#------------------------------------------------------------------------------
#$Date: 2025-07-01 14:04:12 +0300 (Tue, 01 Jul 2025) $
#$Revision: 1179 $
#$URL: svn://crystallography.net/testcod/cif/4/00/00/4000007.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000007
loop_
_publ_author_name
'Turrina, Alessandro'
'Garcia, Raquel'
'Cox, Paul A.'
'Casci, John L.'
'Wright, Paul A.'
_publ_section_title
;
 Retrosynthetic Co-Templating Method for the Preparation of
 Silicoaluminophosphate Molecular Sieves
;
_journal_issue                   14
_journal_name_full               'Chemistry of Materials'
_journal_page_first              4998
_journal_page_last               5012
_journal_paper_doi               10.1021/acs.chemmater.6b01676
_journal_volume                  28
_journal_year                    2016
_chemical_formula_moiety         'Al24 P18 Si6 O96'
_chemical_formula_sum            'Al O4 P0.75 Si0.25'
_chemical_formula_weight         121.23
_chemical_name_common
'SAPO-56 calcined dehydrated(trimethylamine,diDABCO-C4)'
_space_group_IT_number           163
_space_group_name_Hall           '-P 3 2c'
_space_group_name_H-M_alt        'P -3 1 c'
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-P 3 2c'
_symmetry_space_group_name_H-M   'P -3 1 c'
_audit_creation_date             2015-02-08T16:20
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2015-02-08T16:20  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                120.0
_cell_formula_units_Z            24
_cell_length_a                   13.75940(31)
_cell_length_b                   13.7594
_cell_length_c                   19.7610(10)
_cell_measurement_temperature    295
_cell_volume                     3239.95(18)
_computing_structure_refinement  GSAS
_diffrn_ambient_temperature      295
_diffrn_detector                 'Linear PSD'
_diffrn_radiation_polarisn_ratio 0.55
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.54056
_diffrn_source                   X-ray
_exptl_absorpt_coefficient_mu    5.251
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 0
 No correction is applied.
;
_exptl_crystal_density_diffrn    1.491
_exptl_crystal_F_000             1434.0
_pd_block_id
2015-02-08T16:20|SAPO-56_calcined_(diDABCO-C4)|A_Turrina|Stoe_STADI_P
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  white
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.01
_pd_meas_2theta_range_max        79.99
_pd_meas_2theta_range_min        3.0
_pd_meas_number_of_points        7700
_pd_phase_name
'from C:/gsas/PhD/SAPO-AFX/C4_calc_S763/SAPO-56.cif'
_pd_proc_2theta_range_inc        0.01
_pd_proc_2theta_range_max        79.99
_pd_proc_2theta_range_min        3.0
