#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:17:59 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1216 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000021.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000021
loop_
_publ_author_name
'Harvey, Howard G.'
'Attfield, Martin P.'
_publ_section_title
;
 Synthesis, Crystal Structures, and Properties of Novel Lamellar Gallium
 Methylenediphosphonates
;
_journal_issue                   2
_journal_name_full               'Chemistry of Materials'
_journal_page_first              199
_journal_page_last               209
_journal_paper_doi               10.1021/cm034745q
_journal_volume                  16
_journal_year                    2004
_chemical_formula_sum            'C3.5 Ga N0.5 O7 P2'
_chemical_formula_weight         292.70
_space_group_IT_number           14
_space_group_name_Hall           '-P 2ybc'
_space_group_name_H-M_alt        'P 1 21/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_audit_creation_date             2003-07-10T10:37
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2003-07-10T10:37  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 104.5374(14)
_cell_angle_gamma                90.0
_cell_formula_units_Z            4
_cell_length_a                   11.08476(23)
_cell_length_b                   8.44413(18)
_cell_length_c                   9.44187(14)
_cell_volume                     855.48(3)
_computing_structure_refinement  GSAS
_diffrn_radiation_polarisn_ratio 0.98
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.250182
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_pd_block_id                     2003-07-10T10:37|133MPA|Martin_Attfield|2.3
_pd_calc_method                  'Rietveld Refinement'
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01
_pd_meas_2theta_range_max        80.0
_pd_meas_2theta_range_min        5.5
_pd_meas_number_of_points        7451
_pd_phase_name                   GaP2O7C3.5N0.5H7.5(1)
_pd_proc_2theta_range_inc        0.01
_pd_proc_2theta_range_max        80.00379
_pd_proc_2theta_range_min        5.50379
_pd_proc_info_datetime           2003-07-10T10:37:27
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 2 with  3 terms.
 Cosine Fourier series
      1:    0.00000     2:    0.00000     3:    0.00000    
;
_pd_proc_ls_peak_cutoff          0.00500
_pd_proc_ls_profile_function
;
 CW Profile function number 3 with  19 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 #1(GU)   =   45.788 #2(GV)   =  -13.133 #3(GW)   =    4.293
 #4(GP)   =    0.000 #5(LX)   =    1.131 #6(LY)   =    0.000
 #7(S/L)  =   0.0005 #8(H/L)  =   0.0005
 #9(trns) =     0.00 #10(shft)=   0.0000
 #11(stec)=     4.68 #12(ptec)=     3.41 #13(sfec)=     0.00
 #14(L11) =    0.000 #15(L22) =    0.000 #16(L33) =    0.000
 #17(L12) =    0.000 #18(L13) =    0.000 #19(L23) =    0.000
 Peak tails are ignored  where the intensity is below 0.0050 times the peak
   Aniso. broadening axis   1.0   1.0   0.0
;
_pd_proc_ls_prof_R_factor        0.0600
_pd_proc_ls_prof_wR_expected     0.0654
_pd_proc_ls_prof_wR_factor       0.0751
