2n' _space_group_name_H-M_alt 'P n c a' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M 'P n c a' _audit_creation_date 2008-01-25T12:03 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_update_record ' 2008-01-25T12:03 Initial CIF as created by GSAS2CIF' _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 90.0 _cell_formula_units_Z 4 _cell_length_a 9.62547(5) _cell_length_b 13.35545(8) _cell_length_c 9.55038(5) _cell_measurement_temperature 1050 _cell_volume 1227.725(12) _computing_structure_refinement GSAS _diffrn_radiation_polarisn_ratio 0.68 _diffrn_radiation_probe x-ray _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _pd_block_id 2008-01-25T12:03|T11K|Zhou_Yongkai|Philips_Xpert _pd_calc_method 'Rietveld Refinement' _pd_instr_location ' ?' _pd_meas_2theta_range_inc 0.017 _pd_meas_2theta_range_max 119.9874 _pd_meas_2theta_range_min 10.0144 _pd_meas_number_of_points 6470 _pd_proc_2theta_range_inc 0.017 _pd_proc_2theta_range_max 119.9874 _pd_proc_2theta_range_min 10.0144 _pd_proc_info_datetime 2008-01-25T12:30:46 _pd_proc_info_excluded_regions ' ?' _pd_proc_ls_background_function ; GSAS Background function number 1 with 12 terms. Shifted Chebyshev function of 1st kind 1: 385.012 2: -23.9601 3: -7.76589 4: 54.7664 5: -6.93079 6: 10.8819 7: -12.2698 8: 6.97940 9: 9.34731 10: -24.7793 11: 22.1684 12: -5.79838 ; _pd_proc_ls_peak_cutoff 0.00250 _pd_proc_ls_pref_orient_corr ; March-Dollase AXIS 1 Ratio= 0.95921 h= 0.000 k= 1.000 l= 0.000 Prefered orientation correction range: Min= 0.93945, Max= 1.13305 ; _pd_proc_ls_profile_function ; CW Profile function number 3 with 19 terms Pseudovoigt profile coefficients as parameterized in P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994). J. Appl. Cryst.,27,892-900. #1(GU) = 6.473 #2(GV) = -5.347 #3(GW) = 2.203 #4(GP) = 0.000 #5(LX) = 0.727 #6(LY) = 5.529 #7(S/L) = 0.0313 #8(H/L) = 0.0250 #9(trns) = 0.00 #10(shft)= -15.3303 #11(stec)= 0.00 #12(ptec)= 0.00 #13(sfec)= 0.00 #14(L11) = 0.000 #15(L22) = 0.000 #16(L33) = 0.000 #17(L12) = 0.000 #18(L13) = 0.000 #19(L23) = 0.000 Peak tails are ignored where the intensity is below 0.0025 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_prof_R_factor 0.0502 _pd_proc_ls_prof_wR_expected 0.0363 _pd_proc_ls_prof_wR_factor 0.0657 _pd_proc_number_of_points 6470 _pd_spec_mounting ' ?' _refine_ls_goodness_of_fit_all 1.85 _refine_ls_matrix_type full _refine_ls_number_parameters 51 _refine_ls_number_restraints 0 _refine_ls_R_Fsqd_factor 0.07153 _refine_ls_shift/su_max 0.03 _refine_ls_shift/su_mean 0.01 _reflns_d_resolution_high 0.890 _reflns_d_resolution_low 6.678 _reflns_limit_h_max 10 _reflns_limit_h_min 0 _reflns_limit_k_max 15 _reflns_limit_k_min 0 _reflns_limit_l_max 10 _reflns_limit_l_min 0 _reflns_number_total 1825 _cod_data_source_file cm800466y_si_022.cif _cod_data_source_block T1050K _cod_original_cell_volume 1227.725(14) _cod_database_code 4000048 _gsas_exptl_extinct_corr_t_min 1.00000 _gsas_exptl_extinct_corr_t_max 1.00000 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 -x+1/2,+y+1/2,+z+1/2 3 +x,-y+1/2,+z+1/2 4 -x+1/2,-y,+z -1 -x,-y,-z -2 +x+1/2,-y+1/2,-z+1/2 -3 -x,+y+1/2,-z+1/2 -4 +x+1/2,+y,-z loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Sc Sc1 0.4708(4) 0.38198(26) 0.2477(5) 1.0 Uiso 0.0290(12) 8 W W1 0.25 0.0 0.47111(16) 1.0 Uiso 0.03109(34) 4 W W2 0.11256(12) 0.35641(8) 0.39095(12) 1.0 Uiso 0.03109(34) 8 O O1 0.0929(14) 0.1264(10) 0.0668(14) 1.0 Uiso 0.0721(21) 8 O O2 0.1523(14) 0.0753(9) 0.3718(15) 1.0 Uiso 0.0721(21) 8 O O3 0.0053(13) 0.2655(10) 0.3138(13) 1.0 Uiso 0.0721(21) 8 O O4 0.3353(14) 0.4061(9) 0.0759(14) 1.0 Uiso 0.0721(21) 8 O O5 0.0515(13) 0.4729(10) 0.3190(14) 1.0 Uiso 0.0721(21) 8 O O6 0.2888(15) 0.3484(10) 0.3385(14) 1.0 Uiso 0.0721(21) 8 loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Sc 8.0 0.000 0.000 9.18900 9.02130 7.36790 0.57290 1.64090 136.108 1.46800 51.3531 1.33290 International_Tables_Vol_C W 12.0 0.000 0.000 29.0818 1.72029 15.4300 9.22590 14.4327 0.32170 5.11982 57.0560 9.88750 International_Tables_Vol_C O 48.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C loop_ _diffrn_radiation_wavelength _diffrn_radiation_wavelength_wt _diffrn_radiation_type _diffrn_radiation_wavelength_id 1.540500 1.000 K\a~1~ 1 1.544300 0.000 K\a~2~ 2 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Sc1 O2 90.4(5) -2_666 . -2_666 N O1 Sc1 O3 95.6(5) -2_666 . -2_666 N O1 Sc1 O4 172.5(6) -2_666 . 1_555 N O1 Sc1 O5 80.4(5) -2_666 . 4_565 N O1 Sc1 O6 96.3(6) -2_666 . 1_555 N O2 Sc1 O3 88.4(5) -2_666 . -2_666 N O2 Sc1 O4 92.8(6) -2_666 . 1_555 N O2 Sc1 O5 90.6(5) -2_666 . 4_565 N O2 Sc1 O6 173.0(6) -2_666 . 1_555 N O3 Sc1 O4 91.3(5) -2_666 . 1_555 N O3 Sc1 O5 175.8(6) -2_666 . 4_565 N O3 Sc1 O6 92.8(5) -2_666 . 1_555 N O4 Sc1 O5 92.8(5) 1_555 . 4_565 N O4 Sc1 O6 80.3(5) 1_555 . 1_555 N O5 Sc1 O6 88.7(5) 4_565 . 1_555 N O2 W1 O2 110.9(10) 1_555 . 4_555 N O2 W1 O4 118.5(6) 1_555 . 2_545 N O2 W1 O4 98.7(6) 1_555 . 3_555 N O2 W1 O4 98.7(6) 4_555 . 2_545 N O2 W1 O4 118.5(6) 4_555 . 3_555 N O4 W1 O4 112.6(8) 2_545 . 3_555 N O1 W2 O3 116.1(6) 3_555 . 1_555 N O1 W2 O5 102.9(6) 3_555 . 1_555 N O1 W2 O6 113.1(6) 3_555 . 1_555 N O3 W2 O5 104.2(7) 1_555 . 1_555 N O3 W2 O6 113.8(6) 1_555 . 1_555 N O5 W2 O6 104.9(6) 1_555 . 1_555 N Sc1 O1 W2 152.6(8) -2_466 . 3_554 N Sc1 O2 W1 155.8(8) -2_555 . 1_555 N Sc1 O3 W2 150.0(8) -2_466 . 1_555 N Sc1 O4 W1 144.6(7) 1_555 . 2_554 N Sc1 O5 W2 166.2(8) 4_565 . 1_555 N Sc1 O6 W2 160.9(8) 1_555 . 