_pd_proc_info_datetime           2015-02-08T16:20:16
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 32 terms.
 Shifted Chebyshev function of 1st kind
      1:    466.392     2:   -314.389     3:    129.075     4:   -9.49031    
      5:    5.32373     6:   -93.8336     7:    127.098     8:   -78.9389    
      9:    30.7499    10:   0.718225    11:    16.6162    12:   -39.4733    
     13:    45.8169    14:   -35.7893    15:    11.8680    16:    5.11999    
     17:   -10.3148    18:   0.225960    19:    6.36327    20:   -13.7139    
     21:    6.36103    22:    8.37524    23:   -11.1036    24:    4.20066    
     25:    5.06965    26:   -7.23310    27:    6.91511    28:   -1.15767    
     29:  -0.505350    30:  -0.579267    31:   -3.98019    32:   5.984900E-02
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  16 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 #1(GU)   =  181.418 #2(GV)   =  183.437 #3(GW)   =   -8.805
 #4(GP)   =    5.922 #5(LX)   =   12.444 #6(ptec) =     0.00
 #7(trns) =     0.00 #8(shft) =  -3.5433 #9(sfec) =     0.00
 #10(S/L) =   0.0226 #11(H/L) =   0.0222 #12(eta) =   0.0000
 #13(S400 ) =  0.0E+00 #14(S004 ) =  2.2E-02
 #15(S202 ) = -9.2E-03 #16(S211 ) =  1.5E-02
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   0.0   0.0   1.0
;
_pd_proc_ls_prof_R_factor        0.0472
_pd_proc_ls_prof_wR_expected     0.0409
_pd_proc_ls_prof_wR_factor       0.0598
_pd_proc_number_of_points        7700
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   1.55
_refine_ls_matrix_type           full
_refine_ls_number_parameters     44
_refine_ls_number_restraints     40
_refine_ls_R_Fsqd_factor         0.15609
_refine_ls_shift/su_max          0.05
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        1.201
_reflns_d_resolution_low         11.916
_reflns_limit_h_max              10
_reflns_limit_h_min              0
_reflns_limit_k_max              6
_reflns_limit_k_min              0
_reflns_limit_l_max              17
_reflns_limit_l_min              -16
_reflns_number_total             666
_cod_data_source_file            cm6b01676_si_001.cif
_cod_data_source_block           SAPO-56(C4)_calcined_publ
_cod_original_cell_volume        3239.95(17)
_cod_database_code               4000007
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -y,x-y,+z
3 y-x,-x,+z
4 +y,+x,+z+1/2
5 -x,y-x,+z+1/2
6 x-y,-y,+z+1/2
-1 -x,-y,-z
-2 +y,y-x,-z
-3 x-y,+x,-z
-4 -y,-x,-z+1/2
-5 +x,x-y,-z+1/2
-6 y-x,+y,-z+1/2
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Al AL1 0.0076(6) 0.2299(5) 0.0753(4) 1.0 Uiso 0.0218(7) 12
Al AL2 0.3266(5) 0.4314(6) 0.1741(4) 1.0 Uiso 0.0218(7) 12
P P1 0.10608(31) 0.44279(31) 0.16824(31) 0.75 Uiso 0.0218(7) 12