_pd_proc_number_of_points        7451
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.18
_refine_ls_matrix_type           full
_refine_ls_number_parameters     56
_refine_ls_number_restraints     20
_refine_ls_R_Fsqd_factor         0.17124
_refine_ls_shift/su_max          0.01
_refine_ls_shift/su_mean         0.00
_reflns_d_resolution_high        0.977
_reflns_d_resolution_low         10.730
_reflns_limit_h_max              11
_reflns_limit_h_min              0
_reflns_limit_k_max              8
_reflns_limit_k_min              0
_reflns_limit_l_max              9
_reflns_limit_l_min              -9
_reflns_number_observed          963
_cod_data_source_file            cm034745qsi20030806_113949.cif
_cod_data_source_block           GaP2O7C3.5N0.5H7.5(1)_publ
_cod_original_cell_volume        855.47498
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_original_formula_sum        'C3.50 Ga N0.50 O7 P2'
_cod_database_code               4000021
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y+1/2,-z+1/2
-1 -x,-y,-z
-2 +x,-y+1/2,+z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
GA GA1 0.13938(33) 0.2349(5) 0.6118(4) 1.0 Uiso 0.0191(6) 4
P P1 0.2775(7) 0.0699(9) 0.4064(9) 1.0 Uiso 0.0191(6) 4
P P2 0.0162(7) 0.0579(10) 0.3144(8) 1.0 Uiso 0.0191(6) 4
O O1 0.1021(11) 0.0423(13) 0.7104(15) 1.0 Uiso 0.0107(15) 4
O O2 0.0077(9) 0.1446(15) 0.1687(12) 1.0 Uiso 0.0107(15) 4
O O3 0.2611(10) 0.2093(14) 0.2951(10) 1.0 Uiso 0.0107(15) 4
O O4 0.0094(9) 0.1819(14) 0.4332(10) 1.0 Uiso 0.0107(15) 4
C C1 0.1501(9) 0.9324(12) 0.3659(28) 1.0 Uiso 0.0107(15) 4
O O7 0.4023(10) -0.0161(16) 0.4248(14) 1.0 Uiso 0.0107(15) 4
O O6 0.2812(9) 0.3632(15) 0.0579(12) 1.0 Uiso 0.0107(15) 4
O O5 0.1786(12) 0.0587(12) 0.0048(14) 1.0 Uiso 0.0107(15) 4
C C2 0.4156(14) 0.6035(20) 0.4178(22) 1.0 Uiso 0.0107(15) 4
N N1 0.4372(17) 0.4603(26) 0.3618(10) 0.5 Uiso 0.0107(15) 4
C C3 0.4625(19) 0.6282(16) 0.5674(24) 1.0 Uiso 0.0107(15) 4
C CN1 0.4372(17) 0.4603(26) 0.3618(10) 0.5 Uiso 0.0107(15) 4
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
GA 4.0 -1.354 0.777 15.2354 3.06690 6.70060 0.24120 4.35910 10.7805 2.96230
61.4135 1.71890 International_Tables_Vol_C
P 8.0 0.283 0.434 6.43450 1.90670 4.17910 27.1570 1.78000 0.52600 1.49080
68.1645 1.11490 International_Tables_Vol_C
O 28.0 0.047 0.032 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
C 14.0 0.017 0.009 2.31000 20.8439 1.02000 10.2075 1.58860 0.56870 0.86500
51.6512 0.21560 International_Tables_Vol_C
N 2.0 0.029 0.018 12.2126 0.00570 3.13220 9.89330 2.01250 28.9975 1.16630
0.58260 -11.529 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 GA1 O2 92.3(7) 1_555 . -2_566 N
O1 GA1 O3 87.7(6) 1_555 . -2_566 N
O1 GA1 O4 91.2(6) 1_555 . 1_555 N
O1 GA1 O6 92.9(6) 1_555 . -2_566 N
O1 GA1 O5 179.661(4) 1_555 . -2_566 N
O2 GA1 O3 91.6(5) -2_566 . -2_566 N
O2 GA1 O4 85.3(5) -2_566 . 1_555 N
O2 GA1 O6 173.6(7) -2_566 . -2_566 N
O2 GA1 O5 87.7(6) -2_566 . -2_566 N
O3 GA1 O4 176.7(6) -2_566 . 1_555 N
O3 GA1 O6 84.9(5) -2_566 . -2_566 N
O3 GA1 O5 92.6(6) -2_566 . -2_566 N
O4 GA1 O6 98.3(5) 1_555 . -2_566 N
O4 GA1 O5 88.4(6) 1_555 . -2_566 N