1_555 N loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sc1 O1 2.128(14) . -2_555 N Sc1 O2 2.163(14) . -2_555 N Sc1 O3 2.083(14) . -2_555 N Sc1 O4 2.121(13) . 1_555 N Sc1 O5 2.066(13) . 4_565 N Sc1 O6 2.005(14) . 1_555 N W1 O2 1.672(13) . 1_555 N W1 O2 1.672(13) . 4_555 N W1 O4 1.802(12) . 2_545 N W1 O4 1.802(12) . 3_555 N W2 O1 1.706(13) . 3_555 N W2 O3 1.755(13) . 1_555 N W2 O5 1.799(13) . 1_555 N W2 O6 1.772(14) . 1_555 N O1 Sc1 2.128(14) . -2_455 N O1 W2 1.706(13) . 3_554 N O2 Sc1 2.163(14) . -2_455 N O2 W1 1.672(13) . 1_555 N O3 Sc1 2.083(14) . -2_455 N O3 W2 1.755(13) . 1_555 N O4 Sc1 2.121(13) . 1_555 N O4 W1 1.802(12) . 2_554 N O5 Sc1 2.066(13) . 4_565 N O5 W2 1.799(13) . 1_555 N O6 Sc1 2.005(14) . 1_555 N O6 W2 1.772(14) . 1_555 N loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 311.0 0.0 644.82654 . 311.0 0.0 641.11761 . 324.0 0.0 637.43756 . 307.0 0.0 633.78595 . 287.0 0.0 630.16229 . 291.0 0.0 626.56738 . 279.0 0.0 623.00024 . 327.0 0.0 619.46094 . 307.0 0.0 615.94977 . 298.0 0.0 612.46564 . 301.0 0.0 609.00952 . 315.0 0.0 605.58051 . 309.0 0.0 602.17865 . 295.0 0.0 598.80408 . 302.0 0.0 595.45624 . 320.0 0.0 592.13525 . 295.0 0.0 588.84088 . 301.0 0.0 585.57275 . 326.0 0.0 582.33160 . 334.0 0.0 579.11652 . 315.0 0.0 575.92749 . 300.0 0.0 572.76440 . 296.0 0.0 569.62695 . 291.0 0.0 566.51550 . 313.0 0.0 563.42975 . 327.0 0.0 560.36938 . 332.0 0.0 557.33417 . 313.0 0.0 554.32416 . 301.0 0.0 551.33911 . 308.0 0.0 548.37952 . 315.0 0.0 545.44409 . 328.0 0.0 542.53363 . 335.0 0.0 539.64752 . 327.0 0.0 536.78613 . 304.0 0.0 533.94904 . 307.0 0.0 531.13593 . 314.0 0.0 528.34680 . 324.0 0.0 525.58148 . 326.0 0.0 522.84015 . 314.0 0.0 520.12262 . 296.0 0.0 517.42841 . 299.0 0.0 514.75763 . 315.0 0.0 512.10992 . 315.0 0.0 509.48569 . 333.0 0.0 506.88452 . 328.0 0.0 504.30612 . 293.0 0.0 501.75046 . 309.0 0.0 499.21729 . 314.0 0.0 496.70712 . 293.0 0.0 494.21915 . 324.0 0.0 491.75366 . 312.0 0.0 489.31003 . 337.0 0.0 486.88846 . 310.0 0.0 484.48904 . 330.0 0.0 482.11151 . 323.0 0.0 479.75571 . 334.0 0.0 477.42130 . 316.0 0.0 475.10825 . 375.0 0.0 472.81689 . 338.0 0.0 470.54681 . 312.0 0.0 468.29770 . 311.0 0.0 466.06952 . 334.0 0.0 463.86221 . 324.0 0.0 461.67584 . 286.0 0.0 459.51016 . 293.0 0.0 457.36508 . 325.0 0.0 455.24020 . 324.0 0.0 453.13574 . 306.0 0.0 451.05154 . 331.0 0.0 448.98758 . 321.0 0.0 446.94357 . 297.0 0.0 444.91928 . 303.0 0.0 442.91486 . 323.0 0.0 440.93002 . 328.0 0.0 438.96494 . 318.0 0.0 437.01920 . 313.0 0.0 435.09262 . 305.0 0.0 433.18552 . 305.0 0.0 431.29733 . 318.0 0.0 429.42834 . 336.0 0.0 427.57834 . 338.0 0.0 425.74680 . 326.0 0.0 423.93408 . 310.0 0.0 422.13995 . 331.0 0.0 420.36453 . 359.0 0.0 418.60727 . 367.0 0.0 416.86832 . 358.0 0.0 415.14752 . 345.0 0.0 413.44473 . 350.0 0.0 411.76007 . 338.0 0.0 410.09320 . 318.0 0.0 408.44400 . 317.0 0.0 406.81247 . 321.0 0.0 405.19843 . 322.0 0.0 403.60199 . 333.0 0.0 402.02298 . 310.0 0.0 400.46100 . 307.0 0.0 398.91620 . 317.0 0.0 397.38849 . 313.0 0.0 395.87778 . 302.0 0.0 394.38391 . 317.0 0.0 392.90668 . 323.0 0.0 391.44614 . 332.0 0.0 390.00226 . 352.0 0.0 388.57471 . 319.0 0.0 387.16360 . 303.0 0.0 385.76865 . 331.0 0.0 384.39005 . 353.0 0.0 383.02737 . 346.0 0.0 381.68073 . 343.0 0.0 380.35001 . 312.0 0.0 379.03497 . 333.0 0.0 377.73557 . 292.0 0.0 376.45203 . 328.0 0.0 375.18378 . 313.0 0.0 373.93100 . 301.0 0.0 372.69357 . 298.0 0.003356 371.47119 371.47031 306.0 0.003268 370.26419 370.26343 327.0 0.003058 369.07211 369.07132 326.0 0.003067 367.89502 367.89426 313.0 0.003195 366.73279 366.73206 313.0 0.003195 365.58524 365.58450 327.0 0.003058 364.45242 364.45172 301.0 0.003322 363.33429 363.33359 323.0 0.003096 362.23056 362.22992 317.0 0.003155 361.14120 361.14059 352.0 0.002841 360.06622 360.06561 348.0 0.002874 359.00543 359.00494 332.0 0.003012 357.95886 357.95834 304.0 0.003289 356.92633 356.92578 318.0 0.003145 355.90775 355.90723 328.0 0.003049 354.90298 354.90253 335.0 0.002985 353.91211 353.91165 311.0 0.003215 352.93494 352.93448 325.0 0.003077 351.97144 351.97098 320.0 0.003125 351.02136 351.02097 322.0 0.003106 350.08469 350.08441 306.0 0.003268 349.16156 349.16122 317.0 0.003155 348.25171 348.25131 320.0 0.003125 347.35495 347.35461 327.0 0.003058 346.47137 346.47107 323.0 0.003096 345.60068 345.60043 314.0 0.003185 344.74313 344.74292 322.0 0.003106 343.89844 343.89822 346.0 0.002890 343.06653 343.06622 339.0 0.002950 342.24722 342.24695 317.0 0.003155 341.44043 341.44025 331.0 0.003021 340.64645 340.64633 344.0 0.002907 339.86484 339.86469 332.0 0.003012 339.09555 339.09549 328.0 0.003049 338.33862 338.33853 333.0 0.003003 337.59384 337.59369 325.0 0.003077 336.86127 336.86111 329.0 0.003040 336.14069 336.14069 330.0 0.003030 335.43216 335.43204 320.0 0.003125 334.73547 334.73544 321.0 0.003115 334.05057 334.05057 349.0 0.002865 333.37753 333.37753 341.0 0.002933 332.71613 332.71609 324.0 0.003086 332.06622 332.06631 337.0 0.002967 331.42801 331.42804 306.0 0.003268 330.80106 330.80109 343.0 0.002915 330.18558 330.18567 327.0 0.003058 329.58130 329.58142 331.0 0.003021 328.98828 328.98840 328.0 0.003049 328.40637 332.08313 362.0 0.002762 327.83551 331.82611 309.0 0.003236 327.27576 333.46576 333.0 0.003003 326.72678 333.49438 370.0 0.002703 326.18869 333.63318 334.0 0.002994 325.66132 333.91260 370.0 0.002703 325.14462 334.37906 342.0 0.002924 324.63861 335.11169 388.0 0.002577 324.14313 336.30661 407.0 0.002457 323.65808 338.78888 421.0 0.002375 323.18344 345.09094 452.0 0.002212 322.71912 358.06091 