P P2 0.22761(34) 0.22017(34) 0.08322(34) 0.75 Uiso 0.0218(7) 12
O O1 -0.1161(4) 0.1194(5) 0.1015(4) 1.0 Uiso 0.0246(15) 12
O O2 0.1083(4) 0.1957(6) 0.0959(4) 1.0 Uiso 0.0246(15) 12
O O3 0.0287(7) 0.3479(6) 0.1207(5) 1.0 Uiso 0.0246(15) 12
O O4 0.0084(11) 0.2607(8) -0.00957(31) 1.0 Uiso 0.0246(15) 12
O O5 0.2249(4) 0.4651(6) 0.1542(5) 1.0 Uiso 0.0246(15) 12
O O6 0.0944(8) 0.5475(6) 0.1515(5) 1.0 Uiso 0.0246(15) 12
O O7 0.0786(9) 0.4083(8) 0.24073(26) 1.0 Uiso 0.0246(15) 12
O O8 0.3023(5) 0.3083(6) 0.1337(4) 1.0 Uiso 0.0246(15) 12
Si Si1 0.10608(31) 0.44279(31) 0.16824(31) 0.25 Uiso 0.0218(7) 12
Si Si2 0.22761(34) 0.22017(34) 0.08322(34) 0.25 Uiso 0.0218(7) 12
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Al 24.0 0.000 0.000 6.42020 3.03870 1.90020 0.74260 1.59360 31.5472 1.96460
85.0886 1.11510 International_Tables_Vol_C
P 18.0 0.000 0.000 6.43450 1.90670 4.17910 27.1570 1.78000 0.52600 1.49080
68.1645 1.11490 International_Tables_Vol_C
O 96.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
Si 6.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100
81.6937 1.14070 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 AL1 O2 105.4(4) 1_555 . 1_555 N
O1 AL1 O3 107.6(5) 1_555 . 1_555 N
O1 AL1 O4 113.3(6) 1_555 . 1_555 N
O2 AL1 O3 110.5(5) 1_555 . 1_555 N
O2 AL1 O4 113.0(6) 1_555 . 1_555 N
O3 AL1 O4 107.0(5) 1_555 . 1_555 N
O5 AL2 O6 105.6(6) 1_555 . 2_665 N
O5 AL2 O7 111.8(5) 1_555 . -6_556 N
O5 AL2 O8 111.6(5) 1_555 . 1_555 N
O6 AL2 O7 108.5(5) 2_665 . -6_556 N
O6 AL2 O8 113.1(5) 2_665 . 1_555 N
O7 AL2 O8 106.2(5) -6_556 . 1_555 N
O3 P1 O5 106.1(5) 1_555 . 1_555 N
O3 P1 O6 108.0(5) 1_555 . 1_555 N
O3 P1 O7 111.1(4) 1_555 . 1_555 N
O5 P1 O6 111.6(4) 1_555 . 1_555 N
O5 P1 O7 108.2(5) 1_555 . 1_555 N
O6 P1 O7 111.6(4) 1_555 . 1_555 N
O1 P2 O2 109.1(4) 3_555 . 1_555 N
O1 P2 O4 110.2(7) 3_555 . -2_555 N
O1 P2 O8 104.9(6) 3_555 . 1_555 N
O2 P2 O4 110.8(7) 1_555 . -2_555 N
O2 P2 O8 107.2(5) 1_555 . 1_555 N
O4 P2 O8 114.5(5) -2_555 . 1_555 N
AL1 O1 P2 147.4(6) 1_555 . 2_555 N
AL1 O1 Si2 147.4(6) 1_555 . 2_555 N
P2 O1 Si2 0.0 2_555 . 2_555 N
AL1 O2 P2 145.8(6) 1_555 . 1_555 N
AL1 O2 Si2 145.8(6) 1_555 . 1_555 N
P2 O2 Si2 0.0 1_555 . 1_555 N
AL1 O3 P1 146.3(6) 1_555 . 1_555 N
AL1 O3 Si1 146.3(6) 1_555 . 1_555 N
P1 O3 Si1 0.0 1_555 . 1_555 N
AL1 O4 P2 148.9(7) 1_555 . -3_555 N
AL1 O4 Si2 148.9(7) 1_555 . -3_555 N
P2 O4 Si2 0.0 -3_555 . -3_555 N
AL2 O5 P1 146.5(6) 1_555 . 1_555 N
AL2 O5 Si1 146.5(6) 1_555 . 1_555 N
P1 O5 Si1 0.0 1_555 . 1_555 N
AL2 O6 P1 151.2(7) 3_565 . 1_555 N
AL2 O6 Si1 151.2(7) 3_565 . 1_555 N
P1 O6 Si1 0.0 1_555 . 1_555 N
AL2 O7 P1 152.0(7) -6_555 . 1_555 N
AL2 O7 Si1 152.0(7) -6_556 . 1_555 N