O6 GA1 O5 87.1(6) -2_566 . -2_566 N
O3 P1 C1 113.1(9) 1_555 . 1_545 N
O3 P1 O7 112.5(9) 1_555 . 1_555 N
O3 P1 O6 108.8(9) 1_555 . -2_566 N
C1 P1 O7 111.0(8) 1_545 . 1_555 N
C1 P1 O6 105.9(12) 1_545 . -2_566 N
O7 P1 O6 104.9(7) 1_555 . -2_566 N
O1 P2 O2 105.6(6) -1_556 . 1_555 N
O1 P2 O4 106.8(9) -1_556 . 1_555 N
O1 P2 C1 109.6(8) -1_556 . 1_545 N
O2 P2 O4 108.8(9) 1_555 . 1_555 N
O2 P2 C1 112.6(11) 1_555 . 1_545 N
O4 P2 C1 113.1(10) 1_555 . 1_545 N
GA1 O1 P2 131.2(8) 1_555 . -1_556 N
GA1 O2 P2 127.5(8) -2_565 . 1_555 N
GA1 O3 P1 135.5(7) -2_565 . 1_555 N
GA1 O4 P2 127.8(7) 1_555 . 1_555 N
P1 C1 P2 103.3(6) 1_565 . 1_565 N
GA1 O6 P1 124.4(7) -2_565 . -2_565 N
N1 C2 C3 118.0(7) 1_555 . 1_555 N
N1 C2 CN1 0.0 1_555 . 1_555 N
C3 C2 CN1 118.0(7) 1_555 . 1_555 N
C2 N1 C3 119.7(7) 1_555 . -1_666 N
C2 C3 N1 117.7(7) 1_555 . -1_666 N
C2 C3 CN1 117.7(7) 1_555 . -1_666 N
N1 C3 CN1 0.0 -1_666 . -1_666 N
C2 CN1 C3 119.7(7) 1_555 . -1_666 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
GA1 O1 1.969(6) . 1_555 N
GA1 O2 1.962(6) . -2_566 N
GA1 O3 1.966(6) . -2_566 N
GA1 O4 1.975(6) . 1_555 N
GA1 O6 1.954(6) . -2_566 N
GA1 O5 2.113(6) . -2_566 N
P1 O3 1.558(6) . 1_555 N
P1 C1 1.794(6) . 1_545 N
P1 O7 1.533(6) . 1_555 N
P1 O6 1.528(6) . -2_566 N
P2 O1 1.528(6) . -1_556 N
P2 O2 1.540(6) . 1_555 N
P2 O4 1.550(6) . 1_555 N
P2 C1 1.789(6) . 1_545 N
O1 GA1 1.969(6) . 1_555 N
O1 P2 1.528(6) . -1_556 N
O2 GA1 1.962(6) . -2_565 N
O2 P2 1.540(6) . 1_555 N
O3 GA1 1.966(6) . -2_565 N
O3 P1 1.558(6) . 1_555 N
O4 GA1 1.975(6) . 1_555 N
O4 P2 1.550(6) . 1_555 N
C1 P1 1.794(6) . 1_565 N
C1 P2 1.789(6) . 1_565 N
O7 P1 1.533(6) . 1_555 N
O6 GA1 1.954(6) . -2_565 N
O6 P1 1.528(6) . -2_565 N
O5 GA1 2.113(6) . -2_565 N
C2 N1 1.365(6) . 1_555 N
C2 C3 1.393(6) . 1_555 N
C2 CN1 1.365(6) . 1_555 N
N1 C2 1.365(6) . 1_555 N
N1 C3 1.367(6) . -1_666 N
C3 C2 1.393(6) . 1_555 N
C3 N1 1.367(6) . -1_666 N
C3 CN1 1.367(6) . -1_666 N
CN1 C2 1.365(6) . 1_555 N
CN1 C3 1.367(6) . -1_666 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
350.0 . . .
377.0 0.000783 254.43352 0.0
292.0 0.000839 261.86667 0.0
346.0 0.000803 269.30017 0.0
312.0 0.000825 276.73334 0.0
247.0 0.000872 284.16684 0.0
325.0 0.000816 291.60001 0.0
292.0 0.000839 291.67163 0.0
337.0 0.000808 291.74329 0.0
346.0 0.000803 291.81491 0.0
286.0 0.000843 291.88657 0.0
298.0 0.000835 291.95819 0.0
269.0 0.000855 292.02985 0.0
356.0 0.000796 292.10147 0.0
300.0 0.000833 292.17310 0.0
311.0 0.000826 292.24475 0.0
321.0 0.000819 292.31638 0.0
264.0 0.000859 292.38803 0.0
280.0 0.000847 292.45966 0.0
341.0 0.000806 292.53131 0.0
290.0 0.000840 292.60294 0.0
259.0 0.000863 292.67459 0.0
271.0 0.000854 292.74622 0.0
289.0 0.000841 292.81784 0.0
307.0 0.000829 292.88950 0.0
404.0 0.000767 292.96112 0.0
277.0 0.000850 293.03278 0.0
323.0 0.000818 293.10440 0.0
317.0 0.000822 293.17606 0.0
272.0 0.000853 293.24768 0.0
366.0 0.000790 293.31934 0.0
285.0 0.000844 293.39096 0.0
295.0 0.000837 293.46259 0.0
360.0 0.000794 293.53424 0.0
307.0 0.000829 293.60587 0.0
329.0 0.000814 293.67752 0.0
401.0 0.000769 293.74915 0.0
289.0 0.000841 293.82080 0.0