442.0 0.002262 322.26505 377.76624 431.0 0.002320 321.82117 403.18625 470.0 0.002128 321.38748 433.00095 475.0 0.002105 320.96371 466.15414 462.0 0.002165 320.54999 502.48575 521.0 0.001919 320.14612 542.27997 572.0 0.001748 319.75217 586.05597 611.0 0.001637 319.36792 634.44446 639.0 0.001565 318.99332 688.20898 717.0 0.001395 318.62830 748.44720 784.0 0.001276 318.27304 816.45679 859.0 0.001164 317.92715 894.05542 921.0 0.001086 317.59064 983.71063 1078.0 0.000928 317.26355 1088.84961 1244.0 0.000804 316.94568 1214.51929 1412.0 0.000708 316.63708 1368.44006 1723.0 0.000580 316.33765 1563.32568 2088.0 0.000479 316.04727 1822.53491 2725.0 0.000367 315.76593 2198.70410 3431.0 0.0002915 315.49353 2819.76196 4021.0 0.0002487 315.23001 3700.01050 3900.0 0.0002564 314.97531 3892.53931 2932.0 0.0003411 314.72943 2874.56787 1940.0 0.000515 314.49213 1921.11829 1125.0 0.000889 314.26355 1009.90356 633.0 0.001580 314.04343 558.56842 487.0 0.002053 313.83188 436.76831 433.0 0.002309 313.62885 396.79684 395.0 0.002532 313.43414 374.90579 388.0 0.002577 313.24765 360.80145 409.0 0.002445 313.06949 351.08405 379.0 0.002639 312.89951 344.05981 353.0 0.002833 312.73767 338.79074 356.0 0.002809 312.58389 334.71957 341.0 0.002933 312.43802 331.49789 341.0 0.002933 312.30023 328.89716 340.0 0.002941 312.17023 326.76212 341.0 0.002933 312.04807 324.98428 349.0 0.002865 311.93365 323.48581 365.0 0.002740 311.82693 322.20944 350.0 0.002857 311.72787 321.11276 339.0 0.002950 311.63644 320.16302 342.0 0.002924 311.55240 319.33502 336.0 0.002976 311.47586 314.11819 357.0 0.002801 311.40683 311.40720 333.0 0.003003 311.34506 311.34540 348.0 0.002874 311.29059 311.29102 356.0 0.002809 311.24326 311.24374 336.0 0.002976 311.20325 311.20361 352.0 0.002841 311.17029 311.17065 357.0 0.002801 311.14435 311.14474 339.0 0.002950 311.12540 311.12579 327.0 0.003058 311.11340 311.11386 334.0 0.002994 311.10846 311.10876 325.0 0.003077 311.11008 311.11050 339.0 0.002950 311.11859 311.11899 322.0 0.003106 311.13385 311.13422 329.0 0.003040 311.15573 311.15604 316.0 0.003165 311.18423 311.18460 368.0 0.002717 311.21930 311.21967 345.0 0.002899 311.26083 311.26120 362.0 0.002762 311.30884 311.30923 321.0 0.003115 311.36325 311.36359 344.0 0.002907 311.42395 311.42432 345.0 0.002899 311.49097 311.49130 360.0 0.002778 311.56418 311.56454 366.0 0.002732 311.64359 311.64392 357.0 0.002801 311.72910 311.72949 341.0 0.002933 311.82074 311.82111 354.0 0.002825 311.91840 311.91873 345.0 0.002899 312.02197 316.86005 346.0 0.002890 312.13147 317.35657 354.0 0.002825 312.24686 320.29315 359.0 0.002786 312.36801 321.10571 391.0 0.002558 312.49500 322.02649 384.0 0.002604 312.62759 323.07962 379.0 0.002639 312.76596 324.29868 397.0 0.002519 312.90991 325.73096 419.0 0.002387 313.05936 327.44855 437.0 0.002288 313.21436 329.56882 442.0 0.002262 313.37482 332.33759 433.0 0.002309 313.54071 336.67538 419.0 0.002387 313.71194 345.87454 438.0 0.002283 313.88849 365.05594 495.0 0.002020 314.07034 395.41354 513.0 0.001949 314.25742 435.62283 506.0 0.001976 314.44965 484.50043 524.0 0.001908 314.64688 540.15948 615.0 0.001626 314.84927 601.98163 677.0 0.001477 315.05667 670.51141 733.0 0.001364 315.26917 746.69635 821.0 0.001218 315.48645 832.02771 872.0 0.001147 315.70862 928.47858 917.0 0.001091 315.93567 1038.41101 1049.0 0.000953 316.16763 1165.43396 1200.0 0.000833 316.40414 1314.35132 1418.0 0.000705 316.64548 1492.32166 1658.0 0.000603 316.89145 1710.35535 1974.0 0.000507 317.14203 1986.61304 2413.0 0.000414 317.39719 2354.63159 3112.0 0.0003213 317.65680 2890.73071 3972.0 0.0002518 317.92099 3775.59106 4923.0 0.0002031 318.18951 4981.29395 4712.0 0.0002122 318.46240 5103.24707 3542.0 0.0002823 318.73972 3688.71362 2499.0 0.000400 319.02136 2610.89722 1360.0 0.000735 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451.18268 1191.59851 1446.0 0.000692 450.97018 1497.23718 1880.0 0.000532 450.75787 1935.08167 2661.0 0.000376 450.54568 2606.38745 3703.0 0.0002701 450.33365 3615.81934 4522.0 0.0002211 450.12170 4328.73633 3242.0 0.0003085 449.90976 3293.94409 1935.0 0.000517 449.69809 2151.45801 2003.0 0.000499 449.48651 2035.70935 2402.0 0.000416 449.27502 2333.25146 2120.0 0.000472 449.06366 2037.93665 1216.0 0.000822 448.85245 1203.65161 767.0 0.001304 448.64142 792.76453 653.0 0.001531 448.43045 689.63025 675.0 0.001481 448.21967 681.58881 648.0 0.001543 448.00903 709.67963 728.0 0.001374 447.79852 766.25275 796.0 0.001256 447.58820 856.41095 939.0 0.001065 447.37799 992.48846 1187.0 0.000842 447.16797 1205.23633 1501.0 0.000666 446.95813 1540.35425 1751.0 0.000571 446.74829 1857.28064 1546.0 0.000647 446.53885 1610.07727 1106.0 0.000904 446.32947 1138.93188 983.0 0.001017 446.12030 1032.81372 1079.0 0.000927 445.91138 1137.43665 1090.0 0.000917 445.70242 1117.59802 875.0 0.001143 445.49384 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439.73795 480.50555 454.0 0.002203 439.53583 470.69458 446.0 0.002242 439.33414 463.93155 380.0 0.002632 439.13254 460.09338 426.0 0.002347 438.93127 457.38394 413.0 0.002421 438.73038 455.18634 424.0 0.002358 438.52960 445.25766 408.0 0.002451 438.32922 444.32507 382.0 0.002618 438.12903 443.51239 433.0 0.002309 437.92926 442.79324 400.0 0.002500 437.72971 437.95612 380.0 0.002632 437.53036 437.72589 409.0 0.002445 437.33145 437.50214 402.0 0.002488 437.13272 437.28314 443.0 0.002257 436.93439 437.06802 423.0 0.002364 436.73630 436.85583 409.0 0.002445 436.53848 436.64618 427.0 0.002342 436.34109 