P1 O7 Si1 0.0 1_555 . 1_555 N
AL2 O8 P2 143.6(4) 1_555 . 1_555 N
AL2 O8 Si2 143.6(4) 1_555 . 1_555 N
P2 O8 Si2 0.0 1_555 . 1_555 N
O3 Si1 O5 106.1(5) 1_555 . 1_555 N
O3 Si1 O6 108.0(5) 1_555 . 1_555 N
O3 Si1 O7 111.1(4) 1_555 . 1_555 N
O5 Si1 O6 111.6(4) 1_555 . 1_555 N
O5 Si1 O7 108.2(5) 1_555 . 1_555 N
O6 Si1 O7 111.6(4) 1_555 . 1_555 N
O1 Si2 O2 109.1(4) 3_555 . 1_555 N
O1 Si2 O4 110.2(7) 3_555 . -2_555 N
O1 Si2 O8 104.9(6) 3_555 . 1_555 N
O2 Si2 O4 110.8(7) 1_555 . -2_555 N
O2 Si2 O8 107.2(5) 1_555 . 1_555 N
O4 Si2 O8 114.5(5) -2_555 . 1_555 N
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
AL1 O1 1.700(7) . 1_555 N
AL1 O2 1.720(7) . 1_555 N
AL1 O3 1.747(7) . 1_555 N
AL1 O4 1.728(6) . 1_555 N
AL1 Si2 3.100(7) . 1_555 N
AL1 Si2 3.103(7) . 2_555 N
AL2 O5 1.725(6) . 1_555 N
AL2 O6 1.724(8) . 2_665 N
AL2 O7 1.717(7) . -6_555 N
AL2 O8 1.748(7) . 1_555 N
AL2 Si1 3.118(6) . 1_555 N
AL2 Si1 3.119(8) . -6_555 N
AL2 Si2 3.094(9) . 1_555 N
P1 O3 1.527(7) . 1_555 N
P1 O5 1.531(5) . 1_555 N
P1 O6 1.563(5) . 1_555 N
P1 O7 1.497(5) . 1_555 N
P2 O1 1.532(5) . 3_555 N
P2 O2 1.523(5) . 1_555 N
P2 O4 1.523(7) . -2_555 N
P2 O8 1.508(7) . 1_555 N
O1 AL1 1.700(7) . 1_555 N
O1 P2 1.532(5) . 2_555 N
O1 Si2 1.532(5) . 2_555 N
O2 AL1 1.720(7) . 1_555 N
O2 P2 1.523(5) . 1_555 N
O2 Si2 1.523(5) . 1_555 N
O3 AL1 1.747(7) . 1_555 N
O3 P1 1.527(7) . 1_555 N
O3 Si1 1.527(7) . 1_555 N
O4 AL1 1.728(6) . 1_555 N
O4 P2 1.523(7) . -3_555 N
O4 Si2 1.523(7) . -3_555 N
O5 AL2 1.725(6) . 1_555 N
O5 P1 1.531(5) . 1_555 N
O5 Si1 1.531(5) . 1_555 N
O6 AL2 1.724(8) . 3_565 N
O6 P1 1.563(5) . 1_555 N
O6 Si1 1.563(5) . 1_555 N
O7 AL2 1.717(7) . -6_555 N
O7 P1 1.497(5) . 1_555 N
O7 Si1 1.497(5) . 1_555 N
O8 AL2 1.748(7) . 1_555 N
O8 P2 1.508(7) . 1_555 N
O8 Si2 1.508(7) . 1_555 N
Si1 AL2 3.118(6) . 1_555 N
Si1 AL2 3.119(8) . -6_555 N
Si1 O3 1.527(7) . 1_555 N
Si1 O5 1.531(5) . 1_555 N
Si1 O6 1.563(5) . 1_555 N
Si1 O7 1.497(5) . 1_555 N
Si2 AL1 3.100(7) . 1_555 N
Si2 AL1 3.103(7) . 3_555 N
Si2 AL2 3.094(9) . 1_555 N
Si2 O1 1.532(5) . 3_555 N
Si2 O2 1.523(5) . 1_555 N
Si2 O4 1.523(7) . -2_555 N
Si2 O8 1.508(7) . 1_555 N
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
2163.0 0.0 2136.18579 .
2204.0 0.0 2117.31982 .
2151.0 0.0 2098.65283 .
2070.0 0.0 2080.18262 .
2085.0 0.0 2061.91089 .
2040.0 0.0 2043.83643 .
1956.0 0.0 2025.95813 .
2055.0 0.0 2008.27686 .
2007.0 0.0 1990.79089 .
2017.0 0.0 1973.49902 .
1926.0 0.0 1956.40173 .
1881.0 0.0 1939.49768 .
1943.0 0.0 1922.78540 .
1890.0 0.0 1906.26453 .
1918.0 0.0 1889.93579 .
1944.0 0.0 1873.79468 .
1837.0 0.0 1857.84314 .
1835.0 0.0 1842.07800 .
1848.0 0.0 1826.49976 .
1818.0 0.0 1811.10632 .
1794.0 0.0 1795.89539 .