346.0 0.000803 293.89243 0.0
308.0 0.000828 293.96405 0.0
354.0 0.000797 294.03571 0.0
317.0 0.000822 294.10733 0.0
332.0 0.000812 294.17899 0.0
362.0 0.000792 294.25061 0.0
302.0 0.000832 294.32227 0.0
303.0 0.000831 294.39389 0.0
420.0 0.000758 294.46555 0.0
316.0 0.000822 294.53717 0.0
353.0 0.000798 294.60880 0.0
280.0 0.000847 294.68045 0.0
331.0 0.000812 294.75208 0.0
340.0 0.000806 294.82373 0.0
363.0 0.000792 294.89536 0.0
339.0 0.000807 294.96701 0.0
221.0 0.000892 295.03864 0.0
299.0 0.000834 295.11029 0.0
320.0 0.000820 295.18192 0.0
337.0 0.000808 295.25354 0.0
344.0 0.000804 295.32520 0.0
293.0 0.000838 295.39682 0.0
383.0 0.000779 295.46848 0.0
265.0 0.000858 295.54010 0.0
337.0 0.000808 295.61176 0.0
302.0 0.000832 295.68338 0.0
263.0 0.000860 295.75500 0.0
284.0 0.000845 295.82666 0.0
336.0 0.000809 295.89828 0.0
352.0 0.000799 295.96994 0.0
353.0 0.000798 296.04156 0.0
259.0 0.000863 296.11322 0.0
345.0 0.000803 296.18484 0.0
359.0 0.000794 296.25650 0.0
343.0 0.000805 296.32813 0.0
272.0 0.000853 296.39975 0.0
315.0 0.000823 296.47141 0.0
313.0 0.000824 296.54303 0.0
307.0 0.000829 296.61469 0.0
338.0 0.000808 296.68631 0.0
340.0 0.000806 296.75797 0.0
292.0 0.000839 296.82959 34.93330
314.0 0.000824 296.90125 36.80322
303.0 0.000831 296.97287 38.82697
401.0 0.000769 297.04449 41.02184
409.0 0.000764 297.11615 43.40763
368.0 0.000789 297.18777 46.00708
405.0 0.000766 297.25943 48.84635
333.0 0.000811 297.33105 51.95579
395.0 0.000772 297.40271 55.37066
330.0 0.000813 297.47433 59.13210
415.0 0.000760 297.54596 63.28844
378.0 0.000782 297.61761 67.89669
384.0 0.000779 297.68924 73.02443
358.0 0.000795 297.76089 78.75230
353.0 0.000798 297.83252 85.17715
432.0 0.000751 297.90417 92.41602
441.0 0.000746 297.97580 100.61134
471.0 0.000729 298.04745 109.93791
477.0 0.000726 298.11908 120.61195
390.0 0.000775 298.19070 132.90337
433.0 0.000750 298.26236 147.15234
423.0 0.000756 298.33398 163.79221
484.0 0.000723 298.40564 183.38145
464.0 0.000733 298.47726 206.64914
487.0 0.000721 298.54892 234.56265
503.0 0.000713 298.62054 268.43719
649.0 0.000646 298.69220 310.14346
615.0 0.000660 298.76382 362.57797
757.0 0.000604 298.83545 430.82581
878.0 0.000562 298.90710 524.91846
1024.0 0.000520 298.97873 665.49347
1185.0 0.000480 299.05038 892.95477
1643.0 0.000393 299.12201 1277.22388
2193.0 0.0003233 299.19366 1918.68469
3376.0 0.0002339 299.26529 2926.29541
4963.0 0.0001706 299.33691 4364.40381
7021.0 0.0001262 299.40857 6173.06006
8304.0 0.0001086 299.48019 8063.90869
9996.0 0.0000918 299.55185 9420.84961
9445.0 0.0000967 299.62347 9524.55273
8684.0 0.0001043 299.69513 8308.51465
7034.0 0.0001260 299.76675 6448.35010
5384.0 0.0001591 299.83841 4603.46436
3343.0 0.0002357 299.91003 3104.76953
2276.0 0.0003149 299.98166 2037.74219
1557.0 0.000407 300.05331 1350.38855
1203.0 0.000476 300.12494 936.14154
967.0 0.000536 300.19659 691.35834
766.0 0.000600 300.26822 541.45349
710.0 0.000621 300.33987 442.33829
703.0 0.000624 300.41150 371.18585
508.0 0.000710 300.48315 316.88129
468.0 0.000731 300.55478 273.85516
515.0 0.000707 300.62640 238.99464