436.38397 420.0 0.002381 436.14389 436.18253 404.0 0.002475 435.94708 435.98196 396.0 0.002525 435.75064 435.78238 384.0 0.002604 435.55429 435.55496 379.0 0.002639 435.35855 435.35910 376.0 0.002660 435.16293 435.16348 390.0 0.002564 434.96771 434.96835 382.0 0.002618 434.77283 434.77344 400.0 0.002500 434.57822 434.57880 398.0 0.002513 434.38397 434.38455 418.0 0.002392 434.18994 434.19064 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428.72235 428.72314 412.0 0.002427 428.53952 428.54025 378.0 0.002646 428.35715 428.35785 400.0 0.002500 428.17514 428.17584 465.0 0.002151 427.99344 427.99420 414.0 0.002415 427.81229 427.81305 419.0 0.002387 427.63147 427.63226 414.0 0.002415 427.45114 427.45190 426.0 0.002347 427.27112 427.27194 410.0 0.002439 427.09158 427.09238 377.0 0.002653 426.91254 426.91327 415.0 0.002410 426.73380 426.73453 417.0 0.002398 426.55554 426.55630 400.0 0.002500 426.37772 426.37839 417.0 0.002398 426.20023 426.20096 419.0 0.002387 426.02319 426.02396 410.0 0.002439 425.84665 425.84738 394.0 0.002538 425.67053 425.67139 413.0 0.002421 425.49478 425.49564 432.0 0.002315 425.31949 425.32025 407.0 0.002457 425.14471 425.14551 423.0 0.002364 424.97031 424.97110 408.0 0.002451 424.79633 424.79715 433.0 0.002309 424.62289 424.62366 430.0 0.002326 424.44983 426.32712 411.0 0.002433 424.27719 426.27884 403.0 0.002481 424.10495 426.24380 409.0 0.002445 423.93329 426.22391 411.0 0.002433 423.76202 426.22119 417.0 0.002398 423.59122 427.18402 407.0 0.002457 423.42087 427.28726 421.0 0.002375 423.25095 427.42395 409.0 0.002445 423.08154 427.59946 396.0 0.002525 422.91251 427.82071 414.0 0.002415 422.74402 428.09622 420.0 0.002381 422.57596 436.40891 406.0 0.002463 422.40839 437.36990 425.0 0.002353 422.24130 438.48315 431.0 0.002320 422.07465 439.77966 436.0 0.002294 421.90842 441.29883 429.0 0.002331 421.74277 447.10193 410.0 0.002439 421.57745 449.51083 424.0 0.002358 421.41275 455.78772 437.0 0.002288 421.24847 459.49225 447.0 0.002237 421.08469 464.02502 436.0 0.002294 420.92126 469.69754 467.0 0.002141 420.75848 477.04626 534.0 0.001873 420.59616 490.05209 527.0 0.001898 420.43427 506.90665 550.0 0.001818 420.27283 538.89551 611.0 0.001637 420.11200 592.67761 688.0 0.001453 419.95157 674.10681 772.0 0.001295 419.79160 780.12488 908.0 0.001101 419.63226 924.05646 1164.0 0.000859 419.47324 1133.37976 1506.0 0.000664 419.31488 1455.64368 2009.0 0.000498 419.15689 1933.95447 2425.0 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981.83215 963.0 0.001038 414.94174 1023.46442 886.0 0.001129 414.79883 922.79041 702.0 0.001425 414.65634 691.92938 578.0 0.001730 414.51450 568.98041 518.0 0.001931 414.37311 523.52094 467.0 0.002141 414.23236 486.57202 473.0 0.002114 414.09207 473.38855 476.0 0.002101 413.95230 464.03500 455.0 0.002198 413.81311 457.05206 430.0 0.002326 413.67447 451.66147 431.0 0.002320 413.53635 440.11255 434.0 0.002304 413.39883 437.33597 452.0 0.002212 413.26187 428.53827 430.0 0.002326 413.12537 427.50250 450.0 0.002222 412.98947 426.95090 445.0 0.002247 412.85403 427.06161 413.0 0.002421 412.71927 428.51822 410.0 0.002439 412.58496 429.42435 413.0 0.002421 412.45132 437.55472 417.0 0.002398 412.31808 449.64828 429.0 0.002331 412.18549 466.11353 443.0 0.002257 412.05350 488.85614 490.0 0.002041 411.92188 523.66840 498.0 0.002008 411.79102 579.12708 541.0 0.001848 411.66061 640.96082 527.0 0.001898 411.53076 621.11090 495.0 0.002020 411.40155 533.49774 446.0 0.002242 411.27283 499.55054 444.0 0.002252 411.14468 510.55457 468.0 0.002137 411.01709 532.57660 463.0 0.002160 410.88998 513.44000 458.0 0.002183 410.76358 463.65366 456.0 0.002193 410.63770 439.39792 432.0 0.002315 410.51242 432.52658 430.0 0.002326 410.38760 430.75153 425.0 0.002353 410.26334 430.74298 416.0 0.002404 410.13974 431.86978 430.0 0.002326 410.01669 434.03879 454.0 0.002203 409.89423 438.81860 479.0 0.002088 409.77231 443.92047 516.0 0.001938 409.65097 451.69113 513.0 0.001949 409.53015 465.32028 554.0 0.001805 409.40994 495.66562 540.0 0.001852 409.29031 550.69727 681.0 0.001468 409.17120 634.94391 785.0 0.001274 409.05270 752.56177 853.0 0.001172 408.93484 917.38196 1154.0 0.000867 408.81747 1151.51038 1563.0 0.000640 408.70068 1521.86914 2231.0 0.000448 408.58453 2055.20337 2428.0 0.000412 408.46890 2322.84204 1801.0 0.000555 408.35385 1700.08386 1204.0 0.000831 408.23938 1164.93396 1163.0 0.000860 408.12558 1104.80591 1327.0 0.000754 408.01227 1279.58191 1397.0 0.000716 407.89951 1362.29382 1059.0 0.000944 407.78735 1003.92444 665.0 0.001504 407.67584 670.50555 568.0 0.001761 407.56485 547.84027 526.0 0.001901 407.45450 510.39542 494.0 0.002024 407.34464 496.21033 524.0 0.001908 407.23544 492.73734 528.0 0.001894 407.12680 500.53372 553.0 0.001808 407.01874 525.64764 630.0 0.001587 406.91122 569.81140 713.0 0.001403 406.80435 642.33905 809.0 0.001236 406.69806 745.63861 969.0 0.001032 406.59238 905.66809 1213.0 0.000824 406.48724 1155.92761 1613.0 0.000620 406.38269 1542.28137 1971.0 0.000507 406.27878 1972.40857 2002.0 0.000500 406.17538 1990.38818 1952.0 0.000512 406.07257 1836.01587 2231.0 0.000448 405.97043 2105.94336 2484.0 0.000403 405.86884 2436.39429 2189.0 0.000457 405.76779 2098.03833 1581.0 0.000633 405.66742 1535.39038 1232.0 0.000812 405.56760 1195.04761 1210.0 0.000826 405.46835 1191.20239 1258.0 0.000795 405.36981 1256.88574 1037.0 0.000964 405.27167 1002.12128 739.0 0.001353 405.17422 699.73669 624.0 0.001603 405.07733 586.91089 620.0 0.001613 404.98108 575.38934 