1756.0 0.0 1780.86780 .
1826.0 0.0 1766.02185 .
1773.0 0.0 1751.35559 .
1759.0 0.0 1736.86621 .
1807.0 0.0 1722.55603 .
1733.0 0.0 1708.42017 .
1709.0 0.0 1694.45898 .
1625.0 0.0 1680.67053 .
1724.0 0.0 1667.05396 .
1692.0 0.0 1653.60632 .
1671.0 0.0 1640.32715 .
1643.0 0.0 1627.21545 .
1681.0 0.0 1614.26770 .
1616.0 0.0 1601.48450 .
1614.0 0.0 1588.86377 .
1596.0 0.0 1576.40295 .
1631.0 0.0 1564.10083 .
1500.0 0.0 1551.95605 .
1597.0 0.0 1539.96704 .
1585.0 0.0 1528.13281 .
1560.0 0.0 1516.45020 .
1495.0 0.0 1504.91821 .
1568.0 0.0 1493.53564 .
1470.0 0.0 1482.30078 .
1485.0 0.0 1471.21094 .
1436.0 0.0 1460.26526 .
1475.0 0.0 1449.46289 .
1433.0 0.0 1438.80090 .
1463.0 0.0 1428.27795 .
1386.0 0.0 1417.89319 .
1393.0 0.000718 1407.64392 1409.17871
1394.0 0.000717 1397.52869 1399.07153
1415.0 0.000707 1387.54651 1389.09741
1431.0 0.000699 1377.69482 1379.25378
1380.0 0.000725 1367.97278 1369.54004
1415.0 0.000707 1358.37842 1359.95386
1296.0 0.000772 1348.91052 1350.49438
1372.0 0.000729 1339.56677 1341.15894
1351.0 0.000740 1330.34558 1331.94629
1349.0 0.000741 1321.24597 1322.85522
1338.0 0.000747 1312.26599 1313.88379
1357.0 0.000737 1303.40417 1305.03064
1280.0 0.000781 1294.65845 1296.29370
1244.0 0.000804 1286.02795 1287.67200
1282.0 0.000780 1277.51074 1279.16370
1270.0 0.000787 1269.10571 1270.76758
1231.0 0.000812 1260.81079 1262.48169
1231.0 0.000812 1252.62451 1254.30457
1212.0 0.000825 1244.54553 1246.23474
1293.0 0.000773 1236.57263 1238.27112
1229.0 0.000814 1228.70386 1230.41162
1308.0 0.000765 1220.93799 1222.65515
1255.0 0.000797 1213.27319 1214.99988
1269.0 0.000788 1205.70874 1207.44495
1213.0 0.000824 1198.24219 1199.98804
1242.0 0.000805 1190.87280 1192.62842
1166.0 0.000858 1183.59937 1185.36475
1231.0 0.000812 1176.42017 1178.19543
1195.0 0.000837 1169.33350 1171.11877
1184.0 0.000845 1162.33838 1164.13367
1125.0 0.000889 1155.43347 1157.23889
1153.0 0.000867 1148.61731 1150.43298
1184.0 0.000845 1141.88879 1143.71484
1187.0 0.000842 1135.24622 1137.08264
1139.0 0.000878 1128.68860 1130.53552
1110.0 0.000901 1122.21448 1124.07202
1183.0 0.000845 1115.82251 1117.69067
1114.0 0.000898 1109.51196 1111.39087
1073.0 0.000932 1103.28088 1105.17065
1029.0 0.000972 1097.12866 1099.02942
1074.0 0.000931 1091.05383 1092.96558
1103.0 0.000907 1085.05518 1086.97815
1094.0 0.000914 1079.13147 1081.06567
1098.0 0.000911 1073.28186 1075.22742
1063.0 0.000941 1067.50500 1069.46204
1097.0 0.000912 1061.79968 1063.76819
1066.0 0.000938 1056.16479 1058.14502
1111.0 0.000900 1050.59949 1052.59143
1043.0 0.000959 1045.10229 1047.10608
1037.0 0.000964 1039.67261 1041.68835
1032.0 0.000969 1034.30884 1036.33667
978.0 0.001022 1029.01038 1031.05042
1062.0 0.000942 1023.77612 1025.82837
1061.0 0.000943 1018.60510 1020.66980
1014.0 0.000986 1013.49603 1015.57324
989.0 0.001011 1008.44836 1010.53821
1032.0 0.000969 1003.46094 1005.56348
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726.0 0.001377 645.52142 709.76355
708.0 0.001412 646.22375 713.20551
689.0 0.001451 646.92902 716.90863
717.0 0.001395 647.63733 720.91479
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1266.0 0.000790 665.47687 1202.15979