427.0 0.000754 300.69806 210.32112
453.0 0.000739 300.76968 186.45642
398.0 0.000770 300.84134 166.39166
421.0 0.000757 300.91296 149.36859
418.0 0.000759 300.98462 134.80753
362.0 0.000792 301.05624 122.25954
390.0 0.000775 301.12787 111.37268
360.0 0.000794 301.19952 101.86819
406.0 0.000766 301.27115 93.52303
321.0 0.000819 301.34280 86.15710
376.0 0.000784 301.41443 79.62379
349.0 0.000801 301.48608 73.80283
301.0 0.000833 301.55771 68.59476
358.0 0.000795 301.62936 63.91680
354.0 0.000797 301.70099 59.69970
370.0 0.000787 301.77261 55.88505
339.0 0.000807 301.84427 52.42341
348.0 0.000801 301.91589 49.27268
350.0 0.000800 301.98755 46.39682
326.0 0.000816 302.05917 43.76486
317.0 0.000822 302.13083 41.35005
307.0 0.000829 302.20245 39.12921
276.0 0.000850 302.27411 37.08216
335.0 0.000810 302.34573 0.0
349.0 0.000801 302.41736 0.0
353.0 0.000798 302.48901 0.0
364.0 0.000791 302.56064 0.0
328.0 0.000814 302.63229 0.0
339.0 0.000807 302.70392 0.0
285.0 0.000844 302.77557 0.0
281.0 0.000847 302.84720 0.0
354.0 0.000797 302.91882 0.0
352.0 0.000799 302.99048 0.0
295.0 0.000837 303.06210 0.0
336.0 0.000809 303.13376 0.0
277.0 0.000850 303.20538 0.0
329.0 0.000814 303.27704 0.0
314.0 0.000824 303.34866 0.0
327.0 0.000815 303.42032 0.0
259.0 0.000863 303.49194 0.0
302.0 0.000832 303.56357 0.0
313.0 0.000824 303.63522 0.0
299.0 0.000834 303.70685 0.0
343.0 0.000805 303.77850 0.0
312.0 0.000825 303.88556 0.0
305.0 0.000830 304.00778 0.0
308.0 0.000828 304.13000 0.0
329.0 0.000814 304.25223 0.0
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163.0 0.00380 176.27443 9.62534
193.0 0.003413 176.28075 9.92915
180.0 0.00357 176.28708 10.32825
159.0 0.00386 176.29341 10.80434
186.0 0.003497 176.29974 11.33097
177.0 0.00361 176.30608 11.88054
176.0 0.00362 176.31241 12.41844
201.0 0.003322 176.31874 12.96849
194.0 0.003401 176.32507 13.40370
180.0 0.00357 176.33141 13.78511
192.0 0.003425 176.33774 14.12499
174.0 0.00365 176.34406 14.42188
189.0 0.003460 176.35039 14.70012
205.0 0.003279 176.35672 14.98668
188.0 0.003472 176.36305 15.22001
188.0 0.003472 176.36938 15.39385
191.0 0.003436 176.37572 15.46128
163.0 0.00380 176.38205 15.37391
182.0 0.00355 176.38838 15.11648
194.0 0.003401 176.39471 14.63836
187.0 0.003484 176.40105 13.98222
181.0 0.00356 176.40736 13.19562
177.0 0.00361 176.41370 12.35823
178.0 0.00360 176.42003 11.49304
184.0 0.00352 176.42636 10.67727
185.0 0.00351 176.43269 9.95224
175.0 0.00364 176.43903 9.35747
167.0 0.00375 176.44536 8.92082
180.0 0.00357 176.45169 8.66237
185.0 0.00351 176.45801 8.59587
197.0 0.003367 176.46434 8.73093
177.0 0.00361 176.47067 9.06966
165.0 0.00377 176.47701 9.61327
176.0 0.00362 176.48334 10.35847
187.0 0.003484 176.48967 11.29905
174.0 0.00365 176.49600 12.42528
179.0 0.00358 176.50233 13.71195
195.0 0.003390 176.50867 15.15837
177.0 0.00361 176.51500 16.72151
178.0 0.00360 176.52132 18.34942
204.0 0.003289 176.52765 19.93665
191.0 0.003436 176.53398 21.48648
199.0 0.003344 176.54031 22.86819
221.0 0.003115 176.54665 23.99921
210.0 0.003226 176.55298 24.81742
214.0 0.003185 176.55931 25.29156