602.0 0.001661 404.88541 606.16400 649.0 0.001541 404.79028 670.94006 720.0 0.001389 404.69586 767.50067 884.0 0.001131 404.60196 910.61694 1136.0 0.000880 404.50873 1146.38123 1541.0 0.000649 404.41599 1507.70435 1728.0 0.000579 404.32385 1777.79602 1474.0 0.000678 404.23233 1496.32703 1185.0 0.000844 404.14142 1204.11707 1208.0 0.000828 404.05112 1266.93579 1660.0 0.000602 403.96146 1581.89917 2135.0 0.000468 403.87225 2002.39124 2212.0 0.000452 403.78375 2055.11401 1522.0 0.000657 403.69586 1478.80652 936.0 0.001068 403.60849 986.60876 816.0 0.001225 403.52179 871.59485 944.0 0.001059 403.43561 948.52228 1023.0 0.000978 403.35004 1037.42346 890.0 0.001124 403.26511 876.13068 601.0 0.001664 403.18076 624.58746 508.0 0.001969 403.09702 512.97583 508.0 0.001969 403.01385 476.50104 487.0 0.002053 402.93130 460.90134 431.0 0.002320 402.84937 452.41229 411.0 0.002433 402.76810 447.52292 468.0 0.002137 402.68732 444.63693 457.0 0.002188 402.60718 443.83255 469.0 0.002132 402.52756 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3538.0 0.0002826 399.25589 3109.72974 3067.0 0.0003261 399.30035 2879.44434 1876.0 0.000533 399.34534 1777.99780 1274.0 0.000785 399.39078 1267.65759 1341.0 0.000746 399.43655 1291.25195 1650.0 0.000606 399.48282 1570.65442 1987.0 0.000503 399.52945 1840.65576 1690.0 0.000592 399.57663 1522.81445 998.0 0.001002 399.62427 929.12158 608.0 0.001645 399.67224 647.41071 574.0 0.001742 399.72070 554.31879 539.0 0.001855 399.76956 521.60352 535.0 0.001869 399.81885 507.63815 525.0 0.001905 399.86856 510.79321 546.0 0.001832 399.91876 529.09381 585.0 0.001709 399.96933 567.81940 645.0 0.001550 400.02032 625.33917 777.0 0.001287 400.07178 721.19952 963.0 0.001038 400.12360 854.70581 1022.0 0.000978 400.17584 914.32599 843.0 0.001186 400.22861 752.47107 668.0 0.001497 400.28162 616.52557 608.0 0.001645 400.33524 590.25964 654.0 0.001529 400.38916 624.25220 721.0 0.001387 400.44348 684.99091 759.0 0.001318 400.49826 698.15869 718.0 0.001393 400.55350 607.70526 660.0 0.001515 400.60910 545.69232 628.0 0.001592 400.66504 534.90796 650.0 0.001538 400.72144 548.65759 708.0 0.001412 400.77829 580.15137 813.0 0.001230 400.83548 640.47980 950.0 0.001053 400.89310 777.28662 1111.0 0.000900 400.95111 1028.31470 1433.0 0.000698 401.00949 1425.99365 1952.0 0.000512 401.06833 2010.74683 3021.0 0.0003310 401.12759 2920.36841 4449.0 0.0002248 401.18716 4250.17773 5795.0 0.0001726 401.24722 5463.36426 4646.0 0.0002152 401.30759 4523.14990 2624.0 0.000381 401.36835 2618.25708 1858.0 0.000538 401.42957 1917.13452 1949.0 0.000513 401.49109 2058.96729 2610.0 0.000383 401.55307 2599.38574 3134.0 0.0003191 401.61545 3054.61841 2504.0 0.000399 401.67822 2383.33130 1487.0 0.000672 401.74127 1371.02222 1001.0 0.000999 401.80484 951.65814 926.0 0.001080 401.86871 875.34637 1009.0 0.000991 401.93292 925.93610 1162.0 0.000861 401.99756 1079.19336 1520.0 0.000658 402.06259 1335.42554 1937.0 0.000516 402.12802 1550.16174 1606.0 0.000623 402.19376 1377.91077 1198.0 0.000835 402.25986 1180.56628 1281.0 0.000781 402.32645 1222.09753 1676.0 0.000597 402.39328 1453.27478 2022.0 0.000495 402.46054 1786.95227 2088.0 0.000479 402.52814 1771.38928 1516.0 0.000660 402.59610 1270.61877 1075.0 0.000930 402.66449 943.42749 949.0 0.001054 402.73322 874.15308 1039.0 0.000962 402.80225 931.48712 1174.0 0.000852 402.87164 1040.07141 1153.0 0.000867 402.94147 1017.61737 1063.0 0.000941 403.01163 903.46570 1081.0 0.000925 403.08209 945.10413 1205.0 0.000830 403.15292 1142.17053 1567.0 0.000638 403.22415 1514.15808 2167.0 0.000461 403.29568 2083.69727 2588.0 0.000386 403.36758 2584.12207 2639.0 0.000379 403.43985 2641.94336 2803.0 0.000357 403.51245 2935.60791 3285.0 0.0003044 403.58545 3492.34888 3339.0 0.0002995 403.65872 3375.68237 2997.0 0.0003337 403.73233 3018.27271 2475.0 0.000404 403.80630 2534.53198 1923.0 0.000520 403.88065 1964.05493 1717.0 0.000582 403.95529 1826.86926 1798.0 0.000556 404.03030 1955.93542 1711.0 0.000584 404.10556 1763.78394 1419.0 0.000705 404.18124 1424.15991 1036.0 0.000965 404.25726 1050.46204 769.0 0.001300 404.33356 752.91364 658.0 0.001520 404.41016 627.13263 637.0 0.001570 404.48721 590.66437 655.0 0.001527 404.56448 595.37622 651.0 0.001536 404.64206 637.68066 736.0 0.001359 404.72006 721.71411 882.0 0.001134 404.79834 855.59180 1163.0 0.000860 404.87698 1073.95593 1578.0 0.000634 404.95584 1384.09424 1717.0 0.000582 405.03506 1579.66125 1373.0 0.000728 405.11469 1261.09473 939.0 0.001065 405.19455 902.69604 810.0 0.001235 405.27463 824.76953 937.0 0.001067 405.35513 920.27271 1167.0 0.000857 405.43591 1118.81274 1361.0 0.000735 405.51706 1318.10706 1337.0 0.000748 405.59848 1315.65198 1248.0 0.000801 405.68018 1248.64233 1031.0 0.000970 405.76224 1040.79956 765.0 0.001307 405.84454 772.60028 696.0 0.001437 405.92712 671.81958 734.0 0.001362 406.01010 678.64758 773.0 0.001294 406.09335 744.26233 902.0 0.001109 406.17691 824.51685 845.0 0.001183 406.26065 794.30212 780.0 0.001282 406.34479 708.60321 783.0 0.001277 406.42917 734.30255 926.0 0.001080 406.51389 870.07440 1179.0 0.000848 406.59888 1123.10498 1605.0 0.000623 406.68411 1535.38696 2265.0 0.000442 406.76968 2154.96240 2943.0 0.0003398 406.85556 2760.16797 2968.0 0.0003369 406.94171 2749.37939 2965.0 0.0003373 407.02808 2600.08008 2709.0 0.000369 407.11475 2456.10229 1939.0 0.000516 407.20175 1866.74841 1598.0 0.000626 407.28894 1624.88489 1739.0 0.000575 407.37650 1731.44446 1716.0 0.000583 407.46423 1673.51904 1649.0 0.000606 