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1694.0 0.000590 673.34222 1564.61389
1669.0 0.000599 674.14124 1568.37073
1657.0 0.000604 674.94226 1560.77319
1702.0 0.000588 675.74561 1541.89941
1689.0 0.000592 676.55103 1512.81567
1551.0 0.000645 677.35858 1475.37061
1517.0 0.000659 678.16815 1431.84290
1463.0 0.000684 678.97980 1384.57654
1447.0 0.000691 679.79346 1335.71130
1400.0 0.000714 680.60907 1287.03723
1333.0 0.000750 681.42657 1239.95813
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1177.0 0.000850 684.71606 1084.24463
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989.0 0.001011 688.86884 983.87476
952.0 0.001050 689.70459 976.15637
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978.0 0.001022 693.06415 981.37750
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1002.0 0.000998 694.75342 1003.84851
1022.0 0.000978 695.60016 1019.77222
978.0 0.001022 696.44855 1038.78333
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1046.0 0.000956 698.14960 1086.06250
1083.0 0.000923 699.00226 1114.35400
1135.0 0.000881 699.85626 1145.76599
1130.0 0.000885 700.71161 1180.30432
1103.0 0.000907 701.56830 1217.95923
1193.0 0.000838 702.42603 1258.69763
1121.0 0.000892 703.28528 1302.45752
1261.0 0.000793 704.14569 1349.13831
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1291.0 0.000775 705.87006 1450.63806
1347.0 0.000742 706.73401 1505.01538
1432.0 0.000698 707.59906 1561.42029
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1594.0 0.000627 711.06958 1798.97327
1631.0 0.000613 711.93982 1859.65381
1722.0 0.000581 712.81091 1918.30908
1906.0 0.000525 713.68292 1975.17285
1930.0 0.000518 714.55585 2029.52246
1941.0 0.000515 715.42957 2080.61816
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2038.0 0.000491 717.17938 2170.05737
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2136.0 0.000468 718.93237 2237.60400
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1912.0 0.000523 727.73517 2124.11938
1887.0 0.000530 728.61823 2074.53882
1789.0 0.000559 729.50165 2020.73779
1746.0 0.000573 730.38544 1963.64270
1692.0 0.000591 731.26953 1904.14856
1657.0 0.000604 732.15381 1843.09814
1692.0 0.000591 733.03845 1781.26624
1578.0 0.000634 733.92340 1719.35059
1484.0 0.000674 734.80847 1657.97009
1469.0 0.000681 735.69385 1597.66418
1418.0 0.000705 736.57928 1538.89526
1352.0 0.000740 737.46478 1482.05298
1284.0 0.000779 738.35046 1427.45813
1286.0 0.000778 739.23602 1375.36621
1301.0 0.000769 740.12177 1325.97363
1266.0 0.000790 741.00751 1279.41968
1174.0 0.000852 741.89319 1235.79431
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1124.0 0.000890 744.54993 1122.71265
1107.0 0.000903 745.43518 1090.83679
1052.0 0.000951 746.32019 1061.73608
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885.0 0.001130 836.82434 974.17365
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879.0 0.001138 839.56580 1002.44086
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2044.0 0.000489 879.53748 2010.29956
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2266.0 0.000441 886.74786 2287.01538
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266.0 . . .