210.0 0.003226 176.56563 25.42500
182.0 0.00355 176.57196 25.25351
192.0 0.003425 176.57829 24.83917
204.0 0.003289 176.58463 24.26100
197.0 0.003367 176.59096 23.60513
222.0 0.003106 176.59729 22.95645
198.0 0.003356 176.60362 22.39209
225.0 0.003077 176.60995 21.97530
209.0 0.003236 176.61629 21.75022
190.0 0.003448 176.62262 21.73594
202.0 0.003311 176.62895 21.95406
196.0 0.003378 176.63527 22.32747
205.0 0.003279 176.64160 22.83820
175.0 0.00364 176.64793 23.44110
219.0 0.003135 176.65427 24.09667
189.0 0.003460 176.66060 24.77043
196.0 0.003378 176.66693 25.46033
186.0 0.003497 176.67326 26.10812
212.0 0.003205 176.67960 26.76428
183.0 0.00353 176.68593 27.37410
200.0 0.003333 176.69225 27.93055
199.0 0.003344 176.69858 28.43177
225.0 0.003077 176.70491 28.88688
197.0 0.003367 176.71124 29.31231
209.0 0.003236 176.71758 29.72170
192.0 0.003425 176.72391 30.12412
207.0 0.003257 176.73024 30.50499
187.0 0.003484 176.73657 30.83355
195.0 0.003390 176.74290 31.03806
199.0 0.003344 176.74922 31.06568
192.0 0.003425 176.75555 30.83717
194.0 0.003401 176.76189 30.29811
206.0 0.003268 176.76822 29.42769
208.0 0.003247 176.77455 28.23907
212.0 0.003205 176.78088 26.78140
172.0 0.00368 176.78722 25.11983
187.0 0.003484 176.79355 23.30940
199.0 0.003344 176.79988 21.43657
190.0 0.003448 176.80621 19.54463
195.0 0.003390 176.81255 17.67502
179.0 0.00358 176.81886 15.90315
160.0 0.00385 176.82520 14.26104
183.0 0.00353 176.83153 12.78158
159.0 0.00386 176.83786 11.55489
167.0 0.00375 176.84419 10.44583
187.0 0.003484 176.85052 9.51829
172.0 0.00368 176.85686 8.79776
175.0 0.00364 176.86317 8.18805
160.0 0.00385 176.86951 7.70711
167.0 0.00375 176.87584 7.35690
186.0 0.003497 176.88217 7.07224
177.0 0.00361 176.88850 6.87425
180.0 0.00357 176.89484 6.74573
151.0 0.00398 176.90117 6.65922
155.0 0.00392 176.90750 6.64696
175.0 0.00364 176.91383 6.68226
168.0 0.00373 176.92017 6.76889
175.0 0.00364 176.92650 6.87207
173.0 0.00366 176.93282 6.98904
159.0 0.00386 176.93915 7.10147
194.0 0.003401 176.94548 7.18902
169.0 0.00372 176.95181 7.22980
182.0 0.00355 176.95815 7.20791
167.0 0.00375 176.96448 7.10229
172.0 0.00368 176.97081 6.94111
179.0 0.00358 176.97713 6.72213
177.0 0.00361 176.98346 6.46373
171.0 0.00369 176.98979 6.17632
173.0 0.00366 176.99612 5.88295
190.0 0.003448 177.00246 5.59433
171.0 0.00369 177.00879 5.32146
169.0 0.00372 177.01512 5.07342
177.0 0.00361 177.02145 4.85089
173.0 0.00366 177.02779 4.67261
156.0 0.00391 177.03412 4.53516
168.0 0.00373 177.04044 4.44001
156.0 0.00391 177.04677 4.38793
175.0 0.00364 177.05310 4.37603
155.0 0.00392 177.05943 4.39709
168.0 0.00373 177.06577 4.45772
154.0 0.00394 177.07210 4.54625
159.0 . . .
181.0 . . .
159.0 . . .
167.0 . . .
152.0 . . .
152.0 . . .
159.0 . . .
165.0 . . .
178.0 . . .
189.0 . . .
176.0 . . .
195.0 . . .
157.0 . . .
199.0 . . .
164.0 . . .
160.0 . . .
185.0 . . .
171.0 . . .
181.0 . . .
177.0 . . .
173.0 . . .
185.0 . . .
172.0 . . .
179.0 . . .
172.0 . . .
174.0 . . .
174.0 . . .
198.0 . . .
160.0 . . .
173.0 . . .
184.0 . . .
187.0 . . .
172.0 . . .
178.0 . . .
202.0 . . .
190.0 . . .