407.55234 1509.13623 1508.0 0.000663 407.64069 1381.79968 1066.0 0.000938 407.72928 993.31549 715.0 0.001399 407.81818 689.34882 557.0 0.001795 407.90732 566.40131 480.0 0.002083 407.99670 518.05536 504.0 0.001984 408.08633 492.59641 497.0 0.002012 408.17627 476.13269 449.0 0.002227 408.26654 465.64267 455.0 0.002198 408.35693 457.68253 468.0 0.002137 408.44763 453.25894 461.0 0.002169 408.53864 450.56744 456.0 0.002193 408.62988 449.75632 464.0 0.002155 408.72131 451.33365 466.0 0.002146 408.81299 457.36942 466.0 0.002146 408.90497 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507.0 0.001972 364.56540 514.98743 540.0 0.001852 364.63959 514.44696 543.0 0.001842 364.71378 509.84549 496.0 0.002016 364.78799 500.81186 488.0 0.002049 364.86218 486.57224 432.0 0.002315 364.93655 468.59531 451.0 0.002217 365.01089 450.23813 421.0 0.002375 365.08533 434.05402 385.0 0.002597 365.15982 421.22543 395.0 0.002532 365.23419 411.87006 411.0 0.002433 365.30878 405.70084 419.0 0.002387 365.38330 402.37814 421.0 0.002375 365.45807 401.43210 400.0 0.002500 365.53281 402.74823 421.0 0.002375 365.60745 405.88730 434.0 0.002304 365.68228 410.33008 460.0 0.002174 365.75705 415.60504 434.0 0.002304 365.83206 420.67499 412.0 0.002427 365.90695 424.34097 429.0 0.002331 365.98193 425.99835 419.0 0.002387 366.05701 426.36514 414.0 0.002415 366.13211 426.71082 428.0 0.002336 366.20731 428.03094 452.0 0.002212 366.28250 430.29419 463.0 0.002160 366.35767 432.88092 452.0 0.002212 366.43307 434.85010 446.0 0.002242 366.50842 435.50037 453.0 0.002208 366.58389 434.72058 433.0 0.002309 366.65942 431.87247 434.0 0.002304 366.73489 426.45959 426.0 0.002347 366.81058 418.82782 374.0 0.002674 366.88617 410.41977 390.0 0.002564 366.96194 402.73642 396.0 0.002525 367.03787 396.57956 386.0 0.002591 367.11356 392.10043 388.0 0.002577 367.18951 389.11523 401.0 0.002494 367.26547 387.28918 377.0 0.002653 367.34158 386.10083 370.0 0.002703 367.41772 385.20755 368.0 0.002717 367.49380 384.69031 396.0 0.002525 367.57004 384.47375 373.0 0.002681 367.64639 384.67508 368.0 0.002717 367.72278 385.42365 355.0 0.002817 367.79926 386.88882 393.0 0.002545 367.87573 389.15350 387.0 0.002584 367.95239 392.06464 397.0 0.002519 368.02896 395.10297 393.0 0.002545 368.10574 397.28394 378.0 0.002646 368.18250 397.65909 385.0 0.002597 368.25934 396.01169 371.0 0.002695 368.33636 393.09390 397.0 0.002519 368.41327 390.00809 376.0 0.002660 368.49048 387.27991 378.0 0.002646 368.56766 385.11603 362.0 0.002762 368.64481 383.57993 389.0 0.002571 368.72217 382.77512 377.0 0.002653 368.79962 382.60434 377.0 0.002653 368.87711 383.02722 365.0 0.002740 368.95465 383.74695 381.0 0.002625 369.03223 385.07501 380.0 0.002632 369.10995 387.17874 381.0 0.002625 369.18774 390.06802 401.0 0.002494 369.26566 393.60062 394.0 0.002538 369.34363 397.13086 421.0 0.002375 369.42166 399.91583 401.0 0.002494 369.49985 400.71597 395.0 0.002532 369.57806 399.35672 408.0 0.002451 369.65640 396.52158 380.0 0.002632 369.73480 393.42792 390.0 0.002564 369.81317 390.93277 363.0 0.002755 369.89188 389.20392 359.0 0.002786 369.97046 388.55801 370.0 0.002703 370.04932 388.48941 382.0 0.002618 370.12827 388.43732 372.0 0.002688 370.20712 387.91034 374.0 0.002674 370.28622 386.83942 397.0 0.002519 370.36530 385.55698 381.0 0.002625 370.44461 384.42654 367.0 0.002725 370.52396 383.65884 364.0 0.002747 370.60327 383.36469 364.0 0.002747 370.68283 383.65576 368.0 0.002717 370.76251 384.59583 379.0 0.002639 370.84229 386.31918 388.0 0.002577 370.92209 388.74274 385.0 0.002597 371.00198 391.98337 361.0 0.002770 371.08209 395.81180 395.0 0.002532 371.16220 399.92911 414.0 0.002415 371.24246 403.67255 383.0 0.002611 371.32288 406.43170 379.0 0.002639 371.40326 408.05878 394.0 0.002538 371.48389 408.50690 400.0 0.002500 371.56458 407.53574 406.0 0.002463 371.64542 405.03616 389.0 0.002571 371.72632 401.70987 372.0 0.002688 371.80725 398.52298 409.0 0.002445 371.88849 396.10992 402.0 0.002488 371.96979 394.79044 418.0 0.002392 372.05112 394.81509 415.0 0.002410 372.13266 396.31982 422.0 0.002370 372.21414 399.53516 407.0 0.002457 372.29593 404.55054 473.0 0.002114 372.37775 411.20917 500.0 0.002000 372.45972 418.93182 482.0 0.002075 372.54187 426.32718 452.0 0.002212 372.62405 431.23749 403.0 0.002481 372.70639 431.90530 444.0 0.002252 372.78882 428.58078 427.0 0.002342 372.87146 423.33633 413.0 0.002421 372.95413 418.37411 381.0 0.002625 373.03696 414.81985 406.0 0.002463 373.11996 412.74524 393.0 0.002545 373.20309 411.97324 376.0 0.002660 373.28638 411.63373 408.0 0.002451 373.36978 411.15536 382.0 0.002618 373.45316 410.37134 401.0 0.002494 373.53690 409.48224 399.0 0.002506 373.62064 408.71863 409.0 0.002445 373.70459 407.89539 447.0 0.002237 373.78870 406.46942 397.0 0.002519 373.87280 404.16940 416.0 0.002404 373.95721 401.35403 380.0 0.002632 374.04166 398.68518 377.0 0.002653 374.12637 396.64368 420.0 0.002381 374.21121 395.60028 388.0 0.002577 374.29602 395.55334 377.0 0.002653 374.38107 396.69025 401.0 0.002494 374.46631 399.09125 427.0 0.002342 374.55167 402.64136 463.0 0.002160 374.63730 407.13913 433.0 0.002309 374.72290 412.09735 416.0 0.002404 374.80878 416.68402 426.0 0.002347 374.89471 420.07828 422.0 0.002370 374.98096 422.45557 447.0 0.002237 375.06720 424.92236 440.0 0.002273 375.15366 428.66153 451.0 0.002217 375.24030 434.10431 469.0 0.002132 375.32706 440.77039 480.0 0.002083 375.41403 447.42017 529.0 0.001890 375.50119 452.58289 495.0 0.002020 375.58841 455.04755 449.0 0.002227 375.67593 454.14905 444.0 0.002252 375.76349 450.57877 469.0 0.002132 375.85135 446.34787 457.0 0.002188 375.93924 443.14255 459.0 0.002179 376.02728 441.25330 490.0 0.002041 376.11566 439.70917 483.0 0.002070 376.20407 436.90836 454.0 0.002203 376.29291 431.76938 434.0 0.002304 376.38165 424.78857 418.0 0.002392 376.47061 417.40195 406.0 0.002463 376.55984 410.78387 393.0 0.002545 376.64923 405.42853 391.0 0.002558 376.73883 401.53598 376.0 0.002660 376.82861 398.94220 382.0 0.002618 376.91843 397.46008 397.0 0.002519 377.00861 397.05432 400.0 0.002500 377.09885 397.67651 407.0 0.002457 377.18942 399.39194 438.0 0.002283 377.28015 402.36749 394.0 0.002538 377.37094 406.88022 430.0 0.002326 377.46207 413.22925 447.0 0.002237 377.55338 421.64615 451.0 0.002217 377.64484 431.88071 513.0 0.001949 377.73657 443.35391 557.0 0.001795 377.82834 454.77969 496.0 0.002016 377.92050 464.05502 464.0 0.002155 378.01270 468.39816 431.0 0.002320 378.10526 466.23480 479.0 0.002088 378.19800 458.94037 475.0 0.002105 378.29080 449.85959 440.0 0.002273 378.38394 441.53488 461.0 0.002169 378.47720 435.06226 471.0 0.002123 378.57089 430.30258 443.0 0.002257 378.66464 426.49319 435.0 0.002299 378.75845 423.30618 386.0 0.002591 378.85275 421.01395 444.0 0.002252 378.94708 420.05588 470.0 0.002128 379.04187 420.48499 411.0 0.002433 379.13669 421.82608 448.0 0.002232 379.23166 423.10599 431.0 0.002320 379.32706 423.06699 379.0 0.002639 379.42252 421.26053 369.0 0.002710 379.51834 418.34662 365.0 0.002740 379.61435 415.52997 382.0 0.002618 379.71045 413.87064 426.0 0.002347 379.80704 413.81485 394.0 0.002538 379.90369 415.72610 420.0 0.002381 380.00067 419.55847 442.0 0.002262 380.09778 424.98691 409.0 0.002445 380.19510 431.22549 439.0 0.002278 380.29285 436.99802 449.0 0.002227 380.39066 441.23218 432.0 0.002315 380.48889 443.32849 431.0 0.002320 380.58728 443.01547 430.0 0.002326 380.68588 440.30661 425.0 0.002353 380.78482 436.03467 408.0 0.002451 380.88388 431.19919 384.0 0.002604 380.98340 426.66672 391.0 0.002558 381.08304 423.24072 381.0 0.002625 381.18283 421.60529 397.0 0.002519 381.28305 422.18741 438.0 0.002283 381.38348 425.17947 438.0 0.002283 381.48416 430.50806 445.0 0.002247 381.58524 437.80853 459.0 0.002179 381.68634 445.59088 460.0 0.002174 381.78790 452.27652 479.0 0.002088 381.88968 456.27408 460.0 0.002174 381.99167 456.87805 455.0 0.002198 382.09412 454.39514 449.0 0.002227 382.19656 449.55402 410.0 0.002439 382.29947 443.61929 417.0 0.002398 382.40256 437.88831 414.0 0.002415 382.50601 433.13409 433.0 0.002309 382.60977 429.38806 399.0 0.002506 382.71362 426.53348 431.0 0.002320 382.81799 424.58643 406.0 0.002463 382.92249 423.49542 413.0 0.002421 383.02744 422.92593 425.0 0.002353 383.13260 422.65009 433.0 0.002309 383.23792 422.76263 417.0 0.002398 383.34378 423.39337 432.0 0.002315 383.44971 424.62747 438.0 0.002283 383.55618 425.83289 396.0 0.002525 383.66275 426.34311 438.0 0.002283 383.76956 425.70407 460.0 0.002174 383.87692 424.33978 393.0 0.002545 383.98441 423.16479 409.0 0.002445 384.09235 423.18799 407.0 0.002457 384.20053 424.96432 427.0 0.002342 384.30890 428.86368 412.0 0.002427 384.41785 434.97769 449.0 0.002227 384.52682 443.05695 500.0 0.002000 384.63641 452.23206 491.0 0.002037 384.74615 461.57660 507.0 0.001972 384.85614 470.02008 467.0 0.002141 384.96661 475.87628 498.0 0.002008 385.07727 477.37408 476.0 0.002101 385.18845 474.25830 436.0 0.002294 385.29993 468.43295 478.0 0.002092 385.41147 462.29211 436.0 0.002294 385.52359 457.38678 427.0 0.002342 385.63596 454.44055 457.0 0.002188 385.74878 453.61172 472.0 0.002119 385.86191 454.35965 451.0 0.002217 385.97522 455.31287 445.0 0.002247 386.08905 454.57608 437.0 0.002288 386.20309 451.60904 399.0 0.002506 386.31766 447.22894 419.0 0.002387 386.43246 443.12155 433.0 0.002309 386.54752 440.17838 432.0 0.002315 386.66315 438.54489 429.0 0.002331 386.77902 437.91364 403.0 0.002481 386.89529 437.65179 426.0 0.002347 387.01196 437.08148 455.0 0.002198 387.12881 435.46338 448.0 0.002232 387.24622 432.77277 402.0 0.002488 387.36389 429.78726 379.0 0.002639 387.48212 427.41025 424.0 0.002358 387.60056 426.15573 441.0 0.002268 387.71915 426.24146 445.0 0.002247 387.83847 427.56119 461.0 0.002169 387.95810 429.81488 464.0 0.002155 388.07813 432.16342 432.0 0.002315 388.19849 433.63596 425.0 0.002353 388.31909 433.48889 453.0 0.002208 388.44028 432.11365 425.0 0.002353 388.56174 430.54279 420.0 0.002381 388.68381 429.66074 436.0 0.002294 388.80609 430.01114 452.0 0.002212 388.92868 431.81360 437.0 0.002288 389.05182 434.92838 438.0 0.002283 389.17529 438.94528 446.0 0.002242 389.29935 442.83072 479.0 0.002088 389.42358 446.06427 466.0 0.002146 389.54825 448.56277 443.0 0.002257 389.67346 450.59631 448.0 0.002232 389.79904 452.14246 435.0 0.002299 389.92502 453.20996 427.0 0.002342 390.05142 454.50543 430.0 0.002326 390.17807 457.17242 445.0 0.002247 390.30539 462.09894 494.0 0.002024 390.43304 469.62363 532.0 0.001880 390.56119 479.83716 569.0 0.001757 390.68976 492.63452 598.0 0.001672 390.81860 506.98022 619.0 0.001616 390.94800 520.32520 595.0 0.001681 391.07776 528.25293 537.0 0.001862 391.20810 527.28558 518.0 0.001931 391.33887 517.19690 468.0 0.002137 391.46982 501.42581 447.0 0.002237 391.60144 484.33411 431.0 0.002320 391.73352 468.97592 441.0 0.002268 391.86600 456.86230 433.0 0.002309 391.99902 448.40051 452.0 0.002212 392.13223 443.55960 454.0 0.002203 392.26624 441.90787 465.0 0.002151 392.40051 442.84094 488.0 0.002049 392.53540 445.41153 447.0 0.002237 392.67065 448.33191 505.0 0.001980 392.80618 450.41666 476.0 0.002101 392.94250 451.27567 473.0 0.002114 393.07910 451.44287 482.0 0.002075 393.21640 451.81656 468.0 0.002137 393.35394 452.47992 481.0 0.002079 393.49191 452.95209 459.0 0.002179 393.63062 452.74884 455.0 0.002198 393.76962 451.83282 460.0 0.002174 393.90927 450.68103 435.0 0.002299 394.04935 450.13361 448.0 0.002232 394.18973 451.07156 458.0 0.002183 394.33084 454.14090 467.0 0.002141 394.47235 459.37921 489.0 0.002045 394.61453 466.05420 499.0 0.002004 394.75705 472.38696 508.0 0.001969 394.89990 476.10547 482.0 0.002075 395.04358 475.42041 458.0 0.002183 395.18756 470.76144 454.0 0.002203 395.33231 464.10144 453.0 0.002208 395.47729 457.48929 451.0 0.002217 395.62280 452.16556 459.0 0.002179 395.76904 448.41055 432.0 0.002315 395.91568 445.80362 415.0 0.002410 396.06296 443.66516 445.0 0.002247 396.21082 441.61227 454.0 0.002203 396.35886 439.59439 433.0 0.002309 396.50769 437.90439 418.0 0.002392 396.65701 436.33871 418.0 0.002392 396.80698 434.54102 407.0 0.002457 396.95749 432.48349 433.0 0.002309 397.10818 430.51071 415.0 0.002410 397.25983 429.02582 435.0 0.002299 397.41180 428.29019 431.0 0.002320 397.56458 428.14804 445.0 0.002247 397.71771 428.34396 447.0 0.002237 397.87134 428.70264 433.0 0.002309 398.02579 429.11877 445.0 0.002247 398.18054 429.83884 443.0 0.002257 398.33597 431.10291 465.0 0.002151 398.49203 433.13977 449.0 0.002227 398.64850 435.79086 440.0 0.002273 398.80573 438.95422 420.0 0.002381 398.96341 442.47247 443.0 0.002257 399.12183 446.42862 440.0 0.002273 399.28070 451.16068 496.0 0.002016 399.44006 456.64905 501.0 0.001996 399.60025 462.45673 483.0 0.002070 399.76077 467.53812 502.0 0.001992 399.92215 470.75998 482.0 0.002075 400.08401 471.60330 473.0 0.002114 400.24631 470.62643 446.0 0.002242 400.40952 468.95218 442.0 0.002262 400.57306 467.53522 435.0 0.002299 400.73752 466.69946 533.0 0.001876 400.90237 466.40500 475.0 0.002105 401.06775 465.98965 451.0 0.002217 401.23398 464.43204 441.0 0.002268 401.40067 460.88834 404.0 0.002475 401.56815 455.70633 449.0 0.002227 401.73608 450.13556 443.0 0.002257 401.90460 445.14041 432.0 0.002315 402.07397 441.54749 423.0 0.002364 402.24380 439.66037 428.0 0.002336 402.41443 439.46445 449.0 0.002227 402.58572 440.84976 454.0 0.002203 402.75729 443.28354 454.0 0.002203 402.92984 445.97388 446.0 0.002242 403.10291 447.91797 439.0 0.002278 403.27682 448.97928 426.0 0.002347 403.45132 449.08496 425.0 0.002353 403.62619 448.91220 422.0 0.002370 403.80206 449.29147 438.0 0.002283 403.97842 450.74509 453.0 0.002208 404.15561 453.62015 462.0 0.002165 404.33344 457.92334 468.0 0.002137 404.51169 463.36072 482.0 0.002075 404.69083 469.53253 508.0 0.001969 404.87061 476.20139 493.0 0.002028 405.05118 483.57541 510.0 0.001961 405.23236 491.98099 515.0 0.001942 405.41400 501.29852 495.0 0.002020 405.59674 511.05011 544.0 0.001838 405.77985 520.24823 556.0 0.001799 405.96396 527.99225 540.0 0.001852 406.14856 533.34393 522.0 0.001916 406.33377 534.77771 508.0 0.001969 406.51996 530.83380 497.0 0.002012 406.70660 521.55450 503.0 0.001988 406.89420 509.32050 471.0 0.002123 407.08240 496.89584 467.0 0.002141 407.27109 485.89197 444.0 0.002252 407.46088 476.85904 435.0 0.002299 407.65112 469.62857 443.0 . . . loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 0 2 0 1 o 43497.98 39496.43 0.00 6.67772 15.37 0 2 0 2 o 43044.17 39496.43 0.00 6.67772 7.56 1 1 1 1 o 18744.881 18393.959 0.00 6.04525 18.76 1 1 1 2 o 18434.020 18393.959 0.00 6.04525 9.16 2 0 0 1 o 629.878 747.523 180.00 4.81274 0.00 2 0 0 2 o 629.878 747.523 180.00 4.81274 0.00 0 0 2 1 o 32623.322 35225.15 0.00 4.77519 3.64 0 0 2 2 o 33187.809 35225.15 0.00 4.77519 1.86 1 2 1 1 o 6141.443 6528.811 0.00 4.75745 2.20 1 2 1 2 o 5694.272 6528.811 0.00 4.75745 0.93 2 1 0 1 o 161683.25 161740.41 180.00 4.52773 41.11 2 1 0 2 o 160345.42 161740.41 180.00 4.52773 20.25 1 0 2 1 o 221131.08 225762.16 0.00 4.27771 50.05 1 0 2 2 o 217302.13 225762.16 0.00 4.27771 24.40 2 1 1 1 o 124317.67 117669.85 0.00 4.09124 53.13 2 1 1 2 o 122270.81 117669.85 0.00 4.09124 25.94 1 1 2 1 o 122622.96 119694.88 0.00 4.07385 51.57 1 1 2 2 o 118678.75 119694.88 0.00 4.07385 24.71 0 3 1 1 o 431273.1 446019.9 180.00 4.03497 100.00 0 3 1 2 o 437174.0 446019.9 180.00 4.03497 50.54 2 2 0 1 o 86296.76 80853.16 180.00 3.90438 17.19 2 2 0 2 o 81926.96 80853.16 180.00 3.90438 8.05 0 2 2 1 o 51662.70 51757.23 0.00 3.88425 10.09 0 2 2 2 o 51798.13 51757.23 0.00 3.88425 5.04 1 3 1 1 o 84004.32 78413.91 180.00 3.72124 33.20 1 3 1 2 o 82331.19 78413.91 180.00 3.72124 16.14 2 2 1 1 o 184408.52 179538.72 180.00 3.61403 62.59 2 2 1 2 o 182557.42 179538.72 180.00 3.61403 30.78 1 2 2 1 o 521.942 480.016 0.00 3.60202 0.18 1 2 2 2 o 806.914 480.016 0.00 3.60202 0.15 2 0 2 1 o 154184.13 141470.56 180.00 3.38977 23.29 2 0 2 2 o 153272.58 141470.56 180.00 3.38977 11.51 0 4 0 1 o 145122.55 138414.50 180.00 3.33886 12.90 0 4 0 2 o 140984.41 138414.50 180.00 3.33886 6.22 2 1 2 1 o 12912.397 13498.179 180.00 3.28559 3.60 2 1 2 2 o 12546.985 13498.179 180.00 3.28559 1.73 2 3 0 1 o 39380.80 43141.38 180.00 3.26806 5.41 2 3 0 2 o 35086.52 43141.38 180.00 3.26806 2.33 0 1 3 1 o 145345.19 147627.64 180.00 3.09670 16.92 2 3 1 1 o 40614.41 40822.15 0.00 3.09204 10.19 0 1 3 2 o 148389.23 147627.64 180.00 3.09670 8.62 2 3 1 2 o 42547.89 40822.15 0.00 3.09204 5.35 1 3 2 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